DE2445163A1 - COSMETIC PREPARATION - Google Patents

Description

- PATENT AGENCY OFFICE

ERLlN - MUNICH

PATENT LAWYERS

DIPL-ING. W. MEISSNER (BLN) DIPL-ING. P. E. MEISSNER (MCHN) DIPL-ING. H.-J. PRESTING (BLN)

1 BERLIN 33, HERBERTSTR. 22nd

Your sign Your letter from Our Sign Berlin, September 19, 1974

The Quaker Oats Company, Merchandise Mart Plaza, Chicago, Illinois, USA

Cosmetic preparation

Summary:

Improved cosmetic preparations are obtained through a content of finely divided oat flour.

The invention relates to improvements in cosmetic preparations.

A wide variety of cosmetic preparations is available Grouting, and the cosmetic industry is constantly striving to make cosmetics both functional and aesthetic

to improve in points of view.
σ

The main aim of this invention is therefore improvements in kosiNj rivet approaches.

° A specific object of the invention are liquid ingredients to and / or solid components in cosmetic preparations,

BORO MÖNCHEN: TELEX:

MONKS 22
ST. ANNASTR. 11

TELEGRAM: PHONE: BANK ACCOUNT: CHECK ACCOUNT: INVENTION BERLIN BERLINER BANK AG. W. MEISSNER, BLN-W BERLIN 030/885 60 37 BERLIN 31 122 82-109 030/886 23 82 3695716000

which also contain small solid material in a form desired for application to the skin.

The invention is based on the discovery that oatmeal of a defined particle size is advantageously cosmetic Approaches can be incorporated to impart various desirable properties, such as absorption.

i
and to give the skin a supple feel and appearance. The finely divided oatmeal has the necessary adhesiveness so that it adheres to the skin after the volatile components of the cosmetic formulation have evaporated.

The oat flour, which has been found to be particularly useful in cosmetic preparations according to the invention, is a finely divided material with a particle size in which more than 98 % passes through a 200 mesh sieve (clear mesh size 0.074 mm), USSieve Series, and preferably at least about 95 % pass through a 325 mesh sieve (clear mesh size 0.044 mm). The flour is used in cosmetic batches in amounts of about 1 to 20 % or more of the batch weight. This finely divided oatmeal can be characterized in such a way that it forms colloidal dispersions in solvents and therefore remains suspended in liquid carrier media for extended periods of time. This particular oatmeal is obtained by grinding oatmeal in a conventional manner followed by air classification to obtain the desired particulate material. On a dry basis, this oatmeal has a relatively high content of starch (generally above 7 o%) and lipids (generally 7 »6 %) and a relatively low content of gum, ash (generally below 2.5 ^) and fiber (generally below 0 , 6 %) and a protein content generally of about 16 % or less, with virtually no degradation of the protein as the pail would be if the flour were obtained by repeated milling, sieving or sieving operations.

The special oat flour can advantageously be used in a very wide range of cosmetic preparations. The oatmeal shows compatibility with the ionic and

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nonionic materials commonly used for emulsification purposes; it is rapidly in numerous liquid Solvents disperse and subject to water of hydration, with which there is an increase in apparent Viscosity leads. In emulsion systems containing a certain amount of oil, the flour presents no processing problems and leads to cosmetic preparations which are extremely satisfactory from a cosmetic point of view. The special oatmeal can be successfully incorporated into cosmetic preparations such as hand lotions and creams To obtain an aesthetically elegant system that the confectionery process runs of protein and the softening properties and moisturizing properties. hydrophobic lipid materials owns. The oatmeal can be incorporated into the aqueous phase of such systems just prior to a heating operation, if such is required.

Moisturizing creams and lotions can be prepared with the oatmeal which among others o ^ e-wden. and soft making the skin a soft, cutting edge. ° iriff awards. Night creams and lotions can be used with be compounded with the special oat flour. These systems can be configured to achieve pH values which πenen come close to normal skin. Because the oatmeal is compatible with various residues of cosmetic approaches, it becomes possible to produce products with a pH of approximately 5.5 (about skin pH) equip. As a v / ashes with soaps or other alkaline detergents are usually the normal ones Acid mantle changes the skin, the use of on can approximate Approaches geared towards the skin pH of normal skin help a rough, dryjrissiece to heal epidermis. The physical Presence of oatmeal on the skin after evaporation of relatively volatile components such as water or water Alcohols provide a very desirable skin feel.

The uses of oatmeal in under-malaip moisturizers and lotions these products can not just match the desired ones. The properties of moisture, but that

* In

S09812 / KK3 BAD ORIGINAL

Flour also helps various makeup types adhere to the surface of the skin. Since oatmeal contains whole protein, which is a polymer-like material is believed to have this desirable property with this as well as the others Components in the flour is related. This means a downgraded need for makeup refresh in the course of a day. In addition, the flour helps as a result of it Oil and water adsorption properties, the makeup before streaking or discoloration due to evaporation or the. Oils. Which can be found on the surface of the epidermal layer are to protect.

Mostly, cleansing lotions and creams emulsion systems containing a certain amount of oils is between 15 and 5o wt -.% Vary. These systems are intended for the removal of many cosmetic preparations such as lipsticks, face make-up and eye make-up using solvent and emulsification mechanisms. In some cases, products are formulated so that they can be removed from the face with water after the cleansing operation. In other cases, these masses must be rubbed with cloth after they have been used to remove various cosmetics. In any case, they offer a cleaning function that differs from that provided by soap. These systems can be equipped to approximate the pH of the normal epidermis in contrast to most soaps, which in turn tend to be somewhat alkaline. Furthermore, these lotions and creams are less easy to emulsify and remove lipids normally found on the surface of the epidermal layer, thereby defatting and potentially exposing the skin to more flammability.

Oatmeal can not only be incorporated into cleansing lotions and creams due to its protein content a skin conditioning It also has moisturizing properties due to the presence of lipids. Cleansing creams and lotions are not just mildly effective Removal of "make-up", environmental residues such as dust and

609812/1043

Dirt, but they also provide an excellent method of drying and moisturizing dry skin. Oatmeal can cleansing creams and lotions for the individual user who find this method of cleaning more acceptable than with soap.

Oatmeal in anhydrous bath oils enhances the positive

Properties of eating, moisturizing and softening, attributed to the oils such as mineral oil, lanolin derivatives or fatty acids used in these products will. In addition, the dermatological properties inherent in oatmeal due to its protein and lipid content complement each other further the effect of the anhydrous bath oil.

The addition of this special oatmeal helps alleviate oatmeal because of its emollient properties Inflammation of the skin which can develop without affecting the foam properties of the bath oils.

Massage lotions and creams can be equipped so that they combine a number of useful properties when oatmeal is used as one of the batch ingredients. The system can be designed to approximate the normal epidermal acid mantle. This can be achieved by using batch ingredients such as nonionic emulsifying agents that prevent the incorporation of substances allow the. to maintain a hydrogen! on concentration corresponding to a pH of about 5 »5 can be used. Using oatmeal in situations that require this pH will not result in a mass with tolerance issues.

Oatmeal can also contribute to the stability of these emulsions due to an effect on the apparent viscosity of these Systems as well as the solubility properties contribute. Oatmeal seem to have hydrophilic (water-affine) as well as lipaphilic groups, which obviously show the value of the flour as Determine emulsifying agent. Apparently the condi-

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tioning effects of protein play a role in enhancing the functional properties of massage products and related products. The presence of fat in the flour offers moisturizing effects.

The use of protein in shampoos and the market success of these products is well known. The so-called protein, however, the one used in these products is usually Stertes collagen, which contains amino acids, polypeptides and other protein residues contains. In the case of oatmeal, the protein found in this material is not hydrolyzed and therefore quite. Oatmeal contains lipids, which also applies to the surface of the brain shell. These lipids help the hair fiber to give a healthy shine. In addition, they can desolate the cuticle layer of the fiber, so that it is Let cells gently move past the cells of neighboring fibers, which makes combing easier. Oatmeal can be used in shampoos can be incorporated without adversely affecting the foam properties.

Shampoos can be made up in the form of creams and liquids. In the case of liquids, these can be low to have nutifere apparent viscosity. The oatmeal is suitable for use in any of these products, however the method of incorporating the material will vary. in the Case of liquid shampoos with a low to low viscosity For example, the easiest way to incorporate the oatmeal is by making an aqueous dispersion of the flour.

In the case of hair conditioning agents, the use of oatmeal is advantageous because of its protein and lipid content. Hair conditioning agents are usually used for Treatment applied to those people whose hair has been damaged by the use of hair dyes, hair waving products, hair combs, Hoow to i * urw and other procedures that are normally a Damage to the cuticle or hair fiber protein has been injured. An injury to the cuticle can / and. manifests itself r-m. unsightly split ends, with damage to the protein of the fiber,

509812/1043

which is far more serious, can manifest itself as hair breakage and hair loss. Treatments containing lipid conditioning agents and other lipid conditioning agents are widely used in an attempt to relieve this undesirable stanoia. Usually the use of a conditioning agent is a cover-up because the problem is usually not resolved, but the fiber continues to grow through the use of conditioning products, creating a new, undamaged fiber. Some researchers have vervwvl4et aw & a / vic ( the use of devices for measuring the tensile strength of fibers that hair conditioning agents containing protein can increase the strength of individual fibers. From an aesthetic point of view, the use of conditioning agents containing protein as well as setting agents such as special Cationic Materials ^ make hair shiny, manageable, softer, and sometimes thicker The use of bulk oatmeal of this type provides whole protein derived from a "natural" source, as well as lipids.

Hair sprays and setting aids contain, in large part, high polymers as hair "hold" ingredients. Compositions containing these materials are marked by the manufacturer as providing various holding properties which modify the hair by imparting a relatively stiff to soft natural frizz. By incorporating various ingredients / it is possible, such as plasticizers and neutralizing agents, in such systems with resins containing functional carboxyl groups _; change the firmness of the seat while maintaining the holding properties under adverse environmental conditions such as high humidity. The use of oatmeal as a resin modifier provides the manufacturer with a material in hydroalcoholic systems that contains protein, which is used to condition the hair, as well as lipids, which help to impart a shine. The natural origin of the flour and its pro-content make it particularly suitable for products of this type.

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Face masks are widely used to treat various undesirable, to help treat conditions related to the epidermis. They can be used in treating oily skin to give it lipid adsorption effects. They are sometimes used to help suppress wrinkles by exercising a contracting effect. They are sometimes used to treat acne and other related problems with, phenomena in adolescence or hyperactive

{_verwew «cr
Sebum glands by incorporating antibacterial agents as well as auxiliary agents such as aluminum phenol sulfonate. In addition to absorbing excess oils, this natural flour with its protein content is particularly good in products of this type.

Cleaning> utU6 can be strong in their form and function vary. The cleaning composition can take the form of a moderately viscous Take in fluids which contain a certain amount of contains synthetic surfactant material that is used for careful Cleansing the skin is used. The re-ripple effect In this case, the colloidal character will be emulsified and finally unrrsemulsified Dispersing effect of the surface-active material attributed to. This type of product is suitable for "oily skin", but may cause epidermal inflammation in some people cause. The use of oatmeal in cleaning masses of this kind he can help in degrading the skin. t help without fat and a possible associated inflammation that cleaning effectiveness is sacrificed. These detergents can also use various antibacterial agents like Hexachlorophene for the purpose of eliminating various on the Surface of the skin containing orgasms taking place. The use of these antibacterial agents can be a source of additional epidermal inflammation, which is reduced by the incorporation of oatmeal.

Detergents can also take the form of various dispersions have insoluble solid materials, like almond flour in polyhydric alcohols like glycerin or propylene glycol. These not only offer one attributable to the solvent (glycol) Cleansing, the solid, insoluble matter also serves to gently massage the skin and

509812/10 A3

BATH ORIGINAL

speed up. Incorporation of oatmeal in
Masses based on dispersions of various insoluble
solid materials in polyhydric alcohols provide product properties that are based on the protein and lipid content of the flour. The flour supports the skin cleansing operation by effectively removing residues, which is brought about by massaging with the oat flour dispersed in GlycoC.

As the name suggests, skin fresheners are used to create a
A feeling of refreshment and cooling after a bath or one
Shower or used during the day. Skin fresheners can fuse in such a way that they aid in the removal of makeup through their solvent properties - because of these properties they also impart a cool * sensation
and sometimes a skin-tightening effect. Fresher or toiletries such as aftershave lotions can also be considered
Media are used for imparting fragrance, deodorant, astrings ^ and massaging properties on numerous

Area / body, hands and face. They can be used in connection with the daily routine care of persons such as bathing or showering. They can also be used in the course of a day- »around those mentioned above To impart properties as well as cooling and refreshing effects.

It was previously known that the incorporation of talc powder in skin fresheners which contain a liquid carrier medium such as alcohol or agents containing alcohol and water, is very desirable. Because talcum powder absorbs moisture and makes the skin 'soft and smooth' to the touch!

So far, attempts to incorporate talc or talc have met
related materials to serious difficulties in preparation. The incorporation of talc and related components such as magnesium silicate, calcium silicate,

Magnesium carbon at and / or zinc st ecu? at in such
Systems usually leads to sedimentation of these solids

ΒθίβΙί / 104-3-.

-1ο-

because of their poor hydration properties in the suspension vehicle. Even ^el application of the so-called suspending or dispersing agents such as high polymers or surface-active agents, it is difficult to disperse these materials uniformly, so that at. Use of euvtes cleaning agent the powdery components are applied unevenly. A non-uniform layer of the powdery materials is deposited and white areas of high concentration become visible. The aesthetics of such a situation is obviously unacceptable. The use of special oatmeal in products of this type enhances the functional properties of the mass not only because of the proteins and lipids it contains, but also because of the smooth, velvety properties of the residue on the skin that are imparted after the solvents such as water and alcohol have evaporated.

The following numbered examples illustrate representative cosmetic compositions according to the invention, their preparation and properties. The particular oatmeal used in these examples is the particulate oatmeal previously described.

Example 1 imÄfevtJL-

Pigmented Systems Properties: Feuchi? ICondi-

Skin care with anionic

Oil / water systems for use under makeup for a more natural look Skin tone. to rent.

Ingredient % w / w

1. Myvacet type 9-4o o, 25

2. Stearic acid (triple pressed) 3.5

3. Glycerol monostearate (not itself

emulsifiable) 1.7

4. Lanolin (cosmetic grade) 2, ο

5. Mineral oil (65/75 Saybolt) 8, ο

6. propyl paraben o, 1

7. methyl paraben o, 1

8. Special oatmeal 1.5

9. Deionized water QS 100, oo

609812/1043

1ο. Propylene glycol 3 »ο

11. Titanium dioxide 2, ο

12. Eed ^ 2513 ο, 9

13. Ultra Blue 3585 ο, 2 14-, triethanolamine 1, o

15. Dowicil 2oo o, 1

16. Perfume QS

Compounding procedure;

We weigh Wr. 1 to 6 / and heat to 7o-73 ° C »during is continuously stirred. Weigh / VV- 7 to 1o and heat

ο ' ^K

at 7o-73 C; add the ^/ to the heated 01, the phases are combined (both phases should be at 7o-73 ° C). Add numbers 11, 12 and 13 and mix until uniformly dispersed. Add 14, cool to 35-4o ° 0 and add 15 and 16. Fill in e * <. 25-3o ° G.

Example 2

Pigmented systems properties: moisture conditioning ^ * ee ' ^ anionic / nonionic oil / "ί. / Water emulsion system for use

under makeup to give a more natural skin tone.

Component 509812/1043 % W / w 1. Lantrol o, 3 2. Stearic acid (triple pressed) 3.25 5. Polawax 1.5 4. Mineral oil (65/75 S ^ -Bolt) 6, o 5 PropyIparab en o, 1o 6. methyl paraben o, 1o 7. Special oatmeal 2, o 8. Deionized water QS 1oo, oo 9 «propylene glycol 4, o 1ο, titanium dioxide 2, o 11. Lo Micron Pink // £ 2511 o, 7 12th lellow // 2576 o, 3 13. Red // 2513 o, 1 14. Dowicil 2oo o, 1o 15. Perfume QS 16. Triethanolamine 1, o

Kompoundx erpro ζ edur:

Weigh the oil phase [insert No. 1-5; start stirring and heating. Heat to 70-73 ° C. Weigh No. 6.7-8 and 9 and warm to 70-73 ° C. with stirring. Add the "aqueous" phase to the oil phase. Continue to stir and füp; e Hr. 1o, 11, 12 and 13 added. Stir until a uniform dispersion results. Add number 16. Cool to 35-4o ° C. Admit numbers 14 and 15. Fill at 25-yo ⁰ C e \ M.

Example 3

Pigmented systems properties: wears the same Lipstick moderately on, suppleness and

Sa good "glide"

Carnauba wax component % W / W ,O component Ceresin wax Titanium dioxide 5, o , 25 1.Candelilla wax Emerwax 4266-0 D&O Red // 21 2, o , 5 2. Getiol V D&C Red 447 1.5 .25 3. Mineral oil (65/75 Saybolt) QS . Castor Oil 1.5 4th Beeswax 4, o 5. Lanolin (cosmetic grade) Ιοο, οο 6th Amerlate P 8, o A 7. . Viscolan 1o, o 8th. . Special oat flour 1o, o 9. . Pigments 5, o 1o. Pigment base 2, o 11 47, o 12, 1. 2. Parts by weight B 3. 7th 4th 1 1 4o

Compounding procedure:

Weigh in phase A (No. 1 - 1o) and start heating and to stir. Heat to about 8o C and mix until all waxes melted. Prepare Part B several hours in advance

509812/1043

before by adding No. 1 - 3 to Wr.4 and editing with a roller mill. Cool part A to 70-73 ° C and add number 11 and Part B (No.12). Mix carefully and pour into molds.

Example 4

Pigmented Systems Properties: Excellent

Glide, lubricious, good coverage

component % W / W • 1. Candelia wax 5, oo Parts by weight 2. Carnauba wax • 2, oo 8, oo 3. Ozocerite 1.5o 2.25 4. Emerwax 4266-0 1.5o 1.5o 5. Getiol V 4, oo 35.25 6. Mineral oil (65/75 ^ AoIt) 5, oo 7. Beeswax 8, oo 8. Lanolin (cosmetic grade) 1o, oo 9. Oastor Oil QS 1oo, oo 1o.Special oatmeal 2, oo 11. Color pigments 47, oo Pigiiient approach: component 1. Titanium dioxide 2. D&C Red # 19 3. D&C Red # 21 4. Castor Oil

Compoung / cPer procedure:

Weigh in phase A (No. 1 - 9) and start heating and to stir. Heat to about 80 ° C and mix until all Waxes have melted. Prepare part B several hours beforehand by adding No. 1 - 3 to the castor oil and processing with a roller mill. Cool Part A to 7o - 73 ° G and add No. 1o and Part B (No. 11). Mix carefully and pour into molds.

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Example 5

Pigmented systems Properties: moisture retention,

Makup cream S ^ cover, by nature 4->

vagi, «iciuc oil / water ^ anionic) emulsion

component % w / w 1. Avocado oil 4.0 2. Lanolin (cosmetic grade) 2.00 3. Stearic acid (triple pressed) 4.00 4. Glyceryl monostearate (itself not emulsifying) 5, oo 5. stearyl alcohol 2.00 6. Mineral oil (65/75 Saybolt) 4.00 7. Cetiol V 5.00 8. Propyl paraben o, 1o 9. methyl paraben o, 1o 1o. Triethanolamine 1, oo 11. Propylene glycol 5, oo 12. Dowicil 2oo o, 1o 13. Special oatmeal 2, oo 14. Deionized water QS 1oo, oo 15. Perfume QS 16. Titanium dioxide 3.5o 17. Lo Micron Brown 2593 1,3o 18. Lo Micron Pink 2511 o, 3o 19. Lo Micron Yellow 2576 o, 2o

Compoundi erprο ζ edur:

Weigh the ^{M n} oil phase a (ingredients no. 1 - 8) to heat and early "and stir ^ fian FÜA · the aqueous phase to the oil phase. Stirring was continued. Pigments No. 16, 17, 18 and 19 are added. It should be done until the pigment has diapered homogeneously. Add No. 1o. Cool to 35- * ο ° σ and add Np. 12 and 15 too. Fill in at 25-30 ° C.

5098T2 / 10A3

Example 6

Pigmented systems Properties: Uniform distribution

Auara shadows aeckungι supple anionic

Shadows under the eyes ■. Oil / water emulsion, good adhesion

Component # W / W

1. Mineral oil (65/75 Saybolt) 8, ο

2. Amerlate P 2, o.

3. Stearic acid (triple pressed) 4, ο

4. Glycerine monostearate (not itself
emulsifying) 5 »o

5. Cetyl alcohol 2, ο

6. Getiol V 5, ο

7. Propylp arab en ο, Λ ο

8. Methyl paraben .. o, 1o

9. Special oatmeal 1, o

10. triethanolamine 1, o

11. Propylene glycol 5 »o '

12. Dowicil 2oo o, 1o

13. Deionized water QS 100, oo

Pigments:

1. Chromalite I> ark Blue. 3.5

2. Ghromaly Magenta 2 »o

3. Pearl Glow 5.0

Compoundi erpro ζ edur:

Weigh in the ^M Oil "phase components (No. 1 - 7)» start heating and stirring. Heat to 7o-73 0. · Weigh No. 13 »11» 9 and 8 into another container and begin stir and heat. heat to 73 ° 7o-0 "give the components located at 70-73 ⁰ C .the aqueous phase to the oil phase components. lie part A are added and mix, mixed uniformly until the pigments. fullness No. and cool to 35-4o ° C, at which temperature is added No. Fill at 25-3o ° C.

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-'Ib-

Example 7 Material for skin treatment Properties: solvent cleaning effect , adsorbing, conditioned, massage properties due to the insoluble materials

Components 1. Propylene glycol 2. Sorbitol 3. Methyl paraben 4-. Special oat flour 5. zinc oxide 6th Talk 7th Sorbic acid 8th. Formaldehyde solution 9. Deionized water 1o . Perfume 11 . dye

QS

% W / W 17.5oo 17.5oo o, 1oo 15,000 Ιο, οοο 2o, ooo o, 1oo

o, o75 1oo, oo

QS
QS

Compoundi erprο ζ edur:

Weigh in in the order No. 1 to No. 10 while is continuously stirred. Mix about 1.5 hours after all ingredients have been added and continue mixing when pouring in.

example

Masses for skin treatment mud pack

Components

1. Sorbitol

2. Deionized water

3. Methyl paraben 4-, fuller's earth

5. Special oatmeal

6. Dowicil 2oo

QS

fo V / / W

5, ooo

Ιοο, οοο

o, 1oo

3o, ooo

5,000

o, o75

Compounding prοζedur: Man wiefre Iv. 1, 2 to stir. Man for ^? ir.

, 3 and 6 in a container and start

4 and 5 and stir until a 509812/1043

- ^1? - 2,5163

results in a mild homogeneous paste.

Example 9

Hasser: for skin treatment Properties: astringent, con

conditioned, softens the skin

ti w * R ^ ke · and smooths, the appearance helps

of lessening wrinkles

Koinpoundi erpr ο ζ edur:

Weigh in No. 3 and add while / stirring ^ continuous endern ^ No. 1 and 2 too. Heat to 7o - 73 O, start cooling, after mixing at this temperature for 15 minutes. Continue stirring and add # 4 and 5 at 5o-5 <4- ° 0 and no. 6. Continue stirring and cool and add No. 7, 8 and 9 at 25 - 30 ° C.

example

Skin treatment agents Properties: Conditioning,

emulsifies and dispenses and erface and body / shampoo desired epidermal materials

like makeup, dust and dirt, good foam properties

component % W / W Special oat flour 5, oo Gelvatol 3 / 9o 1o, oo Deionized water QS 1oo, oo Glycerine 1, oo Resyn 226o 5.00 Ethyl alcohol SDA ^ Ao 16, oo 2-amino-2-methyl-1,3-propanediol o, o2 dye QS Perfume Q5

Component # W / W

1. Standapol SH-I00 5o, oo

2. Standamid SD 4.00

3. Deionized water QS 100, oo

4. Special oatmeal 1, oo

5. Propylene Glyco1 3.00

6. Perfume · QS

7. Dye QS

8. Dowicil 2oo 509812/10 ^ 3 o, 1o

Compound learning proζedure:

Weigh No. 1 - 5 into a container ^ begin to heat and stir. Heat to 6o-63 ° G while stirring carefully to avoid air pockets. Stir until the resulting dispersion is uniform. Cool to ^35-0

and admit No. 8. Cool to 25-30 ° C and add Vv and 7.

Example 11

Means for skin treatment properties: A / dstringens, konfxpqirhtqmaqkP conditioning, creates a cooling

Besxcn-csmasKe feeling when applied, is light

Wash off with water.

Component % W / W

1. Deionized water QS 100, oo

2. Veegum 1o, oo

3. Special oatmeal 4, oo

4. Methyl paraben o, 1o

5. Dowicil 2oo ο, ϊο

6. Ethyl alcohol (SDA & 4o). 18, oo

7. Dye QS

8. Perfume QS

Compounding pro ζ edur:

Weigh in No. 1 and start stirring. Add No. 2 and mix until the dispersion obtained is homogeneous and free of lumps is. Add # 3 $ 4- »5» 6, 7 and 8. Put that Continue mixing until the dispersion is homogeneous.

Example 12

Skin protection properties: Anionic, moisturizing

Holding hand and body lotion, not greasy

Component % W / W

1. Stearic acid 3,000

2. Cetyl alcohol 0.5o

3. Mineral oil (65/75 Saybolt) 7 »oo

4. Methyl paraben o, 1o

5. Propyl paraben o, 1o

50 981271043

6. Deionized water

7. Special oatmeal

8. Triethanolamine

9. Propylene glycol

10. Dowicil 2oo

11. Perfume

12. Dye

Konipoundi eration pro ζ edur:

Weigh the ingredients Rr.

heat with stirring at about 72 ⁰ C. In another container to cradle 6 7 No., 8 and 9 and heat with stirring to 72 ⁰ C. It add the water phase to Ülphase and cool with stirring to about 4o C, wherein which temperature No. 1o, 11 and 12

should be admitted.

Example 13

Skin protection properties: Anionic, moist

Holding hand and body crosses, non-fatty, can to

Massage purposes can be used.

3, 2AA 5163 QS 1oo, oo 1, oo 1, oo 5, oo o, 1o QS QS 1, 2, 4 and 5 a and e:

component % W / W 1. Stearic acid (triple pressed) 4, oo 2. Emerwax 4266D 4, oo 3. Fluid E37o 5, oo 4th Mineral oil (65/75 Saybolt) 5, oo 5. Propyl paraben o, 1o 6th Methyl paraben o, 1o 7th Deionized water QS 1oo, oo 8th. Dowicil 2oo o, 1o 9. Special oat flour 1, oo 1o . Triethanolamine 1.00 11 . Perfume QS

Compounding procedure:

Weigh the ingredients No. 1 - 6 into a container and heat to about 72 ° C while stirring. Weigh Mr. 7, 9 and 10 in a separate container and heat this to 72 ⁰ O with stirring. Add / water phase components to the

He 509812/1043

BAD OFHGlMAL

Oil phase and cool to about 40 ° G. See nos. 8 and 11.

Fill in at 25-3o ° G.

example

Skin protection properties: Non-ionic, moist

Hand and body lotion pfa ^ efpdT ^^ ' ^{nichtfetterad} '

component QS % W / 1. F omulgen 4, oo 2. Mineral oil (65/75 Saybolt) 8, oo 3. Getyl alcohol 1.5o 4th Pr opy Ip ar ab en o, 1o 5. Methyl paraben o, 1o 6th Deionized water 1oo, oo 7th Special oat flour 1, oo 8th. Propylene glycol 5, oo 9. Dowicil 2oo o, 1o 1ο . Perfume QS 11 . dye QS

Compounding procedure:

Weigh ingredients No. 1 to 4 into a container and heat to 70-73 ° C. while stirring continuously. Weigh No. 5 »6, 7" and 8 into another container and start heating while stirring continuously. Heat to 7 o - 73 G and then add this emulsion phase (water phase) to the oil phase, which is also used in a The temperature should be maintained between 70 ° and 73 ° C. Stirring should take place when the two phases are combined with a high-performance shear mixer.

Example 15 -

Skin protection properties: cooling, gives skin condi-

Skin freshening and fire effects

Component # W / W

Special oat flour (2% dispersion in deionized water) 5o, oo Garbopol 9 ^ o (2 percent dispersion

in gelatinized water) 7.5ο

509812/1043

3- triethanolamine o, 2o

4. Allantoin ο, Ίο

5- Dowicil 2oo o, 1o

6. Methyl paraben o, 1o

7. Propylene glycol 3, ο ο

8. Deionized V / water QS Ιοο, οο

9. Perfume QS 1ο. Dye QS 11. Alcohol SDA & 4o 25, oo

Compounding procedure:

Heat No. 1 to about 63 ° C while stirring continuously, add numbers 4, 6, 7, 8 and 2. Continue stirring and cool the batch to about 40 ° C and add No. 5 »9» 10 and to.

Example 16

Skin protection properties: Condition!

ReinefunFscreme moisturizing, dissolving,

° ^& Drew Makeup Removal Characteristics

th

Ingredient % W / W

1. Beeswax C W ^ O 14, oo

2. LanolinCosmetic Quality) 1o, oo

3. Mineral oil (65/75 Saybolt) 4o, oo

4. Glyceryl monostearate (self-emulsifying) 1.25

5. Polawax ■ o, 50

6. Deionized water QS Ιοο, οο

7. Borax 1.30

8. Methyparaben o, 1o

9. Perfume QS

10. Dye QS

11. Special oatmeal. 1 »5o

Compounding procedure:

Weigh the ingredients No. 1,2,3,4 and 5 into a container and heat to about 72 ° C. with stirring. Weigh the. Components 6, 7 and 8 in a container a and heat with stirring to 72 ⁰ G. At 72 ⁰ O give n. 11 and add to the water phase of the emulsion to the oil phase with stirring.

509812/1043

sz ** Cool to about 4o ^o c7Parfüm and FarbstofriMan fill at 25 - 30 ⁰ G a.

Example 17

Skin protection properties: Smooth, o £ end,

almost neutral pH, desirable non-greasy "handle"

component 1. Polawax % W / W 2. stearyl alcohol 2.25 3. Mineral oil (65/75 Saybolt) 2.5o 4. Getiol V 12, oo 5 · methyl paraben 2, oo 6. Propyl paraben o, 1o 7 · Deionized water QS o, 1o 8. Special oatmeal 1oo, oo 9. Glycerine 2, oo 1o. Carbopol 94-0 5, oo 11. Triethanolamine o, 1o 12. Dowicil 2oo 13. Dye o, 1o 14. Perfume QS QS

Compound practice:

Weigh in ingredients 1 to 6 and begin stirring ^{while warming to about 72 ° G.} In a separate container, add No. 10 to No. 7 with continued mixing, then weigh in and add No. 8 and 9. The water phase is heated to about 72 ° C. with continuous stirring and added to the oil phase, which is also at this temperature. Add No. 11 and continue mixing, then cool the batch to about 40 ° C. at which temperature No. 12, 13 and 14 are added. Fill in at 25-3o ° G.

Example 18

Skin protection properties: Smooth,

■ σ „« ν.4. ·! Η.ν _Λ ; .ι- _η τΛ + -! Λ », o £ end, almost neutral

Feuchtxgkextslotxon ^ _desired ^ _{hter after} " _handle ..

_After " _handle ..

509812/1043

Component # W / W

1. Promulgen D 3 »5o

2. Mineral oil (65/75 Saybolt) 1o, ooo

3. Lanolin (cosmetic grade). 1, ooo

4. Cetiol V 5, ooo

5. PropyIparaben ο, Ίοο

6. Methyl paraben 0.100

7. Deionized water QS Ιοο, οοο

8. Special oatmeal 1, oo

9. Carbopol 961-. o, o? 5

10. Propylene glycol 5,000

11. Dowicil 2oo o, 1oo

12. Perfume QS

13. Dye. QS

Compounding proζedure:

Weigh Nos. 1 through 6 into a container and heat to about 72.0 with stirring. Weigh No. 7 into a separate container and begin stirring while No. 9 is added. Add numbers 8 and 1o. Stirring is continued and the constituents of the aqueous phase are heated to about 72 ° C. Add the water phase, which should be at a temperature of about 72 ° C., to the oil phase, which should have the same temperature. Cool to 4-O ⁰ C and add Nos. 11, 12 and 13. Mar fill in at 25 -3o G.

Example 19

Skin protection · Properties: for dry

Moisturizing lotion skin, non-ionic, o ^ end,

pH of approximately

Component % W / W

1. Petrolatum (White USP) 1o, oo

2. Mineral oil (65/75 Saybolt) 18.00

3. Myrj 52-5 3, oo

4. Lanolin (cosmetic grade) o, 75 5 · methyl paraben o, 1o

6. PropyIp arab en ο, 1ο

7. Carbopol 934-0.30

5. Deionized water QS I00.00

S0Ö-812 / KU3

9. Special oatmeal 1, oo

10. Triethanolamine o, 3o

11. Propylene glycol 3.00

12. Dowicil 2oo o, 1o

13. Perfume. QS

14. Dye QS

Compounding procedure:

Weigh # 1 through # 6 into a container, begin stir and heat to 72 C. Weigh # 8 into one separate container; start stirring, add No. 7 »and 11. Heat the components of the water phase to 72 ° C. and add this to the components of the oil phase. Add No. 10, continue mixing, cool to 40 ° C and add numbers 12, 13 and 14. Fill at 25 - 30 ° C.

example

Skin protection properties: Anionic oil / water

u _a * A - ,, ^ a K _mD -ni _n «nr, -Emulsion, moisturizing, non-greasy. Hand and body lotion pleasant residue properties

Compounding procedure:

Weigh in No. 1-7 and start / to heat> φ.ηΐ er stirring / about 72 C. Weigh No. 8 in another container.

component % W / V / Stearic acid (triple pressed) 3, oo Stearyl alcohol o, 5o Mineral oil (65/75 Saybolt) 5, oo Methy Ip ar ab en o, 1o Propyl paraben o, 1o Isopropyl palmitate 1, o Lanolin (cosmetic grade) 1, o Deionized water QS 1oo, oo Special oat flour 2, oo Propylene glycol . 5, oo Triethanolamine 1, oo Dowicil 2oo o, 1o Perfume QS dye QS

ter and admit No. 9-11, one begins to warm up Stir for 72 hours and add at this temperature one this (aqueous emulsion phase) to the oil phase. Cool to 40 ° G, add No. 12, 13 and 14 ·. Man fill at 25-3o ° G.

Example 21

Skin protection properties: Non-ionic oils /

Moisturizing water emulsion, moisturizing,

ieucntiKicex-Gscreme almost neutral pH

Part of JlS W / W

1. Promulgen _; 4.5

2. Stearyl alcohol 3 «ο

3. Mineral oil (65/75 Saybolt). . 15, ο

4. Getiol V 3.0

5. propyl paraben o, 1

6. methyl paraben o, 1

7. Deionized water QS 100, oo

8. Special oatmeal 2, ο

9. Glycerin. 5 »o

10. Garbopol 961 o, 2 H.'Dowicil 2oo o, 1

12. Dye QS

13. Perfume QS

Compounding procedure:

Weigh Ingredients Nos. 1-5 into a container. Start / to heat - (to about 72 G with continued Ruhrery. Weigh in No. 7 and into another container, start stirring, add No. 1o, 6 and 9 and heat to about 72 G. Add the aqueous emulsion phase the oil phase with continued stirring. Cool to 40 ° and add No. 11, 12 and 13-. Cool up 25 - 3o ° G and fill in.

Example 22

Skin protection properties: Anionic oil / water

-Emulsion, moisturizing, non-greasy, can be used for massage purposes

—Dty- 2445163 component % W / W 1. Stearic acid (triple pressed) 3, oo 2. Stearyl alcohol 2, oo 3. Mineral oil (65/75 Saybolt) 7, oo 4. Pr opy Ip ar ab en o, 1o 5. methyl paraben. o, 1o 6. Deionized water QS 1oo, oo 7. Special oatmeal 2, oo 8. Propylene glycol 5, oo 9. Triethanolamine 1, oo 1o. Dowicil 2oo o, 1oo 11. Perfume QS 12. Dye QS

Compounding procedure

Weigh No. 1, 2, 3 and 4 in a container, begin to stir and heat up? O C. Weigh nos. 5 »6, 7» 8 and 9 into another container. 73 ° C heated
1o, 11 and 12 added.

is heated to 7o -73 ° C. Cool to 4-0 ^° C .; give no.

Example 23

Skin protection properties: Moisturizing, oiling, protective night cream, non-ionic oil / water

-Emulsion

Component % W / V /

1. Arlacel 165 5 »oo

2. Cetyl alcohol 1o, oo

3. Mineral oil (65/75 Saybolt) 25, oo

4. Propyl paraben o, 1o

5. Silicone Fluid 2oo / 35 © öenistokes (19) o.5o

6. Glycerin 5 »oo

7. Methyparaben o, 1o

8. Special oatmeal 1.5o

9. Deionized water QS 100, oo

10. Dowicil 2oo o, 1o

11. Perfume QS

12. Dye. QS

503612/1043

Compounding procedure:

They heat the oil phase (no. 1-5) on 7o -73 ⁰ C under stirring. Warm the aqueous phase (No. 6-9) to 7o-73 C with stirring and add the aqueous phase to the oil phase; cool to about 40 ° C and add No. 10, 11 and 12. Fill in at 25 - «- 3o ^o C.

example 2h

Skin protection properties: Conditioning effects

Bath oil due to the protein content of oats

flour; Supple and oiling, spreading properties, must be shaken before use

component

1. Mineral oil (65/75 Saybolt) QS

2. Is opropylmyri st at

3. Brio 93

4-. Perfume about 2 - 4 #

5. Special oatmeal

6. Dye

% W / W , OO 1oo , OO 2o OO 7, OO 1o, QS

Compounding procedure:

Put numbers ^ and 3 together and mix until homogeneous. Then add these and Nos. A-, 5 and 6 to No. 1. Continue mixing until completely homogeneous. The filling must be done while the batch continues to be stirred.

Example 25 .

Skin protection . ■ Properties: Anionic oil / water

Washable ReiniKunp-screme emulsion, solvent as well as washable germ narrowing cream _disper ^ _ _{ier and} Emul greed ei gen economy s.

Easily washed off with water

Component ' % W / W

1. Stearic acid (triple pressed) 4, oo

2. Lanolin (cosmetic grade) 3, oo

3. Mineral oil (65/75 Saybolt) 1o, oo A-. Methyl paraben o, 1o 5 · propyl paraben o, 1p

6. Getylakohol 1,2o

7. Deionized water QS 100, oo

8. Special oatmeal 2, oo

609812/1043

9. Triethanolamine 1, oo

10. Sipon EG-111 2, supra 11 .. Perfume QS 12. Dye QS

Composition procedure:

Weigh the "ΟΓ" phase of the emulsion (No. 1 - 6) into one One container, begin to heat while stirring, to 7o - 73 G. In another container wito: e nan the water phase (Kr. 7 ~ 1o), start heating while stirring it, to 70 - 73 C. The aqueous phase, which is added should be at this temperature. Cool to 30 ° C and admit No. 11 and 12. Fill at 25 - 30 ° C.

Example 26

Skin protection properties: Nonionic oil /

/ Water emulsion, contains lanolin derivatives, oiling, but not "fetti ?:"

Component % V / / W

1. Amerchol L1o1

2. Promulgen

3. stearyl alcohol

4. Mineral oil (65/75 Saybolt)

5. PropyIparab en

6. methyl paraben

7. Deionized water QS

8. Special oatmeal

9. Glycerine

10. Dowicil 2oo

11. Perfume

12. Dye

Compounding procedure:

Weigh the "oil" phase (No. 1 - 5) into a container, start heating and mixing. Heat to 70-73 ° C. Put the "water ⁿ phase" in another container (Ttr. 6-9), start heating and stirring. Heat this phase to 70-73 ° C. and add it to the oil phase, which is at the same temperature ., one should cool the mixture with stirring to ⁰ 3ο O and Grebe No. 1o, 11 and 12 added Man falls at 25 -.. 3o 0 ° a.

509 & 12/1043 BAD ORIGINAL

5, OO 3, 0 5 » 0 1ο, 0 0, 1 0, 1 1οο, 00 ρ 0 5, O 0, 1 QS OS

skin protection component Bubble bath Natrosol 25OHR Deionized water 1. Special oat flour 2. Methyl paraben 3. Sup er-amides L ° / A 4th Maprofix NH 5. Formaldehyde solution (USP) 6th Uvinuls DS4-9 7th Perfume 8th. . dye 9. 1o

Example 27 .

Properties: high viscosity, good foam, conditioning

% W / Xi

o, 5oo

QS Ιοο, οοο

2, ooo o, 1oo 3, ooo 35 »ooo o, o75 o, o75 QS
QS

Compounding procedure:

Heat No. 2 to 70-73 ° C., start stirring and add No. 1 to. Mix for about 15 minutes and add numbers 3, 4, 5 and 6. Mix about 15 minutes after # 6 is added. Cool to 4o - 43 ° C and add No. 7, 8, 9 and 1o. Man fill, at 25 - 30 ° C.

Example 28

Skin protection properties: Good solvents

_R · -, _ti telwirkung, including emulsifying and

Kexnxgunasiotxon Dxspergierexger.schaften for Ent

removal of makeup or pollution like dust and dirt.

Component % W / W

1. Promulgen 2.5o 2.5o

2. Mineral oil (65/75 Saybolt) 2o, oo

3. Lanolin (cosmetic grade) 1, oo 4 ·. Isopropyl myristate 5 »oo

5. Emcol E6o75 o.25 -

6. Oarbitol solvent o.75

7. Deionized water QS Ιοο, οο

8. Special oatmeal - 2, oo

9. Glycerin 5 »oo

10. Methyl paraben ^ Λόοΐ ^ / ΊΛ / ο. ° » ¹ °

BATH ORIGINAL

-3ο- 2 ^ 45163

11. Propyl paraben o, 1o

12. Dowicil 2oo. o, 1o

13. Perfume 'QS

Compounding pro ζ edur:

Weigh No. 1, 2, J, 4-, 5 and 11 into a container and start heating and stirring. Heat to 7o - 73 ° C. Put Mr. 7, 8, 9 and 10 in another container, begin to heat and stir. Heat to 70-73 ° C and add the "V / as s er" phase of the emulsion to the "oil" phase which should be the same temperature (both should be at 70-73 ° C). After combining the phases, the batch should be ^{cooled to 35-4ο ο} 0, at which temperature No. 12 and 13 are added. Fill at 25 - 30 ° C.

Example 29

Skin protection properties: Moisturizing, moisturizing

Cuticle cream dig, has neutral pH

Component # W / W

1. Polawax 7.5o

2. Stearyl alcohol 6, oo

3. Lantrol 2, oo

4. Mineral oil (65/75 Saybolt) 15, oo

5. Cetiol Y 4, oo

6. Isopropyl palmitate 2, oo

7. Propyl paraben o, 1o

8. Deionized water QS 100, oo

9. Methyl paraben o, 1o

10. Glycerin 5 »oo

11. Special oatmeal o, 1o

12. Dowicil 2oo o, 1o

Compounding prο cedure:

Weigh in the "Oil ^If phase Mr- 1 to 7, start to heat and stir. Heat to 70-73 ° · Weigh in the" Water "phase No. 8-11 and start to heat and stir. Heat to 70-73 G and add the water phase to the oil phase. Both should be -7o -73 ° C. Cool to 40 ° C. and add No.. Fill in at 25-3o °.

509812/1043

Example 3o

Skin protection properties: conditioning,

Freshener with powder-like cooling, leaves powder-like residue properties residue after solvent ^

damping

"Component % ¥ / W

1. Carbopol 94o o, 2o

2. Deionized water 5o, oo

3. Ethyl alcohol SDA / ^ 4-0 .... 15, oo

4. Special oatmeal. 3? Oo

5. Triethanolamine o, 2o

6. Methyl paraben o, 1o

7. Allantoin o, 1o

8. Perfume QS

9. Dye QS

10. Dowicil 2oo. o, 1o

Eorapounding procedure:

Instruct Kr. 2, start stirring, slowly add No. 1. When the Carbopol is completely hydrated, how to proceed further ¹ Ir. Enter 3 and add numbers 6 and 7. Stir until these materials have dissolved and add to the Garbopol water dispersion. Add the remainder of the mass with continued stirring. After the batch has aged for 12-15 hours, stir and pour in.

Example 31

Skin protection properties: conditioning, oiling,

Bath oil. Keeping moisture, ^ are packed in tubes

ice «*«

Component % \ J / V /

1. Special oatmeal 5, ο

2. Cabosil M-5 4-, ο

3. Tween 8o, 8, ο M-. My vac et Type 9-4-0 2o, o

5. Mineral oil (65/75 Saybolt) QS 1oo, oo

6. Isopropyl myristate 5, ο

7. Perfume QS

8. Dye QS

50981 2710 A3

Completion pro ζ edur:

Weigh in all of the ingredients except # 2. Man start stirring. ITr. 2 is added and stirred, whereby one uses a stirrer that provides high shear stress (i.e. propeller type).

Example 32

Skin protection properties: Cooling, supports

Astringent conditioning and moisturizing

Component % W / Vi

1. Deionized water 6o, oo

2. Laponite XLG 2, oo .3. Special oatmeal 3 »oo

4. Chlorhydrol (5o %) 3, oo

5. Ethyl alcohol (SDA / Ao) 16.5o

6. Methyl paraben o, 1o

7. Deionized water QS 100, oo

8. Perfume QS

Compounding pro ζ edur:

Weigh in No. 1 and give Mr. 2 to, with a

ho / iie shear stress is applied. After No. 2 completely

djga) has been pergated and hydrated, ^ ebe one No. 3, M-, 5, 6.7 and 8 too.

Example 33

Skin protection properties: Leaves behind smooth

_Talk residue & C feeling, supports condi

tion and moisture content skin

Component # W / W

1. Talk QS 1oo, oo

2. Magnesium stearate 2.5

3. zinc oxide 2, ο

4. Special oatmeal 3 »o

5. Perfume QS

Compounding proζedure:

Admit No. 2 - 5. No. 1 and mix homogeneously until complete gruesome.

5 O 9 8 1 2 / 1-0 k 3 BAD ORiGlNAL

3ο , OO 6th , 00 ο, 1ο ο, ο2 ο, 2ο 5ο, OO 1οο, OO ο, ο75 QS QS

-οο- Example 34-

Hair protection properties: Conditioning

and manageability imparting liquid shampoo (translucent in appearance)

Component % W / W

Λ . Siponesy
2. ffinol 2o12 Extra
3 · M ethy Ip ar ab en
K. Versene Regular

5. Citric acid (anhydrous)

6.Special oatmeal dispersion (1 % in deionized water)

7. Deionized V / water QS

8. Formalin USP

9. Perfume

10. Dye

Compounding procedure:

Heat No. 1 to 7 to about 60 O with continued stirring. Cool to ¹ Vo C and add No. 8, 9 and 1o.

Example 35

Hair protection properties: conditioning

rend, manageability

Liquid shampoo (pearlescent in appearance)

Part of JiW / W

1. Standapol V / A Special 35 »oo

2. Ninol 128 Extra 5, oo 3-ethylene glycol monostearate 2.5o

4. Methyl paraben ο, Ίο

5. Citric acid - o, 1o

6. Special oatmeal dispersion

(4 # in deionized water) 5o, oo

7. Perfume QS

8. Formalin USP 'o, o75

9. Dye QS

10. Deionized water 100,000

509812/1043

.34-2U5163

Compounding pro ζ edur:

Heat Nos. 1 through 6 to approximately with continued stirring 8o ° C; cool to about 40 ° G and add No. 7, 8, 1o and 9.

Example 36

Hair protection properties: conditioning,

Gels / hampoo (giving permeability in appearance shining)

Component ■ % W / W

1. Maprofix TLS 3o, oo

2. Ninol 128 Extra 8, oo

3. Natrosol 25oHR 1, oo

! f. Special oat flour (2 fo dispersion

in deionized water; 5o, oo

5th verses regular o, o5

6. Methyl paraben - o, 1o

7. Perfume QS

8. Dye QS

9. Deionized water

10. Formalin solution USP o, o75

Compounding procedure:

Heat No. 4 to about 70 ° G with stirring and add No. with stirring. Cool to about 4o ° C and add numbers 1, 2, 5, 6, 7 »8, 9, and 1o.

Example 37

Hair protection properties: Excellent

Foam properties. He manageability

ggete

Cim Aiiqqphpn npflmuftpr- foam properties. Condition- ^{To exude} mother-of-pearl. Granted shine and

Component % W / W

1. Stepanol WA Special 25, ο

2. Steol 4N 25, ο

3. Ninol 128 Extra 6, ο

4. methyl paraben o, 1

5. propyl paraben o, 1

6. Ethylene glycol monostearate 2, ο

5098T2 / 1043

7. Deionized water QS Ιοο, οο

8. Special oatmeal 1, oo

9. Citric acid QS up to pH 7, o

10. Formaldehyde solution USP o, o75

11. Perfume QS

12. Dyes QS

Compounding procedure:

Weigh Mr. 1 to 8 in a container and heat while is carefully stirred to avoid the ingress of air, heat to 7o - 73 ° C, mix for 15 minutes at 7o -73 ° C ^ and cool to 35 - 4-0 G, at which temperature Rr. 9, 1o, 11 and 12 should be added.

Example 38

Hair protection properties: Conditioning and

Cremshanrooo giving manageability, supple

4N ^y paste with excellent water dis

persion properties and foam

Component % W / ¥

1. Stearic acid (triple pressed) 1, ooo

2. Sodium Hydroxide USP 1, ooo

3. Cetyl alcohol (NF Grade) 2,000 M-. Lanamine ■ 5,000

5. Special oatmeal 1, ooo

6. Deionized water QS. Ιοο, οοο 7 · methyl paraben 0.100

8. Standapol VJAQ Special 60,000

9. Perfume · QS

10. Dye 'QS

11. Formalin solution USP O, o75

Compounding procedure:

Dissolve no. 2 in no. 6 under homogeneous mixing and Heat ^ τ ^ β ^ ί 1, 3 and 4 to approximately 62 ⁰ C. This will give the sodium hydroxide solution to the mixture of Nr. 1.3 and 4. Continue stirring and weigh # 5-8 while stirring and add to the heated emulsion. Continue mixing (avoiding air inclusions) while the batch cools to 28 ° C, equal to

509812/10 ^ 3

No. 9 »Io and 11 are admitted early.

Example 59

Hair protection properties: Makes hair

η ■ ·, ... η ·. tt "x." ^ "" -Ui soft, shiny and manageable, cream powder with oatmeal _{during the} conditioning properties

can be granted

Component % W / W

1. Polawax 1, o

2. Arquad 2HT75 2, ο

3. Cetyl alcohol (N.P.) 2, ο 4-. Ceralan o, 5 5- propylparaben o, o5

6. Deionized water QS 100, oo

7. Propylene Glycol 2, ο

8. Special oatmeal 2, ο

9. methyl paraben o, 1

10. Perfume QS

11. Dye QS

Compounding pro ζ edur:

Heat No. 1 to 5 to about 72 ° C while continuing to watch. In another container, heat No. 6 to 9 to about 72 ° C. Give the aqueous phase (6-9), which is at 72.degree should be, to the oil phase 1-5 · Cool the batch to 30 ° C. with continued stirring and add No. 10 and 11. Fill in at 25-3o ° G.

Example 4o

Hair protection properties: Makes soft and comfortable

Hair conditioning lotion conditioned, works in 1 to 2 minutes.

Component - # W / ¥

1. Polawax 3 * oo

2. Stearyl alcohol 1, oo

3. Emcol E6o7S 1, oo

4. Lanolin (cosmetic grade) o, 25

5. Mineral oil (65/75 Saybolt) 2, oo

509812/1043

6. Deionized water QS ioo _t oo

?. Special oatmeal 2, oo

8. Propylene Glycol 2, οο

9. Methyl paraben _{o t 1o}

10. Perfume QS

11. Dye QS

Compounding procedure:

The "oil phase" (Mr. 1 - 5) is heated to about? 2 0 tinter continued stirring. Warm the aqueous phase (Iir- 6 - 9) to 7o - 3 ° ö with continued stirring. Add the aqueous phase to the oil phase, both should be? O-73 G, while stirring continuously. Man. cool to $ o ΰ and add No. 1o and 11 added. Fill in at 25-3o ° G.

Example 41

Hair protection properties: non-ionic / cationic

Hair conditioning cream see emulsion, rapid conditioning, softening endj gives high gloss

Part of ^v _ # W / W

1. Promulgen ^ ^ Ε-, οο

2. Mineral oil (65/75 Saybolt) 5, oo

3. Oetiol ¥ 3 _t oo%. Clrape seed oil 4 _t , oo

5. Stearyl alcohol% _s oq>

6. Propyl paraben "o _e io

7. AamciuSTi - £ & ■ (22)

8. Propylene glycol

9. Deionized water

12. Special oatmeal

Weigh ITr. Put 1 _t 2, 3 «^ * 5 ^ ü <ä 6 in a container, begin to stir and heat ζ, η. It is heated at between 70 and 75 ° C. Weigh Hr. 7 »8, 9, 1q„ 11 and 12 in another container, start stirring and heating. Mari warm up to? Ο-75 ° 0 and srebe aas (: Tr.1-6) -Qemiseh _t which should be at 7o ~ 73 ° ö, added. Cool anif 25—3®''G and pour in.

503 & 12/1042

BATH ORIGINAL

example K2

Hair protection properties: conditioning et »granted

Festierersvstem gloss, manageability and advise hold

üös ^ gepsysTieni under moist conditions. Used

Oatmeal is a softening and conditioning agent

Component % W / V /

1. Gantrez 225 3.5

2. Ethyl alcohol SDA / Ao QS 1oo, oo

3 «Special oat flour ($ 1 dispersion

in deionized water & 1o _t o

4 «diisopropanolamine o, 2

5. Perfume QS

Composition procedure:

Weigh in Kr. 2 and start stirring. One pebe Hr. 1 and mix _t until the dispersion is clear and homogeneous. Add to # 5, 4- and 5, mix until dispersion is uniform.

example

Hair protection properties: fixing properties,

Component _ # W / W

1. Kesyn 28-293 © 2, oo

2. Ammonium hydroxide (28% solution) o _t 12o 3 «ethoxylan 5o o, 25

4. Perfume

5. Ethyl alcohol

6. Special oatmeal (1 ^ ige dispersion

in deionized water) 51 * 78

7 «Fanthenol o _t 5

8. Eormaldehyde solution BSP o, o? 5

9. Dye QS

Campaigning procedure:

Weigh Mr. 5 a U ¹¹ ^ i give TIr with continued stirring. 1, 2,3,4-, 6, 7, 3 and 9 are added. Mix until a completely uniform dispersion results. Filter through 100 mesh or larger. _{50S812 / 1043}

24A5163

example

HautsGhutz
Baby powder

component

1. Talk QS

2. Magnesium steara't-5. Syloid M72.

4. Ottasept Extra

5. Special oatmeal.

6. Perfume

Properties: content of oatmeal gives good adhesion to epidermis, Viass er adsorptions properties and the dermatological properties of the oatmeal. The powder leaves the skin dry, soft and supple, hot to the touch

# W / W

Ίοο, οο 2, oo 1, oo ο, Ίο 1o, oo QS

Compounding procedure:

Add Ingredients Nos. 2 through 6 to the talc, mix until to uniformity.

example

skin protection
Foot powder

component

1. Talk QS

2. Special oatmeal

3. Microdry
M-. 'Zinc oxide

5. Syloid 72

6. Perfume

Properties: epidermal supple natural protein with the dermatological ones Benefits of oatmeal. The powder contains an evaporation-preventing material that also has a Deodorant is.

Ιοο, οο

1o, oo

5, oo 2, oo 2, oo QS

Compounding procedure:

Man e: ebe?! R. 2 to 6 to number 1 and mix homogeneously until uniform .

509812/1043

-4ο-

example

skin protection Properties: Oatmeal provides a source of natural pro-

Kqp / r ^ ertalk with anti-exudation and emollient
properties lipids. Oatmeal has run out

been used to treat a range of dermatological conditions both specific and non-specific Nature, such as itching, dryness and wrinkles, to heal. Powder contains ingredients that help suppress exhalation and have a deodorant effect deliver

component

1. Talk QS

2. Microdry

3. Syloid # 72

4. Special oatmeal 5 · Perfume

VJ / W

Ίοο, οο

3, oo

2, oo

1o, oo

QS

Compounding procedure:

Add No. 2 to 5 to No. 1 and mix until completely

iormig.

Example 47

Skin protection baby powder

component 1. Talk 2. Zinc stearate 3. Syloid # 72 4th Special oat flour 5. zinc oxide 6th Dioxin 7th Perfume

Properties: oat flour provides potential dermatological properties, natural protein, emollient lipids, leave the skin soft and velvety smooth to the touch

% V / / W

9ο , 15 2 »5ο 2 , 00 3 , 00 2 , 00 0 .1ο

509812/1043

Stock ex Talk 1. Special oat flour hicrodry ο ·. Syloid 72 4th Ottasept Extra 5- zinc oxide 6th Perfume 7th

Grain dosing procedure:

Manu rrebe the ingredients No. 2 to 7 to the talc, mix homoren until completely? "pieichiform.

Example 4-8

Skin protection properties: Oatmeal provides conditioning

Ji ¹ H '' ³ neev due to natural protein, good adhesion

^i- "On skin, agent also serves as a deodorant and

contains an agent to reduce exhalation

82.65 3, oo

1o, oo 2, oo

o, 15
2, oo

QS

Compounding pro ζ edur:

I give a plan. 2 to 7 to number 1 and mix homogeneously to uniform.

Example 4-9

Skin protection properties: Oatmeal offers natural

BpodoT ^ t - Kö> nf-rmidf-r ^ otein and emollient lipids, deodorant body powder ^ ₆ Adhesion to the surface

the epidermal layer. Leaves the skin soft and supple to the touch.

Component # W / W

1. Talk 8o, 75

2. Zinc stearate 6, oo

3. Syloid 72 '2, oo 4-, Special Oatmeal 3, oo

5. Titanium dioxide 2, oo

6. Ottasept Extra ο »25

7. Perfume QS

8. Magnesium carbonate '3, oo

509812/1043

BATH ORIGINAL

Comp \ u $ ndi eration pro ζ edur:

Give ITr. 2 to 8 to Iir. 1 and mix the ingredients homogeneously, ice cream are evenly dispersed.

Example 5o

Skin protection properties: Oatmeal supplies

Body talk with deodorant and whole protein and lipids r, ur skin

Anti-exhalation properties conditioning and emollient

^c making. Evaporation inhibitory and

Deodorant effect through aluminum sal:

Component f < ^T :. ^r / ^τ λ

1. Talk δ3.5ο

2. Special oatmeal 3 »5o

3. Microdry 7.5o

4. Syloid 72 3, oo

5. Ottosept Extra o, 15

6. Alumnium stearate 2, oo

7. Perfume

Compounding pro ζ edur:

Give the ingredients? Tr. 2 to 7 to the talc, mix homogeneously ,, until the approach is completely uniform.

Example 51

Soap properties: Soap contains special oats

flour, gives moisturizing and supple Properties and provides protein and lipids

Part of parts by weight

1. Olive oil (purified) 2oo, oo

2. Stearic acid (triple pressed) 100,000

3. Corn oil 100, oo 4-, oleic acid 100, oo

5. Butylated hydroxyanisole 0.15

6. Sodium Hydroxide USP 100, oo

7. Deionized water Ίοο, οο

8. Deionized water 65o, oo

9. Special oatmeal 15o, oo

10. Perfume QS

11. Dye 'QS

509512/1043

BATH ORIGINAL

^{Ko- 7} Ip oundi erun r.spr ο ζ edur:

Heat No. 8 to 75 ° C + 3 ° C and sprinkle No. 9 while mixing with a high-performance propeller-type shear stirrer. Hai warm up Mr. 1 to 5 to 92 ⁰ C + 2 ⁰ G with slow stirring in order to avoid air deficiency. Dissolve No. 6 and 7. While maintaining the "oil mixture" at 92 ⁰ + 2 ⁰ C, slowly add aliquots of the special oat flour dispersion and sodium hydroxide solution, alternating between the oat flour and sodium hydroxide. Maintain the temperature for 1 hour after the addition of the oatmeal and sodium hydroxide have ended while the batch is slowly stirred. Cool to 68 ° C + 2 ° C and add No. 10 and 11. Continue cooling to about 25 ° C. This product can be machined to remove excess moisture by applying a "vacuum" during the process. This product can also be warmed to about 450 for 24 hours prior to pressing to facilitate moisture removal.

Table I.

Explanation of the trade names, identification by their chemical names.

Explanation of the listed material components

Trade name or species name Identification

1. Allantoin 5-ureidohydantoin

2. Amerchol L1o1 extract from lanolin sterols and

complex higher alcohols in free form

3. Anerlate P isopropyl ester of normal ver

branch-chain and hydroxy acids of lanolin.

4. Ammonyx 4 stearyldimethylbenzylammonium

chloride.

5. Arlacel 165 glycerin monosteVat »and polyoxy-

Ethylenst earat

6. Arquad 2HT75 Dialkyl (taln;) - quaterrial Amnon-

niu! Ti salts

7. Beeswax with red part of myricyl palmitate,

Cerotic acid and esters as well as slightly higher carbon paraffins

3. "Rorax" atrium borate ^.

9. ^ ri.i 9? PolyoxyethyienolsVlether

10. Cab-O-Sil. K-5 egg. fumed silica

509812/1043

BATH ORIGINAL

11.12.

15. 16. 17. 18.

19. 2ο.

21. 22.

23/24

25-26. 27

28. 29. 3ο.

31- 32,

33, 34, 35, 36, 37, 38. 39. 4ο.

41.

Carbitol Solvent Garbopol C er al an Geresin Wax Getiol V Chlorhydrol Diethy 1 en glyko lmon ο äthy 1 äth er Carb oxyvinyIp οlymer

Lanolin alcohols

purified ozocerite, mineral wax decyl oleate

Aluminum chlorohydroxide

Chromalite Dark Blue iron oxide pigment

Ghromalite Magenta self-oxide pigment

DSbG Red ^ 7 calcium salt of 4- (0-sulfo-p-tolylazo) -

-3-hydroxy-2-naphthylic acid e

D&G Bed ^ 19 3-ethochloride des 9-0-carboxyphenyl-

6-diethylamino-3-ethylamino-3-isoxanthene ^r is

D&G Red / M21 2,4,5,7-tetrabromo-3,6, fluoranediolÄ

Dowacil 2oo cis isomer of 1- (3-chloroallyl) -3,5,7-

Emcol E6o7S Emerwax 4266-D

Fluid E37o fuller's earth Gantrez -triaza-i-azoniaadamantane chloride

Stearoyl-N-colaminoformyl-methylpyridinium chloride A.

Mixture of higher fatty acid and alcohol esters and alcohols (cetyl palmitate, cetyl alcohol, Lauric, stearic and myristic acid esters)

Polyalkylene glyko1
colloidal aluminum silicate

Monoethyl ester of the polymethyl vinyl ether / maleic acid product

Gelvatol 3 / 9o Lan amine Lanolin Polyvinyl alcohol / acetate

Lanolin amine

mainly cholesterol esters of higher fatty acids

dewaxed lanolin

synthetic inorganic silicate with structural properties similar to hectorite,

Bentonite or montmorillonite similar. Lo Micron Pink 2511 iron oxide pigment Lo Micron Yellow 2576 Iron Oxide Pipe Lo Micron Brown 2593 iron oxide pigment

Lantrol Laponite XLG

Maprofix NH

Maprofix TLS

Methyl paraben

Myrj 52.5

Myvacet type 9-4o

Natrosol 25oHR ammonium laurel sulfate

TriäthanGLiBlaminlaurylsulfat Methyl p-hydroxybenzoate

Polyoxyethylene stearate

distill. acetylated monoglycerides hydroxyethyl cellulose

509812 / 10A3

42. Ninol 128 Extra

43. ; inol 2o12 Extra 44. Pearl Glow 45. Polawax 46. Prormil ^ en 47. Pr opy Ip ar ab en 48. Red ^ 2513 49. Resyn 226o 5ο. Resyn 28-293o 51. Silicone Fluid 2β6 / 35ο

Centistokes 5 ?. Sipon EG-111 5: ·. Sipon ESY

54. Sorbitol

55. Standamid SD

56. Standanol SHI00

57. Stand Oil ^ A Special 58. Standapol ViAQ Special 59. Steol 4H 60 St ep anol ^T *. ^r A Special 61. Suoer Araide L9A 62. Talk 63. Tween 7 ^ 80 64. Ultra Blue 55 ⁸ 5 65. Uvinul DS / A9

66. Yeegum

67 · Vers en e Rec ^ ular

68. Viscolan

69. Yellow 2575

Coconut fatty acid diethanolamine condensate at

Coconut fatty acid diethanolamine condensate bismuth oxychloride
Polyoxyäthylenlanolin- ^l "/ ^r acb.s Polyoxyethylene glycol complex of higher molecular weight natural fresaturated fatty acids

Pr opy1-ρ-hydroxyb en ζο at

Iron oxide pigment

Acrylic copolymer latex

Garboxylated vinyl acetate terpolymer

Dimethylsiloxane polymer

iiatrium cetyl / stearyc sulfate Sodium lauryl ether sulfate, hexavalent alcohol

Coconut Fatty Acid Diethanolamide

anionic dibasic acid monoester -l sodium salt ζ

⁷ I atrium auryl sulfate

liatrium aury! sulfate

Sodium lauryl ether sulfate II atrium lauryl sulfate

Lauric acid

hydrous magnesium silicate polyoxyethylene sorbitan monooleate Iron oxide PiCTi ent

Sulfonated sodium salt! 2-hydroxy -4-methoxyber! zophenon

colloidal magnesium aluminum silicate Ethylenediaminetetraacetic acid (tetrasodium salt)

Dewaxed liquid lanolin iron oxide pi potent

Modifications and equivalents falling within the scope of the invention fall are to be regarded as part of the same.

Pat en t speak

509812/1043

Claims (1)

Claims Ί. Cosmetic preparation, which oatmeal one contains such particles as to be at least about 98 ^ of the same pass through a 2oo mesh (U.S. Sieve Series) screen. 2. Cosmetic preparation according to claim 1, which also Contains water and alcohol. J. Cosmetic preparation according to claim 1, which also contains an oil-in-water emulsion. 4-. Cosmetic preparation according to claim 1, which also contains a water-in-f'1 emulsion. 5. Cosmetic preparation according to claim 1, which in a mixture with talc powder contains a small amount of oatmeal with a particle size such that at least 93 / 'of the same pass through a 200 mesh screen (U.S. Series). 6. Process for the manufacture of cosmetic preparations., characterized in that a small amount of oat flour is added to the batches with a particle size such that at least 98 "·> pass it through a 2oo mesh sieve (U.S. Series), incorporated or incorporated. Dipl.-Ing. P. E. Meissner patent attorney 509812/1043