DE1907195A1 - Magnetically locked, removable high-speed mixing separator for radioactive liquids - Google Patents

Magnetically locked, removable high-speed mixing separator for radioactive liquids

Info

Publication number
DE1907195A1
DE1907195A1 DE19691907195 DE1907195A DE1907195A1 DE 1907195 A1 DE1907195 A1 DE 1907195A1 DE 19691907195 DE19691907195 DE 19691907195 DE 1907195 A DE1907195 A DE 1907195A DE 1907195 A1 DE1907195 A1 DE 1907195A1
Authority
DE
Germany
Prior art keywords
mixing
separator
speed mixing
speed
mixing separator
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DE19691907195
Other languages
German (de)
Inventor
Heinrich Guetter
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Deutsche Gesellschaft fuer Wiederaufarbeitung von Kernbrennstoffen mbH
Original Assignee
Deutsche Gesellschaft fuer Wiederaufarbeitung von Kernbrennstoffen mbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Deutsche Gesellschaft fuer Wiederaufarbeitung von Kernbrennstoffen mbH filed Critical Deutsche Gesellschaft fuer Wiederaufarbeitung von Kernbrennstoffen mbH
Priority to DE19691907195 priority Critical patent/DE1907195A1/en
Priority to US8320A priority patent/US3674196A/en
Publication of DE1907195A1 publication Critical patent/DE1907195A1/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21FPROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT; TREATING RADIOACTIVELY CONTAMINATED MATERIAL; DECONTAMINATION ARRANGEMENTS THEREFOR
    • G21F9/00Treating radioactively contaminated material; Decontamination arrangements therefor
    • G21F9/04Treating liquids
    • G21F9/06Processing
    • G21F9/12Processing by absorption; by adsorption; by ion-exchange
    • G21F9/125Processing by absorption; by adsorption; by ion-exchange by solvent extraction
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/04Solvent extraction of solutions which are liquid
    • B01D11/0446Juxtaposition of mixers-settlers
    • B01D11/0457Juxtaposition of mixers-settlers comprising rotating mechanisms, e.g. mixers, mixing pumps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/40Mounting or supporting mixing devices or receptacles; Clamping or holding arrangements therefor
    • B01F35/42Clamping or holding arrangements for mounting receptacles on mixing devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/57Mixing radioactive materials, e.g. nuclear materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • General Engineering & Computer Science (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Centrifugal Separators (AREA)

Description

GESELLSCHAFT ZUR WIEDERAuTARBEITUIiG VON KERNBRENNSTOFFEN MBHSOCIETY FOR REWORKING OF NUCLEAR FUELS MBH

Magnetarretierte, ausbaubare Senneilmischtrenner für radioaktive FlüssigkeitenMagnetically locked, removable rope mixing separator for radioactive liquids

. Die Extraktion gelöster Stoffe aus einer Flüssigkeit mittels einer anderen Flüssigkeit erfolgt durch inniges Ver— . mischen und anschliessendes Trennen der beiden Flüssigkeiten. Zur Erzielung einer möglichst vollständigen Extraktion werden mehrere Misch- und Trennstufen hintereinander geschaltet, welche kontinuierlich im Gegenstrom arbeiten.. The extraction of solutes from a liquid by means of another liquid takes place by intimate mixing. mix and then separate the two liquids. To achieve the most complete extraction possible, several mixing and separation stages are used one after the other switched, which work continuously in countercurrent.

Sollen spaltstoff— und produkthältige, radioaktive Lösungen extrahiert werden, so müssen kurze Kontaktzeiten der beiden Flüssigkeiten erreicht werden, da sonst die verwendeten Lösungsmittel der Zersetzung durch die radioaktive Strahlung ausgesetzt sind.Should radioactive solutions containing fissile material and products are extracted, the two must have short contact times Liquids can be reached, otherwise the used solvents of the decomposition by the radioactive ones Exposed to radiation.

Die erforderlichen kurzen Kontaktzeiten werden mit dem von der Gesellschaft für Kernforschung mbH, 7500 Karlsruhe, entwickelten und zum Patent angemeldeten "Kompakten Schnell-Mischtrenner für Wiederaufarbeitungsanlagen von Kernbrennstoffen und dergleichen" (Anmeldung P 15 57068.0) erreicht.The required short contact times are provided by the Society for Nuclear Research mbH, 7500 Karlsruhe, developed and patent-pending "compact high-speed mixing separator for reprocessing plants of nuclear fuels and the like "(application P 15 57068.0).

2» Die derzeit bekannte Konstruktion für Schnellmischtrenner weist für den Einsatz in Anlagen zur Extraktion radioaktiver Lösungen eine Reihe von Nachteilen auf, die mit der erfindungsgemässen Konstruktion vermieden werden:2 »The currently known construction for high-speed mixing separators has a number of disadvantages for use in plants for the extraction of radioactive solutions, which with the construction according to the invention can be avoided:

- Der von oben in das Gehäuse eingesetzte Rotor kann unter der hohen Strahlungsbelastung nicht ausgebaut werden.- The rotor inserted into the housing from above can be underneath the high radiation exposure are not expanded.

- Der Austausch des Pumpenrades oder der Mischkammer ist nur nach vorheriger Entleerung und Reinigung der Verfahrenseinheit möglich.- The exchange of the pump wheel or the mixing chamber is only possible after the processing unit has been emptied and cleaned possible.

-2-00 9 8 36/1669 . --2-00 9 8 36/1669. -

Jeglicher Wartungseingriff hat daher Stillstandszeiten und Dekontaminationsarbeiten nicht nur an dem Schnellmischtrenner selbst, sondern auch an allen räumlich-mit— ihm verbundenen Anlageteilen zur Folge. ... . . . ....-,-"Any maintenance work therefore has downtimes and decontamination work not only on the high-speed mixing valve itself, but also on all of the system parts connected to it. ... . . ....-, - "

Bei der erfindungsgemässen Konstruktion sind demgegenüber die bewegten Teile der Schnellmisehtreimer, ä.*h.·. · das Pumpenrad mit der daran anschliessenden Mischkammer sowie der Rotor so ausgebildet, dass sie ohne Stillegung 'des Verfahrens und ohne vorherige Dekontamination des Raumes, in dem sie sich befinden, ein- und ausgebaut werden können. ' \ In the construction according to the invention, on the other hand, the moving parts of the high- speed waste bin, etc., are. · The impeller with the adjoining mixing chamber as well as the rotor are designed in such a way that they can be installed and removed without having to shut down the process and without prior decontamination of the room in which they are located. '\

Abbildung 1 zeigt den Gesamtaufbau des erfindungsgemässen Schnellmischtrenners. ™ -Figure 1 shows the overall structure of the inventive Quick mix separator. ™ -

Abbildung 2 dessen unteren Teil im Maßstab 1:1.Figure 2 its lower part on a scale of 1: 1.

Das von der Rotorwelle (1) angetriebene Pumpenrad (2) sitzt in einer gekapselten Mischkammer (3)? die gegen Verdrehung mittels zylindrischen Passstifte gesichert istο Die Arretierung der gekapselten Mischkammer erfolgt durch paarige Permanentmagnete (5)· ~The pump wheel (2) driven by the rotor shaft (1) sits in an encapsulated mixing chamber (3)? secured against rotation by means of cylindrical dowel pins istο The encapsulated mixing chamber is locked by paired permanent magnets (5) · ~

Zum Ausbau des Schnellmischtrenners wird-zunächst der Motor (7), welcher sich ausserhalb der durch.die Abschirmwand (8) abgetrennten radioaktiven Zone befindet, abgenommen. /To remove the high-speed mixing separator, the Motor (7), which is located outside the radioactive zone separated by the shielding wall (8), removed. /

Mittels einer auf die Rotorwelle aufgesetzten Ziehhiilse werden sodann der Rotor und die Mischkammer mit dem darin befindlichen Pumpenrad aus der Strahlenabschirmung und dem Schnellmischtrennergehäuse (9) gezogen. Die entstandene öffnung in der Abschirmung wird mit einem Stopfen verschlossen. Nach Erfolg der Wartung und der Instandsetzung erfolgt der Wiedereinbau in umgekehrter Reihenfolge. Zwischenzeitlich läuft das Extraktionsverfahren ungestört weiter. By means of a pull sleeve placed on the rotor shaft, the rotor and the mixing chamber with the inside The pump wheel located in the area is pulled out of the radiation shield and the high-speed mixer disconnector housing (9). The resulting opening in the shield is closed with a stopper locked. After the maintenance and repair work has been carried out successfully, reassembly is carried out in reverse Series. In the meantime, the extraction process continues undisturbed.

009 836/1 66 9009 836/1 66 9

Claims (1)

4. Patentansprüche4. Claims 1. Schnellmischtrenner, dadurch gekennzeichnet, dass die Misch- und/oder die Trennkammer. ausgebaut werden können.1. High-speed mixing separator, characterized in that the Mixing and / or the separation chamber. can be expanded. 2. Schnellmischtrenner, dadurch gekennzeichnet, dass die Misch- und/oder die Trennkammer ohne Leerung und Reinigung der Verfahrenseinheit ausgebaut werden können.2. high-speed mixing separator, characterized in that the Mixing and / or separating chamber without emptying and cleaning the processing unit can be expanded. 3- Schnellmischtrenner, dadurch gekennzeichnet, dass die Misch- und/oder die Trennkammer ohne Lösen mechanischer Verbindungen ausgebaut werden können.3- High-speed mixing separator, characterized in that the mixing and / or the separating chamber without loosening mechanical Connections can be expanded. 4. Schnellmischtrenner, dadurch gekennzeichnet, dass die Misch- und/oder die Trennkammer ohne Leerung und Reinigung .der Verfahrenseinheit und ohne. Lösen mechanischer Verbindungen ausgebaut werden können,.4. high-speed mixing separator, characterized in that the Mixing and / or separating chamber without emptying and cleaning .the processing unit and without. Loosening mechanical Connections can be expanded. 5. Schnellmischtrenner, dadurch gekennzeichnet, dass die Misch- und/oder die Trennkammer nach Lösen einer Magnetverbindung ausgebaut werden können. ·5. high-speed mixing separator, characterized in that the Mixing and / or separating chamber can be removed after loosening a magnetic connection. · 6. Schnellmischtrenner, dadurch ,gekennzeichnet, dass die Misch- und/oder die Trennkammer nach Losen einer Magnetverbindung und ohne Leerung und Reinigung der Verfahrenseinheit ausgebaut werden können. 6. high-speed mixing separator, characterized in that the Mixing and / or separating chamber can be removed after a magnetic connection has been loosened and without emptying and cleaning the processing unit. 7- Schnellmischtrenner, dadurch gekennzeichnet, dass die Trennwand zwischen der Misch- und der Trennkammer magnetisch arretiert ist. · 7- high-speed mixing separator, characterized in that the Partition between the mixing and the separation chamber is magnetically locked. · 8. Schnellmischtrenner, dadurch gekennzeichnet, dass zum Ausbau der beweglichen Teile der radioaktiv verseuchte Teil der Anlage nicht betreten zu werden braucht.8. High-speed mixing separator, characterized in that the radioactively contaminated to expand the moving parts Part of the facility does not need to be entered. 0 0 9 8 3 6/16690 0 9 8 3 6/1669
DE19691907195 1969-02-13 1969-02-13 Magnetically locked, removable high-speed mixing separator for radioactive liquids Pending DE1907195A1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
DE19691907195 DE1907195A1 (en) 1969-02-13 1969-02-13 Magnetically locked, removable high-speed mixing separator for radioactive liquids
US8320A US3674196A (en) 1969-02-13 1970-02-03 Centrifugal mixing and extraction apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19691907195 DE1907195A1 (en) 1969-02-13 1969-02-13 Magnetically locked, removable high-speed mixing separator for radioactive liquids

Publications (1)

Publication Number Publication Date
DE1907195A1 true DE1907195A1 (en) 1970-09-03

Family

ID=5725129

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19691907195 Pending DE1907195A1 (en) 1969-02-13 1969-02-13 Magnetically locked, removable high-speed mixing separator for radioactive liquids

Country Status (2)

Country Link
US (1) US3674196A (en)
DE (1) DE1907195A1 (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4226359A (en) * 1979-03-14 1980-10-07 Beckman Instruments, Inc. Direct drive high speed ultracentrifuge
US4322030A (en) * 1979-03-14 1982-03-30 Beckman Instruments, Inc. Lubrication and cooling system for a high speed ultracentrifuge drive assembly
US5254076A (en) * 1992-08-06 1993-10-19 Arch Development Corporation Centrifugal pyrocontactor
US5591340A (en) * 1995-09-01 1997-01-07 Costner Industries Nevada, Inc. Centrifugal separator
US5571070A (en) * 1996-01-16 1996-11-05 Costner Industries Nevada, Inc. Rotor sleeve for a centrifugal separator
US6440054B1 (en) * 2000-09-18 2002-08-27 George M. Galik Apparatus for liquid-liquid extraction
SE521578C2 (en) * 2002-03-21 2003-11-11 Alfa Laval Corp Ab centrifugal
FR2841485B1 (en) * 2002-07-01 2004-08-06 Commissariat Energie Atomique ANNULAR CENTRIFUGAL EXTRACTOR WITH NOYE AGITATION ROTOR
JP3757197B2 (en) * 2002-08-02 2006-03-22 核燃料サイクル開発機構 Centrifugal extractor
JP3711277B2 (en) * 2002-12-17 2005-11-02 核燃料サイクル開発機構 Centrifugal extractor with non-contact shaft structure
WO2008122026A1 (en) * 2007-04-02 2008-10-09 Mark Allen Systems, devices, and methods for reaction and/or separation
US20190184313A1 (en) * 2017-12-15 2019-06-20 Minextech Llc Method and apparatus for separating insoluble liquids of different densities

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2881974A (en) * 1955-08-08 1959-04-14 Ruf Walter Centrifuge

Also Published As

Publication number Publication date
US3674196A (en) 1972-07-04

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