CS274805B2 - Method of reaction mixture treatment from /2,2/ paracyclophane and its derivative production - Google Patents
Method of reaction mixture treatment from /2,2/ paracyclophane and its derivative productionInfo
- Publication number
- CS274805B2 CS274805B2 CS231490A CS231490A CS274805B2 CS 274805 B2 CS274805 B2 CS 274805B2 CS 231490 A CS231490 A CS 231490A CS 231490 A CS231490 A CS 231490A CS 274805 B2 CS274805 B2 CS 274805B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- dimethyl sulfoxide
- reaction mixture
- thermal decomposition
- toluene
- layer
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 239000011541 reaction mixture Substances 0.000 title abstract 3
- OOLUVSIJOMLOCB-UHFFFAOYSA-N 1633-22-3 Chemical compound C1CC(C=C2)=CC=C2CCC2=CC=C1C=C2 OOLUVSIJOMLOCB-UHFFFAOYSA-N 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 9
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 abstract 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 238000005979 thermal decomposition reaction Methods 0.000 abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 125000004429 atom Chemical group 0.000 abstract 1
- 238000010533 azeotropic distillation Methods 0.000 abstract 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical compound BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 229910052731 fluorine Inorganic materials 0.000 abstract 1
- 239000011737 fluorine Substances 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 125000001453 quaternary ammonium group Chemical group 0.000 abstract 1
- 238000004064 recycling Methods 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CS902314A CS231490A2 (en) | 1990-05-10 | 1990-05-10 | Method of reaction mixture treatment from (2,2) paracyclophane and its derivatives production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CS902314A CS231490A2 (en) | 1990-05-10 | 1990-05-10 | Method of reaction mixture treatment from (2,2) paracyclophane and its derivatives production |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CS274805B2 true CS274805B2 (en) | 1991-11-12 |
| CS231490A2 CS231490A2 (en) | 1991-11-12 |
Family
ID=5359915
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS902314A CS231490A2 (en) | 1990-05-10 | 1990-05-10 | Method of reaction mixture treatment from (2,2) paracyclophane and its derivatives production |
Country Status (1)
| Country | Link |
|---|---|
| CS (1) | CS231490A2 (cs) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107216232A (zh) * | 2017-06-05 | 2017-09-29 | 昆山彰盛奈米科技有限公司 | 一种派瑞林f的制备方法 |
-
1990
- 1990-05-10 CS CS902314A patent/CS231490A2/cs unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107216232A (zh) * | 2017-06-05 | 2017-09-29 | 昆山彰盛奈米科技有限公司 | 一种派瑞林f的制备方法 |
| CN116283482A (zh) * | 2017-06-05 | 2023-06-23 | 昆山彰盛奈米科技有限公司 | 一种派瑞林f的制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| CS231490A2 (en) | 1991-11-12 |
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