DE17770C - Innovations in the manufacture of soaps - Google Patents
Innovations in the manufacture of soapsInfo
- Publication number
- DE17770C DE17770C DENDAT17770D DE17770DA DE17770C DE 17770 C DE17770 C DE 17770C DE NDAT17770 D DENDAT17770 D DE NDAT17770D DE 17770D A DE17770D A DE 17770DA DE 17770 C DE17770 C DE 17770C
- Authority
- DE
- Germany
- Prior art keywords
- soap
- soaps
- innovations
- manufacture
- resin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000344 soap Substances 0.000 title claims description 16
- 238000004519 manufacturing process Methods 0.000 title 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N Stearic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 8
- 239000011347 resin Substances 0.000 claims description 8
- 229920005989 resin Polymers 0.000 claims description 8
- 235000021355 Stearic acid Nutrition 0.000 claims description 4
- 239000008117 stearic acid Substances 0.000 claims description 4
- DCXXMTOCNZCJGO-UHFFFAOYSA-N Stearin Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 claims description 2
- 239000004519 grease Substances 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 8
- 235000011121 sodium hydroxide Nutrition 0.000 description 3
- 239000007788 liquid Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000007127 saponification reaction Methods 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 210000002374 Sebum Anatomy 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000012261 resinous substance Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D15/00—Manufacture of resin soap or soaps derived from naphthenic acids; Compositions
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Description
KAISERLICHESIMPERIAL
PATENTAMT.PATENT OFFICE.
PATENTSCHRIFTPATENT LETTERING
KLASSE 23 :/*ettindustrie.CLASS 23: / * ettindustrie.
Patentirt im Deutschen Reiche vom 20. Juli 1881 ab.Patented in the German Empire on July 20, 1881.
Wenn man zur Herstellung einer harten Seife neben Fett auch Harz anwendete, so konnte man von diesem nur wenig hinzusetzen, nämlich etwa 300 kg Harz auf 1000 kg Fett, welche Mischung durch etwa 750 kg Natron mit einer Stärke von 20 ° B. verseift wurde; es war also die Menge des Harzes etwa ein Viertel derjenigen des Fettes. Kam Harz in gröfseren Mengenverhältnissen zur Anwendung, so blieb durch die Menge des absorbirten Wassers die Seife weich und teigartig und trocknete nicht. Die Seife war deshalb keine dauerhafte und nicht geeignet, in Blockform gebracht und zerschnitten zu werden.If you used resin in addition to fat to make a hard soap, you could Add only a little of this, namely about 300 kg of resin to 1000 kg of fat, which mixture was saponified by about 750 kg of soda with a strength of 20 ° B.; so it was the crowd of the resin about a quarter of that of the fat. Resin came in larger proportions When used, the amount of water absorbed kept the soap soft and dough-like, and did not dry. The soap was therefore not permanent and not suitable to be brought into block form and cut up will.
Nach meinem Verfahren kann man zur Herstellung einer harten Seife der betreffenden Masse ein viel gröfseres Quantum von Harz als bisher zusetzen, wobei die Seife trotz der gröfseren Billigkeit die gleichen werthvollen Eigenschaften als Reinigungsmittel behält und ebenso (wenn nicht noch mehr) hart und consistent wird, als die gewöhnliche harte Seife, die mit einör gröfseren Menge von Fett hergestellt wird.According to my method, you can make a hard soap of the subject Add a much larger quantity of resin to the mass than before, the soap in spite of the larger quantity Cheapness retains the same valuable properties as detergents and likewise (if not even more) hard and consistent than the ordinary hard soap that goes with it larger amount of fat is produced.
Mein Verfahren ist folgendes:My procedure is as follows:
Zur Darstellung einer billigen Toiletten-(Wasch-) seife nehme ich etwa 5000 kg guten Talg und verseife denselben in bekannter Weise mit kaustischem Natron von etwa 300 Stärke. Nachdem die erste Einwirkung auf das Fett stattgefunden, setze ich das gleiche Quantum, also etwa 5000 kg reines Harz zu, welches ebenfalls in bekannter Weise zur Verseifung gelangt; auf das Ganze kommen ungefähr 3000 kg kaustisches Natron von ungefähr 30 ° Stärke.To represent a cheap toilet (wash) soap I take about 5000 kg good sebum and verseife same in a known manner with caustic soda of about 30 0 strength. After the first action on the fat has taken place, I add the same quantity, i.e. about 5000 kg of pure resin, which is also saponified in a known manner; There are about 3000 kg of caustic soda of about 30 ° strength on the whole.
Nachdem der Verseifungsprocefs beendet, und während die Lauge noch heifs und flüssig ist, setze ich vor dem Einfüllen in Formen der Seifenmasse ein Quantum im Handel vorkommender krystallisirter Stearinsäure zu, und zwar in einem Mengenverhältnifs von 2 pCt. der ganzen Masse, zu der der Zusatz gemacht wird, oder auch etwa 3 pCt. Stearin. Diese Stoffe setzt man der heifsen, flüssigen Masse allmälig hinzu und mischt sie innig mit der Masse. Dann wird in der bekannten Art das Ganze in Formen gefüllt, worin es zu einer harten consistenten und sehr brauchbaren Seife erkaltet und erhärtet. After the saponification process has ended, and while the lye is still hot and liquid, Before pouring it into molds of the soap mass, I put a quantity of commercially available ones crystallized stearic acid, in a proportion of 2 pCt. The whole Mass to which the addition is made, or about 3 pCt. Stearin. This substance sets one gradually adds to the hot, liquid mass and mixes it intimately with the mass. Then it will be in the well-known way the whole is filled into forms, in which it becomes a hard consistenten and very usable soap cools down and hardens.
Die Stearinsäure wird hierbei also nach stattgefundener Verseifung zugesetzt und nachdem die alkalische Base mit den Fett- und Harzsäuren sich vereinigt hat. < Sie bewirkt, dafs die Seife hart wird, ohne später übermäfsig trocken und spröde zu werden.The stearic acid is added here after saponification has taken place and afterwards the alkaline base has combined with the fatty and resin acids. < It causes the soap to harden without later becoming excessively dry and brittle.
Zugleich macht sie die Seife etwas weniger löslich, wodurch beim Gebrauch an Seife gespart wird.At the same time, it makes the soap a little less soluble, which saves soap when it is used will.
Bei etwas besseren Seifen kann man weniger Harzsubstanz anwenden, ohne dafs man die angewendete Menge von Stearin oder Stearinsäure ändert.With slightly better soaps, less resinous substance can be used without the used one Amount of stearic or stearic acid changes.
Claims (1)
Publications (1)
Publication Number | Publication Date |
---|---|
DE17770C true DE17770C (en) |
Family
ID=294690
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DENDAT17770D Active DE17770C (en) | Innovations in the manufacture of soaps |
Country Status (1)
Country | Link |
---|---|
DE (1) | DE17770C (en) |
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0
- DE DENDAT17770D patent/DE17770C/en active Active
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