CS237765B1 - Method of heat regeneration and saving of cooling water in substances exchange processes - Google Patents

Method of heat regeneration and saving of cooling water in substances exchange processes Download PDF

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Publication number
CS237765B1
CS237765B1 CS811826A CS182681A CS237765B1 CS 237765 B1 CS237765 B1 CS 237765B1 CS 811826 A CS811826 A CS 811826A CS 182681 A CS182681 A CS 182681A CS 237765 B1 CS237765 B1 CS 237765B1
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Czechoslovakia
Prior art keywords
absorber
partial flow
pactbopa
adcopdepa
cooling water
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CS811826A
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Czech (cs)
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CS182681A1 (en
Inventor
Hans Foerster
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Hans Foerster
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Publication of CS182681A1 publication Critical patent/CS182681A1/en
Publication of CS237765B1 publication Critical patent/CS237765B1/en

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Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25B—REFRIGERATION MACHINES, PLANTS OR SYSTEMS; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS
    • F25B37/00—Absorbers; Adsorbers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A30/00—Adapting or protecting infrastructure or their operation
    • Y02A30/27—Relating to heating, ventilation or air conditioning [HVAC] technologies

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Sorption Type Refrigeration Machines (AREA)
  • Gas Separation By Absorption (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Description

OdsaCTB ΠΡΗΜβΗΘΗΗΗ H3QC)peTSHflfl H30ČpeTemie Kacaeica cnocoda pereHepaqHti Tensa πρκ os-ΗΟΒρβΜβΗΗΟΜ yΜβΗΒΐιιβΗΟ ποτρθόΗοοτΗ oxsaJssaiomeis bosu npH adcopd-W ra3ooópa3HOň padoneň cpesu b xocyio aOcopdqnoHHyio cpesy npnBus&jieHHH aócopópHOHHoro Tensa.OdsaCTB ΠΡΗΜβΗΘΗΗΗ H3QC) peTSHflfl H30ČpeTemie Kacaeica cnocoda pereHepaqHti Tensa πρκ os-ΗΟΒρβΜβΗΗΟΜ yΜβΗΒΐιιβΗΟ ποτρθόΗοοτΗ oxsaJssaiomeis bosu adcopd NPH-W ra3ooópa3HOň padoneň CPEs b xocyio aOcopdqnoHHyio CPEs npnBus & jieHHH aócopópHOHHoro is thinner.

XapaKTspKCTMKa n3BecTHux TexHHqecox pemeHHMXapaKTspKCTMKa n3BecTHux TexHHqecox pemeHHM

B adCOpÓIÍHOHHHX XOSOSHSBHHX yCTaHOBKaX ΠΟΛ ΠΟΗΗΤΗβΜ "pe-UHpKysflpHH pacTBopa" noHHuaeTCH cnocod ssn napu BsmecTBB adCOpÓIÍHOHHHX XOSOSHSBHHX yCTaHOBKaX ΠΟΛ ΠΟΗΗΤΗβΜ "pe-UHpKysflpHH pacTBopa" noHHuaeTCH cnocod ssn napu BsmecTB

Ha.0 , KOTopuB oCHOBUBaeTcn Ha tou, ητο npn aocopd-PHH onpeseneHHbrx ra30B hsh napoB shskmmh aócopdeHTauH Buse-sneTCH Tenso, npnneM ssh coxpaHOHun adcopCpHOHHoro paBHOBscuHnpH OSHHaKOBOM S3BS6HHH H yBeSHMHBaK)lHeÍ5Cfl KOHIjeHTpaiJHH paCTBO-pa HeodxoswMO cHraeHHe TeMnepaiypu aócopdqnn. nosTouy b otsh-nne ot KOHseHcaqHH napoB πρκ adcopdqo Heodxosnuo ocymecTBSHTBπροτΗΒΟτοκ pacTBopa m oxsassaioinero cpescTBa. BepTHKas&HO pac-nojiojKeHHue, tbk Ha3UBaeMue, daueHHue adcopdepu Ηβ βηποπηηιοτsto ycsoBne. Ilosy naiom ancn c SByx ctopoh opocnTesBHaH nseHKapacTBopa h oxsassaKJiueň bosu 03HanaeT HanpaBseHHe npauoTOKa no-tokob BemecTBa h Hesonyciauo HH3Kyio pa3H0qy TeMnepaTyp ueacsybxosou 0 buxosom oxsassaioinefi bosu (uiHpHHa noflca oxjiaKseHHfl).noaiouy HaxosHT npHueHeHne ropnsoHTasBHO pacnosofteHHue aócop-(jepu, y KOTopux προτΗΒΟτοκ pacTBopa 0 oxsaacsaromeft bosu odecne-MHBaoTCH 3a cneT pacnosoKeHHfl spyr Has spyrou HecKonBKHx dno- . 237765 3 kqb, πρΗΜβΜ oxnasaaiomaH Bosa προχοΛπτ qepee TpyOn 0 aio BHyr-peHHee npocTpaHOTBO TpyO xopowo TtocrynHO sm οηηοτκη ( tfážče , Π tom, 28-e H3aaHHe, CTpaHHiíu 249-251).Ha.0, the KOTopuB oCHOBUBaeTcn Ha, ητο aocopd npn-PHH onpeseneHHbrx ra30B HSH napoB shskmmh aócopdeHTauH Buse-sneTCH TENS npnneM ssh coxpaHOHun adcopCpHOHHoro paBHOBscuHnpH OSHHaKOBOM S3BS6HHH yBeSHMHBaK H) lHeÍ5Cfl KOHIjeHTpaiJHH paCTBO PA HeodxoswMO cHraeHHe TeMnepaiypu aócopdqnn. nosTouy b otsh-nne ot KOHseHcaqHH napoB πρκ adcopdqo Heodxosnuo ocymecTBSHTBπροτΗΒΟτοκ pacTBopa m oxsassaioinero cpescTBa. BepTHKas & HO pac-nojiojKeHHue, tbk Ha3UBaeMue, daueHHue adcopdepu Ηβ βηποπηηιοτsto ycsoBne. ILOS NAIO ancn c SByx ctopoh opocnTesBHaH nseHKapacTBopa h oxsassaKJiueň bosu 03HanaeT HanpaBseHHe npauoTOKa no-tokob BemecTBa h Hesonyciauo HH3Kyio pa3H0qy TeMnepaTyp ueacsybxosou 0 buxosom oxsassaioinefi BOSU (uiHpHHa noflca oxjiaKseHHfl) .noaiouy HaxosHT npHueHeHne ropnsoHTasBHO pacnosofteHHue aócop- (jepu y KOTopux προτΗΒΟτοκ pacTBopa 0 oxsaacsaromeft BOSU odecne-MHBaoTCH 3a CNET pacnosoKeHHfl SPyr Has Spyrou HecKonBKHx dno-. 237765 3 kqb, πρΗΜβΜ oxnasaaiomaH Bosa προχοΛπτ qepee TpyOn 0 BHyr AIO-peHHee npocTpaHOTBO TpyO xopowo TtocrynHO SM οηηοτκη (tfážče, Π that 28-e H3aaHHe, 249-251 CTpaHHiíu ).

Enarosapa προτκΒΟτοκγ oskhx ποτοκοβ BemecTš TeMnepa-Typa pacTBopa b κοΗΐχβ npouecca aOcopOunn (KOHueHTpnpoBaHHHfipaOTBOp) nOHraaeTCa HaCTOJIBKO (ΚΟΗρβΗΤρΗρΟΒβΗΗΗβ paOTBOp),qTOOH caM BCJiescTBue TewnepaTypHOfi pa3HHUH Mexuy Hanani-Hoň κ ko-HSHHOfi TeMnepaiypoň npouecca aOcopOunn motct cnyoTB oxnaffisa-roiueft cpeuoft, ecjiH oh uo sioro HaxoanTcn nos Oonee bhcokhm aaB-jieHHeM, HanpHwep uo uaBneHHH uecopOepa. Πρπ stom uoaceT Bocnpu-HHMHTB KOHUeHTpMpOBaHHHfi paCTBOp TOJ1BKO $030ΗβΟΚΟΘ Tenno, Bτο BpeMH khk πρπ npouecce aOcopOunn ocBOČorcaaeTCH CKpbiToe τβπ-310 (Tenno KOHseHcaunn 0 aOcopOunn). EnarouapH STOMy Moaei OhtbpeKynepnpOBaHa tojibko nacTB ocBoOoacuaiomerocH Tenna (XypHan ”, tom 20 (1913), CTpaHHUK 1-9,II4-II9, I50-161, tom 21 (1914) οτρ. 7-14, 21-24). 2jih npoBeaeHHH ποαοΟηογο MHorocTyneH^aToro cnocoča pe-UHpKyjiHUHH paciBOpa πρηωβΗΗΐοτ BepiHKanBHO pacnonoKeHHHis ad-copóep B φορωβ TpyÓHOM K0J10HHH 03 Tpex CeKU,0M. Πρκ STOM oxjias-aaeTCH hhkhhh oxaaacsaiomaH ceKU0H oxna®saioineií Bosoň Ha οτοροΗβKosyxa. B cpesHefó oxnaacuaiomefi ceKunn HarpeBaeTcn κοΗρβΗτρπρο-BaHHbift pacTBop b πρπΜοτοκβ κ HanpaBJíeHKH) TeueHHH ra3a uo τθμ-nepaTypH κηπθηηη (nepsán cTyneHB peuMpnynnunn pacTBopa), a bBepxHeň ceKUHH oxjiaoeHHa yacTB KOHueHTpaposaHHoro pacTBopa,0cno3iB3yioinerocH b KanecTse xnauoareHTa, HarpeBaeTCH BuineTeMnepaiypH κηπβΗΗΗ, thk hto padonan cpeua. (xonosHan cpeaa)Bura30BHBaeTCH nacTHHHo ysce nepes nonauaHneM b aecopdep(BTopan CTyneHB peuMpnynnunH pacTBopa) (naTeHT GCCP K? 276977). 3to BHnojiHeHHe ΗΜββτ pna cymecTBeHHHX HesocTaTKOB, κοτο-pne 3aTpyuHHiOT npaKTnuecKoe Hcno?iB3OBaHHe H3odpeTeHHH: I. Ckopoctb TeneHHH oxnasEuawH cpeun b cpeAHefl κ Bepx-Heň oxaaKsaíoinnx ceKUHnx Hpe3BuqaĚH0 Mana a ksk cneacTBne stopoB03HHK3IOT HetínaronpHHTHue ycnosHn sjih TennooOueHa. B cpejwefioxjia^aaioineíí οθκη,ημ (nepBan peuHpKynHUHn) κοηπηβοτΒΟ oÓoraiueH-Horo pacTBopa, κοτορκβ μοηθτ 0cnojiB3OBaTBCH b KanecTBe oxnaK-saoiieií cpeuu, 3asaH0 h eso Hens3H perynnpoBaTS. B Hnraefi ceK-U00 KOJinneCTBO xjiauoareHTa mokho Obcio Oh yBejiHHHTB. Sto OflHa-ko πρΗΒβηο Ou κ sononHHTenBHOuy HesocTaTKy, CBH3aHH0My c Teu,hto b stom cnynae eme Oonsiue CH030nacs Oh pa3H0CTB TeMnepaTyp0 pacxos oxjiaoaromeM bouh CTan Oh HenouepHO bhcokhm. 237765 4 2. HcnonB3OBanne MeaipydHoro npocTpaHCTBa KO&amp;yxoTpyd-hux annapaTOB flnn oxnaatfleHHa nocpeflCTBOu oxnaKflaroiueň bosu(mm ceKqHH) npaKTunecKH ηοκηιοηβΗΟ H3-3a HeH3Óe3Kno boshh-KawinHX 3arpH3HeHHí5 h oicyTCTByioinefi bo3mo3Khocth ohhctkh. 3. HarpeBaHHe κοηηθητρηροβηηηογο pacTBopa flo κηπθηηη bnepBOfl penHpKyjiauHH pacTBopa (cpeflHHH οθκιικπ) npeflnonaraeioqeHB BHCOKH6 HaManBHbie TeMnepaTypu adcopdnnH. Ho H3-3a θτο-ro noJiywaioTCH, c flpyroři ciopoHbí, tojibko οηθηβ Manoň mwpoTUHHTepBan oóe3raKHBaHHH (pa3HHiia b KOHueHTpamm Meatfly κοηηθητ-ΡΗΡΟΒΘΗΗΗΜ Η OdeflHeHHblM paCTBOpOM) H 3T0 npeflnOnaraeT IipaKTH-qecKH otk33 ot TennoodMeHa MejKsy odeflHeHHuu a KOHixeHTpnpoBaH-HUM paCTBOpOM. 4. Enaroflapa npeflBapHTenBHOii sera3aiíHH pado^eň .cpeflu (ox-naacflaioinaH cpefla) bo BTopofi pennpKynniíHH yMeHBiuaeTca KOHueHipa-IÍHH ΚΟΗμθΗΤρΗρθΒ3ΗΗΟΓΟ paCTBOpa H HaXOflflmerOCH C HHM B paBHO-B6CHH napa padonefi cpeflu. Sthm noBHimaeTcn noTpedHOCTB b oxnas-aawen cpese flna npon3BOflCTBa pepHpKynwH b KOHiíeHTpaijHOHHOňKOJiOHHe ascopóepa ujím yiíeHBinaeTCH nncTOTa padonefi cpeflH. Ctohkh 3peHHn hhctote padoneft cpeflu oflHaKO cnenyeT CTpeuHTBca κ Towy, MTodbi κοΗηβΗτρΗρΟΒβΗΗΗβ pacTBop nocTynaa b flecopdep cdonee HH3K0M TeMnepaTypoň w uaKCHManBHO bucokom KOHneHTpaiíHew,ητο<5Η τθμ canítiM odecnenHBanacB BbicoKan οτθπθηβ ode3raoBaHHH.KaK pa3 stu φβκτορκ He odecneHHBaflHCB b m3bscthux ycTpoficTBax. B ropH3OHTaJiBHO pacnonoKeHHux adcopdepax, KOTopue βηποληθηηοπηοθηηημ cnocodoM c 3neueHTaMH, pacnojioKeHHbiMH flpyr Has flpy-roM, dáno dbi, κοηθηηο, bo3mokho, b odnacTjj bhcokoíí TeMnepaTypaadcopdepa (He3HanHTenBH0ii KOHpeHTpaflHH pacTBopa), to eoTB bcawOM ΒβρχΗβΜ adcopdepe, πρΗΐ,ιβΗΗΤΒ KOHneHTpupoEaHHhifí pacTBopb KanecTBe oxna&amp;flaiomeií cpefla η τηκημ odpa3OM ocymecTBHTB cno-cod penupKynnííHH pacTBopa (naTeHT ΦΡΓ !.? 3645S2, V&amp; J -scyp-Han tom 84 (1940) Ks 3, οτρ.41-47). Ητο 3Ta BO3MO3KHOCTB πρηκτηπθοκη dnna He peann30BaHa, oÓBHcHfleTCH yMeHBineHHeM uihphhh oxna^flaromero noHca oxnascflaiomeňBOflbí, T3K κβκ xoth nacTB Tenna adcopdííHH peKynepupyeTCH, hooflHOBpeMeHHO ypoBeHB TeiraepaTypH flna oxnasflaeMOfc boaom nacTHadcopdepa yMeHBiaaeTCH h noaiouiy He ωοκετ daiB flocmrHyTO yiieHE-meHiie pacxofla BOfla.Enarosapa προτκΒΟτοκγ oskhx ποτοκοβ BemecTš TeMnepa-Typa pacTBopa b κοΗΐχβ npouecca aOcopOunn (KOHueHTpnpoBaHHHfipaOTBOp) nOHraaeTCa HaCTOJIBKO (ΚΟΗρβΗΤρΗρΟΒβΗΗΗβ paOTBOp) qTOOH Cam BCJiescTBue TewnepaTypHOfi pa3HHUH Mexuy Hanani-hon κ co-HSHHOfi TeMnepaiypoň npouecca aOcopOunn motct cnyoTB oxnaffisa-roiueft cpeuoft, ecjiH oh uo Siora HaxoanTcn nose Oonee bhcokhm aaB-jieHHeM, HanpHwep uoBneHHH uecopOepa. Bocnpu-HHMHTB KOHUeHTpMpOBaHHHfi paCTBOp TOJ1BKO $ 030ΗβΟΚΟΘ Tenno, BpeMH khk πρπ npouecce aOcopOunn ocBOČorcaaeTCH CKpbiToe τβπ-310 (Tenno KOHseHcaunn 0 aOcopOunn). EnarouapH STOMY Moaei OhtbpeKynepnpOBaHa tojibko nacTB ocBoOoacuaiomerocH Tenna (XypHan ”, tom 20 (1913), CTpaHHUK 1-9, II4-II9, I50-161, tom 21 (1914) οτρ. 7-14, 21-24). 2jih npoBeaeHHH ποαοΟηογο MHorocTyneH ^ aToro cnocoča pe-UHpKyjiHUHH paciBOpa πρηωβΗΗΐοτ BepiHKanBHO pacnonoKeHHHis ad-copóep B φορωβ TpyÓHOM K0J10HHH 03 Tpex CeKU, 0M. Πρκ STOM oxjias-aaeTCH hhkhhh oxaaacsaiomaH ceKU0H oxna®saioineii Boson Ha οτοροΗβKosyxa. B cpesHefó oxnaacuaiomefi ceKunn HarpeBaeTcn κοΗρβΗτρπρο-BaHHbift pacTBop b πρπΜοτοκβ κ HanpaBJíeHKH) TeueHHH ra3a uo τθμ-nepaTypH κηπθηηη (unwritten cTyneHB peuMpnynnunn pacTBopa) and bBepxHeň ceKUHH oxjiaoeHHa yacTB KOHueHTpaposaHHoro pacTBopa, 0cno3iB3yioinerocH b KanecTse xnauoareHTa, HarpeBaeTCH BuineTeMnepaiypH κηπβΗΗΗ, THK HTO padonan cpeua. (xonosHan cpeaa) Bura30BHBaeTCH nacTHHHo ysce do not nonauaHneM b aecopdep (BTopan CTyneHB peuMpnynnunH pacTBopa) (naTeHT GCCP K? 276977). 3to BHnojiHeHHe ΗΜββτ PNA cymecTBeHHHX HesocTaTKOB, κοτο-climbs 3aTpyuHHiOT npaKTnuecKoe Hcno? IB3OBaHHe H3odpeTeHHH: I. Ckopoctb TeneHHH oxnasEuawH cpeun b cpeAHefl Bepx κ-hen oxaaKsaíoinnx ceKUHnx Hpe3BuqaĚH0 Mana and KSK cneacTBne stopoB03HHK3IOT HetínaronpHHTHue ycnosHn sjih TennooOueHa. B cpejwefioxjia aaioinei οθκη, ημ (p H eu eu eu eu eu eu)))) κ Ó o o o o o o o opa opa opa opa opa opa opa opa opa ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens ens B Hnraefi ceK-U00 KOJinneCTBO xjiauoareHTa moko Obcio Oh yBejiHHHTB. Sto OflHa-ko ΗΒ son son sononHHTenBHOuy HesocTaTKy, CBH3aHH0My c Teu, hto b stom cnynae eme Oonsiue CH030nacs Oh pa3H0CTB TeMnepaTyp0 pacxos oxjiaoaromeM bouh CTan Oh HenouepHO bhcokhm. 237 765 4 2. HcnonB3OBanne MeaipydHoro npocTpaHCTBa KO &amp; yxoTpyd-Hux annapaTOB flnn oxnaatfleHHa nocpeflCTBOu oxnaKflaroiueň BOSU (mm ceKqHH) npaKTunecKH ηοκηιοηβΗΟ H3-3a HeH3Óe3Kno boshh-KawinHX 3arpH3HeHHí5 h oicyTCTByioinefi bo3mo3Khocth ohhctkh. 3. HarpeBaHHe κοηηθητρηροβηηηογο pacTBopa flo κηπθηηη bnepBOfl penHpKyjiauHH pacTBopa (cpeflHHH οθκιικπ) npeflnonaraeioqeHB BHCOKH6 HaManBHbie TeMnepaTypu adcopdnnH. Ho H3-3a θτο-ro noJiywaioTCH c flpyroři ciopoHbí, tojibko οηθηβ Manon mwpoTUHHTepBan oóe3raKHBaHHH (b pa3HHiia KOHueHTpamm Meatfly κοηηθητ-ΡΗΡΟΒΘΗΗΗΜ Η OdeflHeHHblM paCTBOpOM) H-3T0 npeflnOnaraeT IipaKTH qecKH otk33 ol TennoodMeHa MejKsy odeflHeHHuu and KOHixeHTpnpoBaH-paCTBOpOM HUM. 4. Enaroflap npefBapHTenBaHaHaHePePeRe (cOfAfacAaLaNH cpefAe) BopofiPnePnCHnMHeHBiAeHcHePHeHHlHHlHcBrHcBp paPBO-B6CHHlMeOCH C HHM B paBHO-B6CHH napa padonefe cpeflu. Sthm noBeTeTcn noTpedHOCTB b oxnAnAnA cpese flnnPon3BOFlCTBa pepHpKynwH b KOHhEHeHeHHOHOnHiOnHeCoPoPoPeReHyHBinEtCH nncTOTa padonefi cpeflH. Ctohkh 3peHHn hhctote padoneft cpeflu oflHaKO cnenyeT CTpeuHTBca κ Towy, MTodbi κοΗηβΗτρΗρΟΒβΗΗΗβ pacTBop nocTynaa b flecopdep cdonee HH3K0M TeMnepaTypoň w uaKCHManBHO bucokom KOHneHTpaiíHew, ητο <5Η τθμ canitie odecnenHBanacB BbicoKan οτθπθηβ ode3raoBaHHH.KaK PA3 growth φβκτορκ He odecneHHBaflHCB b m3bscthux ycTpoficTBax. B ropH3OHTaJiBHO pacnonoKeHHux adcopdepax, KOTopue βηποληθηηοπηοθηηημ cnocodoM c 3neueHTaMH, pacnojioKeHHbiMH flpyr Has flpy-ROM, given DBI, κοηθηηο, bo3mokho b odnacTjj bhcokoíí TeMnepaTypaadcopdepa (He3HanHTenBH0ii KOHpeHTpaflHH pacTBopa) it eoTB bcawOM ΒβρχΗβΜ adcopdepe, πρΗΐ, ιβΗΗΤΒ KOHneHTpupoEaHHhifí pacTBopb KanecTBe oxna &amp; flaiomeií cpefla η τηκημ odpa3OM ocymecTBHTB cno-cod penupKynniHH pacTBopa (naTeHT ΦΡΓ!.? 3645S2, V & J -scyp-Han tom 84 (1940) Ks 3, οτρ.41-47). Ητο 3TA BO3MO3KHOCTB πρηκτηπθοκη DNNA He peann30BaHa, oÓBHcHfleTCH yMeHBineHHeM uihphhh oxna ^ flaromero noHca oxnascflaiomeňBOflbí, T3K κβκ XOTH nacTB Tenna adcopdííHH peKynepupyeTCH, hooflHOBpeMeHHO ypoBeHB TeiraepaTypH flna oxnasflaeMOfc Boao nacTHadcopdepa yMeHBiaaeTCH h noaiouiy He ωοκετ Daiba flocmrHyTO yiieHE-meHiie pacxofla BOfla.

23776J 523776J 5

UejiB H3o6peTeHHHUejiB H3o6peTeHHH

Ilejih H3QdpeieHHH - peKynepupoBaTB κέικ mokho doJiBme no-jie3Hyio qacTL Tenna adcopdmw, ocBOdoxaaionerocH npn adcopGmanra30 - hjih napoodpa3Hbix BemecTB b κκΛκοβ adcopdnnoHHoií cpeae,CHH3WTB HeodXOSHMyiO /WH 3Τ0Γ0 nOTpSÓHOCTB 'OXJiaXaaiOlHeH BOJUI HnonywHTB doflBuiwe ιππροτΕ oxnaKaaiomero nonca oxjiaMísaioiueň bojuj.Πρκ 3T0M flOJIKHH ÓHTh yCTpaHeHH HeaOCTaTKH H3BeCTH0r0 ypOBHflT6XHHKH, KOK OTpaHHMβΗΗΗ CT6II6HH Ο063Γεΐ5ΚΗΒ3ΗΗΗ H KpafiHe Ηβ-TiocTaToqHoro μοποπβ3οβ3ηηη pacnonaraeuoro Tenna.Ilejih H3QdpeieHHH - peKynepupoBaTB κέικ Mokh doJiBme no-jie3Hyio qacTL Tenna adcopdmw, ocBOdoxaaionerocH NPN adcopGmanra30 - hjih napoodpa3Hbix BemecTB b κκΛκοβ adcopdnnoHHoií CPEA, CHH3WTB HeodXOSHMyiO / WH 3Τ0Γ0 nOTpSÓHOCTB 'OXJiaXaaiOlHeH fights HnonywHTB doflBuiwe ιππροτΕ oxnaKaaiomero nonce oxjiaMísaioiueň bojuj.Πρκ 3T0M flOJIKHH ÓHTh yCTpaHeHH HeaOCTaTKH H3BeCTH0r0 ypOBHflT6XHHKH, KOK OTpaHHMβΗΗΗ CT6II6HH Ο063Γεΐ5ΚΗΒ3ΗΗΗ H KpafiHe Ηβ-TiocTaToqHoro μοποπβ3οβ3ηηη pacnonaraeuoro Tenna.

H3jiO3KeHne cyiUHOCTK n3odpeTeHHH B ocHOEy H3oÓp6T6HHH nonoseHa TexHHqeCKan 3aaaia pa3BHTBcnocod, npH KOTOpOM 03BeCTHblft ΠρΗΗΙίΗΠ pei];HpKyJlHU,KH paCTBOpaSJífj peKynepauHH Tenna adcopdiío πριηίεΗΗΐοτ de3 orpammeHUH ma-ρΗΗΜ oxnaxaawro nonca oxna&amp;jiameií bojuj h ue yxyjuaan οτθπθηβodearaMBaHHH paCTBOpa djiaroaapn npejtBapmeJiBHOfi aera3auHH ad-copdHpoEaHHOií padoqeft cpeau bhs aecopdepa npn μιιηημβηβηομ pac-xoae oxnaxaaBineM bose.H3jiO3KeHne cyiUHOCTK n3odpeTeHHH B ocHOEy H3oÓp6T6HHH nonoseHa TexHHqeCKan 3aaaia pa3BHTBcnocod, NPH KOTOpOM 03BeCTHblft ΠρΗΗΙίΗΠ PEI]; HpKyJlHU KH paCTBOpaSJífj peKynepauHH Tenna adcopdiío πριηίεΗΗΐοτ DE3 orpammeHUH ma ρΗΗΜ oxnaxaawro nonce oxna &amp; jiameií fight h UE yxyjuaan οτθπθηβodearaMBaHHH paCTBOpa djiaroaapn npejtBapmeJiBHOfi aera3auHH ad-copdHpoEaHHOií padoqeft CPEA bhs aecopdepa npn μιιηημβηβηομ pac-xoae oxnaxaaBineM bose.

Cootbstctbshho H3odpeTeHHio 3Ta saaana peinaeTCH τβω» ητοcoxpaHHH πρΗΗΐχκπ opouieHHfl , κοτοπξβΗΗΕβ pacTBop, odorameHHEí}padoqefi cpeaoň, pa3aenfleTCH Ha jisa qacTHqHEX ποτοκβ, KOTopuenapajuiejiBHO nponycKaiOTCH b KaqecTse οοηοβηογο ποτοκβ qepe3 ad-copdepa κ b KanecTse qaciHqHoro ποτοκβ qepe3 adcopdep qacmqHO-ro noToxa. Πρκ stom odoramaeTCH η3βθοτηεμ odpasou HCTomeaHufipaciBop b odonx adcopďepax padoqefí cpeaofi. HacTnaHEfi ποτοκ koh-iíeHTpHpoBaHHoro paciBopa, BHTeKaiomHň H3 aacopdepa aacTnaHoronoTOKa, CLíeuiHBaeTca οπητβ c ochobhem ποτοκομ b odnaciH noBumeH-HOfi KOHUeHTpaiíHH, H OdDÍHŮ ΠΟΤΟΚ KOHUeHTpiipOBaHHOPO paCTBOpa H3~npaBnaeTCH 3aTeM b adcopdep qaCTHMHoro noTOKa b KaueciBe oxnas-aaramefi cpeau. Oda adcopdepa padoTaBT npw btom caMHM no cedeH3BecTHHM cnoeodow no npHHnuny προτΗΒΟτοκβ raa b (5jih3kom k He-na y pestHMe. B npeHMymecTBeHHOM ηοποβηθηκη cnocoda cornacHO H3odpeTe-hhk) npeaycMOTpeHO, πτο qacTnqHHfi ποτοκ κοΗηβΗτρηροΒαΗΗΟΓΟ pac-TBopa, noKnaaiomHH adcopdep πθοτηπηογο ποτοκβ, οπητβ CMeuiHBaeTCHc ochobhem ποτοκοω nepea nocnéaHHM aaeMeHTOM adcopdepa. 237765Cootbstctbshho H3odpeTeHHio 3TA saaana peinaeTCH τβω »ητοcoxpaHHH πρΗΗΐχκπ opouieHHfl, κοτοπξβΗΗΕβ pacTBop, odorameHHEí} padoqefi cpeaoň, pa3aenfleTCH Ha Jisa qacTHqHEX ποτοκβ, KOTopuenapajuiejiBHO nponycKaiOTCH b KaqecTse οοηοβηογο ποτοκβ qepe3 ad-copdepa κ b KanecTse qaciHqHoro ποτοκβ qepe3 adcopdep qacmqHO-ro NOTOX. Πρκ stom odoramaeTCH η3βθοτηεμ bypass HCTomeaHufipaciBop b odonx adcopdepax padoqefi cpeaofi. HacTnaHEfi ποτοκ iíeHTpHpoBaHHoro paciBopa KOH, H3 BHTeKaiomHň aacopdepa aacTnaHoronoTOKa, CLíeuiHBaeTca οπητβ c ochobhem ποτοκομ b odnaciH noBumeH-Hofi KOHUeHTpaiíHH H Oddi ΠΟΤΟΚ KOHUeHTpiipOBaHHOPO paCTBOpa H3 ~ npaBnaeTCH 3aTeM b adcopdep qaCTHMHoro noTOKa b KaueciBe oxnas-aaramefi CPEA. Oda adcopdepa padoTaBT NPW btom Camhi no cedeH3BecTHHM cnoeodow no npHHnuny προτΗΒΟτοκβ Raa b (5jih3kom to He-to y pestHMe. B npeHMymecTBeHHOM ηοποβηθηκη cnocoda cornacHO H3odpeTe-HHK) npeaycMOTpeHO, πτο qacTnqHHfi ποτοκ κοΗηβΗτρηροΒαΗΗΟΓΟ pac-TBopa, noKnaaiomHH adcopdep πθοτηπηογο ποτοκβ, οπητβ CMeuiHBaeTCHc ochobhem ποτοκοω nepea nocnéaHHM aaeMeHTOM adcopdepa. 237765

ΠΡΜΜΘΡ BbinOJIHSHHHΠΡΜΜΘΡ BbinOJIHSHHH

Unocod cornacHO H3odpeTeHHio noapodHee ποηοηθη Ha ηημ-cjiesytomeM npHMepe βηποληθηηη. lípu stom npeHwyinecTBeHHo H3jia-raioTCfl oi^eJiBHbie sianu cnocoda Ha ocHOBe npnHiínnnaJn>Hoíi cxe-Mhl COOTBeTCTByromeil yCTaHOBKH.Unocod cornacHO H3odpeTeHHio noapodHee Ha ηημ-cjiesytomeM npHMepe βηποληθηηη. lime stom npeHwyinecTBeHHo H3jia-raioTCfl oi ^ eJiBHbie sianu cnocoda Ha ocHOBe npnHininJn> Hoii cxe-Mhl COOTBeTCTByromeil yCTaHOBKH.

Ha coOTBeTGTByioiHMX aepTeisax nOKa3ano: Φηγ. I - yCTaHOBKa sjih npoBssQHHH cnocoda cornacHOí?3oopereHnra c ropu3OHraJ3BHO pacnoaoiíeHHbíMH adcopdepow h ad-copdepoM yacTiHHoro noTOKa. Φηγ. 2 - ycTaHOEKa coraacHO Φηγ. I, c BepTHKaJiBHO pac-ποηοκβΗΗΗΜ adcopdepow qacTHMHoro noTOKa. B yCTaHOBKaX B COOTBeTCTBKH C φΗΓ.Ι H 2 HCTOmeHHBlíí pac-tbop (I), nocTynaioinHM H3 He H3odpa3seHHoro secopdepa, oxjiaMa-eTCH b TenJioodt.;eHHHKe (10) a paasejifleTCH Ha SBa πηοτηηηηχ πο-τοκη b paenpeseBWTejiBHOM ycTpoňCTBe (7). Ilpu btom πολβολητοηochobhoh ποτοκ HCTomeHHoro pacTBopa I b adcopdep 3, B TO Bpe-MH K3K HaCTHHHblM ΠΟΤΟΚ 6Γ0 I ΠρΟΧΟΜΤ B adcopdep HaCTHHHOrOΠ0Τ0Κ3 2 B C00TB6TGTBHH C ΤβΠΛΟΜ, BOCnpHHHM.aeiíblM KOHUeHTpHpO-βθηηημ pacTBopoM. Adcopdep 3 coctoht, Hanpnisep, H3 neThipexpacnojioseHHbix ropnáOHiaJiBHO aneMeHTOB 3/1 ao 3/4 (nonc adcop-tíepa), b to Bpeun khk adcopdep iiacTJWHoro ποτοκβ'2 codpaH H3τρβχ Γ0ρΗ30ΗΤ3ΛΒΗ0 pacnojioKeHHbix 33ieueHTOB adcoptíepa 2/1 so2/3 (noHC adcopdepa ηθοτηηηογο noTOKa) (Φηγ.Ι) hjih odpa3OBaH0ΛΗΗΜ BepTHKajiBHO pacnonoKeHHEM djiOKObi adcopdepa (Φηγ.2).Ha coOTBeTGTByioiHMX aepTeisax nOKa3ano: Φηγ. I - yCTaHOBKa sjih npoBssQHHH cnocoda cornacHO? 3oopereHnra c ropu3OHraJ3BHO pacnoaoiíeHHbíMH adcopdepow h ad-copdepoM yacTiHHoro noTOKa. Φηγ. 2 - ycTaHOEKa coraacHO Φηγ. I, c BepTHKaJiBHO pac-ποηοκβΗΗΗΜ adcopdepow qacTHMHoro noTOKa. B yCTaHOBKaX B COOTBeTCTBKH C φΗΓ.Ι H 2 HCTOmeHHBi pac-tbop (I), oxjiaMa-eTCH b TenJioodt.; CTomeΓpeCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTblCTΟΤΟΚCTΟΤΟΚCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTCTOCTCTCTCTCTCTCTCTCT00CTCTCTCTCTCT Adcopdep 3 coctoht, Hanpnisep, H3 neThipexpacnojioseHHbix ropnáOHiaJiBHO aneMeHTOB 3/1 and 3/4 (nonce adcoptíepa) b to Bpeun KHK adcopdep iiacTJWHoro ποτοκβ'2 codpaH H3τρβχ Γ0ρΗ30ΗΤ3ΛΒΗ0 pacnojioKeHHbix 33ieueHTOB adcoptíepa 2/1 SO 2/3 (noHC adcopdepa ηθοτηηηογο noTOKa ) (Ιηγ.Ι) hjih odpa3OBaH0ΛΗΗΜ BepTHKajiBHO pacnonoKeHHEM djiOKObi adcopdepa (.2ηγ.2).

HacTH^Hbie ποτοκη HCTomeHHoro pacTBopa I, no23BaeMtie badcopdep 3 h adcopdep πθοτηηηογο noTOKa 2, CTenaioT πλθηκομCBepxy bhh3 napaJmeaBHO spyr Apyry b odowx annapaTax, noraomaHpadonyso cpesy, npHneM pa3tíaBaeHHuft pacTBop I odoramaeTCH nos-BeseHHOíí padoneíí cpe/tofl 6 ot cTyneHH κ CTyneHH.HacTH ^ Hbie ποτοκη HCTomeHHoro pacTBopa I no23BaeMtie badcopdep 3h adcopdep πθοτηηηογο noTOKa 2 CTenaioT πλθηκομCBepxy bhh3 napaJmeaBHO SPyr pyr b odowx annapaTax, noraomaHpadonyso CPEs, nphnami pa3tíaBaeHHuft pacTBop I odoramaeTCH nose-BeseHHOíí padoneíí CPE / 6 OT tofl cTyneHH κ CTyneHH.

BacTHqHhiíi ποτοκ KOHneHTpnpoBaHHoro pacTBopa, βηχοληιιιημ·H3 nocj;e2Hero saeMeHTa adcopdepa ηηοτηηηογο noTOKa 2/3 oh H3BepTHKanBHO pacnojiOKeHHoro adcopdepa nacTHHHoro noTOKa odBesn-ηηθτοη οπητβ c ocHOBHbiu ποτοκομ oóoranieHHoro pacTBopa nepeanoc.nesKHu 326μθητομ 3/4 adcopdepa 3. 3to odBesnHeHHe odonxnacTHHHbtx ποτοκοΒ odorauieHHoro pacTBopa nspea BJieueHTOM ad-copdepa 3/4 HeodXOAHMO SJIH AOCTHKeHHH UaKCHUaHBHO B03M03KH0ÍÍKOHpeKTpauHH doraToro pacTBopa b cawoři HHXHefi (cauofl xojioshoh) 237765 qacTH adcopdepa 3. Odmaň ποτοκ KOHiíeHTpupoBaHHoro pacTBopa5 BuxoflHT nocjie ajieuema adcopdepa 3/4 a3 adcopdepa 3. OxaaHc-S6HHe adcopdepa 3 npoacxosaT tísarosapa no/iBOsy xonosHoropacTBopa bo bxos oxjiawa»meí5 bojím 8 npoTHBOTOKy yepe3 saeMeH-Thj adcopdepa 3/4, 3/3, 3/2 a 3/1 a OTBOjíy HarpeTofí oxaaoa-rameň bojím y BMxosa oxaaKjiaraineK bojím 9. KOHiíeHTpHpoBaHHuft pacTBop 5 nodynaeT yepes cdopHHKpacTBopa 4 b Hacoc II, CMMaerca so doziee βμοοκογο jiaBseHaaa noSBOSWTCH κ adcopdepy nacTannoro ποτοκ-a 2 b KanecTBe ox-jiaMaramefi cpe jím. B KanecTBe oxjiaKsaramea cpejíM προτβκβετ koh-iíeHTptipoBaHHufí padBop 5 b προτπΒΟτοκβ nepe3 oTflejiBHue sneueH-tm adcopdepa ηηοτηηηογο ποτοκβ 2/3, 2/2 a 2/1 hih qepe3 sep-TMKaJiBHO pacnojiOKSHHbíM adcopdep nacTanHoro ποτοκβ 2 a Bocnpa-HisuaeT npa stolí τθιμο adcopduaa. nocjie BHXosa KOHiíeHTpapoBaH-ηογο pacTBopa 5, npaMeneHHoro b KanecTBe oxnascjiaramero cpejíCT-Ba, H3 adcopdepa nacTanHoro ποτοκβ a saJiBHefiuiero OTdopa Ten-aa b TennoodMeHHHKe 10 KOHiíeHTpapoBaHHMíi paciBop ίζοκβτ GmtbBO3BpameH b secopdep. Adcopdep qacTumíoro ποτοκβ 2 Μοκβτ GmtbnosTOwy BbinojiHeH cornacHo tyar.2 b Base ΒβρτπκβηΒΗΟ pácnosoKeH-ηογο annapaia c opomeHaeM nponyCKaeMoro nepe3 TpydKOodorama-eworo pa3daBneHHoro pacTBopa I, τβκ ksk pacTBop napKysapyeTb 3aMKHyT0M Kpyre a MeKTpydHoe npocTpaHCTBO ne uoscei Gmtb3arpH3aeH0 acnojiB3yeMHM b adcopdepe nacianHoro ποτοκβ 2 b Ka-necTBe xnasoareHTa κοΗΐίβΗτρπροΒΒΗΗΜΜ ποτοκομ 5. 237765 8 $OPMVJia ΗΞΟΰρβΤΘΗΗΗBacTHqHhiíi ποτοκ KOHneHTpnpoBaHHoro pacTBopa, βηχοληιιιημ · H3 nocj; e2Hero saeMeHTa adcopdepa ηηοτηηηογο noTOKa 2/3 oh H3BepTHKanBHO pacnojiOKeHHoro adcopdepa nacTHHHoro noTOKa odBesn-ηηθτοη οπητβ c ocHOBHbiu ποτοκομ oóoranieHHoro pacTBopa nepeanoc.nesKHu 326μθητομ 3/4 adcopdepa third 3to odBesnHeHHe odonxnacTHHHbtx ποτοκοΒ odorauieHHoro pacTBopa NSPE BJieueHTOM adcopdepa 3.4 HeodXOAHMO SJIH AOCTHKeHHH UaKCHUaHBHO B03M03KH0ÍÍKOHpeKTpauHH doraToro pacTBopa b cawoři HHXHefi (cauofl xojioshoh) 237765 qacTH adcopdepa third Ödman ποτοκ KOHiíeHTpupoBaHHoro pacTBopa5 BuxoflHT nocjie ajieuema adcopdepa 3.4 a3 adcopdepa third OxaaHc-S6HHe adcopdepa 3 npoacxosaT tísarosapa nO / ibosy xonosHoropacTBopa bo bxos oxjiawa »me5 i'm afraid 8 npoTHBOTOKy yepe3 saeMeH-Thj adcopdepa 3/4, 3/3, 3/2 and 3/1 and OTBOyy HarpeTofi oxaaoa-rama i'm afraid BMxosa oxaaKjiaraineK i'm afraid 9 b Haco c II, CMMaerca so doziee jiaBseHaaa noSBOSWTCH κ adcopdepy nacTannoro ποτοκ-a 2 b KanecTBe ox-jiaMaramefi cpe. B KanecTBe oxjiaKsaramea cpejíM προτβκβετ KOH iíeHTptipoBaHHufí padBop 5 b προτπΒΟτοκβ nepe3 oTflejiBHue sneueH-TM adcopdepa ηηοτηηηογο ποτοκβ 2/3, 2/2 and 2/1 sep-hih qepe3 TMKaJiBHO pacnojiOKSHHbíM adcopdep nacTanHoro ποτοκβ 2 Bocnpa HisuaeT NPA-Stoll τθιμο adcopduaa. nocjie BHXosa KOHiíeHTpapoBaH-ηογο pacTBopa 5, npaMeneHHoro b KanecTBe oxnascjiaramero cpejíCT-Ba, H3 adcopdepa nacTanHoro ποτοκβ and saJiBHefiuiero OTdopa Ten-aa b TennoodMeHHHKe 10 KOHiíeHTpapoBaHHMíi paciBop ίζοκβτ GmtbBO3BpameH b secopdep. Adcopdep qacTumíoro ποτοκβ 2 Μοκβτ GmtbnosTOwy BbinojiHeH cornacHo tyar.2 Base ΒβρτπκβηΒΗΟ pácnosoKeH b-c ηογο annapaia opomeHaeM nponyCKaeMoro nepe3 TpydKOodorama-eworo pa3daBneHHoro pacTBopa I τβκ ksk pacTBop napKysapyeTb 3aMKHyT0M Kpyre and MeKTpydHoe npocTpaHCTBO not uoscei Gmtb3arpH3aeH0 acnojiB3yeMHM adcopdepe nacianHoro ποτοκβ b 2 b Ka necTBe xnasoareHTa 5 237765 8 $ OPMVJia ΗΞΟΰρβΤΘΗΗΗ

1. Cnocod pereHepauwH Tensa n skohoííhh oxnaBsaiomeiíbossi npH atícopdpHK nerKO adcopOnpyeMux rs30B hjih napoB jkhs-kogtbio, conpoBo^saioineMCH BHseneHHeM Tensa adcopdptín, npH pe-reHepaTHBHOM ηοπολβ30β3ημη no bo3uo;íihocth dojiBineft nacTtiTenna adcopdotHH, πρη πρημθηοηηη opoiuaeMHX adcopdepoB, o τ -ji h q a ίο m η ň c h tom, πιο oÓoramaeMMfl pasdaBseHHUÍipadBop I aesHT Ha ssa naCTHHHbix ποτοκθ, κοτορωθ napannesBHospyr spyry npoxosHT nepe3 adcopdep 3 h adcopdep πθοτηπηογοποτοκθ 2, odoramaacB πρη θτομ H3BecTHHM odpa3ou padonefó cpe-soií (6), h naciHnHtifi ποτοκ pacTBopa, BuxosnmHfi H3 adcopdepaqacTHHHoro ποτοκθ (2) οπητβ cuenoaioT c ockobhum ποτοκοιλ do-nee BbicoKoíi KOHbteHTpauHH κ odinnf; ποτοκ KOHiíeHTpnpoBaHHoropacTBopa (5) nosaeTcn 3aTsw b adcopdep πηοτμπηογο ποτοκη (2)b KanecTse oxjiajssaiomeK cpesw, npuneM oda adcopdepa (3,2) pa-dOTHIOT H3BeCTHbIM 0dpa30bi, B pe^HMe npOTHBOTOKa UJÍM djlH3K0U κ Heuiy pexwMe. 2. Cnocod ποπ. I, oiJiHqaBniHfiCfl τθμ,πτοnacTHHHbiií ποτοκ KOHneHTpnpoBaHHoro pacTBopa, noKHsaiomuK ad-copdep naCTHHHOrO Π0Τ0Κ3 (2), ΟΠΗΤΒ ΟΜ6ϋΙΗΒ3!ΟΤ C OCHOBHHMποτοκομ b adcopdepe (3) nepes nocnesHwu sjíeueHTOM adcopdepa(3/4). 237765First Cnocod pereHepauwH Tensa n skohoííhh oxnaBsaiomeiíbossi NPH atícopdpHK nerka adcopOnpyeMux rs30B hjih napoB jkhs-kogtbio, conpoBo ^ saioineMCH BHseneHHeM Tensa adcopdptín, NPH PE reHepaTHBHOM ηοπολβ30β3ημη no bo3uo; íihocth dojiBineft nacTtiTenna adcopdotHH, πρη πρημθηοηηη opoiuaeMHX adcopdepoB on τ -ji hqa ίο m η N Ch fact πιο oÓoramaeMMfl pasdaBseHHUÍipadBop I aesHT Ha SSA naCTHHHbix ποτοκθ, κοτορωθ napannesBHospyr Spyra npoxosHT nepe3 adcopdep 3h adcopdep πθοτηπηογοποτοκθ 2 odoramaacB πρη θτομ H3BecTHHM odpa3ou padonefó CPE-soll (6), h naciHnHtifi ποτοκ pacTBopa, BuxosnmHfi H3 adcopdepaqacTHHHoro ποτοκθ (2) êπητβ cuenoaioT c ockobhum ποτοκοιλ do-nee BbicoKoí KOHbteHTpauHH κ odinnf; ο ae κ OH ae ae pes pes pes pes pes pes pes pes pes pes pes pes pes pes pes pes pes pes j j ui ui ui ui ui ui ui ui ui ui ui ui ui ui ui ui ui. 2. Cnocod ποπ. ,Τiniqqqniqiffiorooroorooroθ oroΤorooroorooroorooroorooroorooroorooroorooroorooroorooroorooroorooroorooroorooroorooroorooroorooroorooroorooroΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤΟΤ 237765

AHHOTAUHHAHHOTAUHH

Cnocod pereHepauww Tenna η θκοηοιζο oxnarKAaiomeíiboah πρκ npopeccax odweHa BemecTB H3odpeTeHHe KacaeTca cnocoda peicynepapHíi Tenna πρκοΛΗΟΒρεωεΗΗΟι,ι coKpameHHH pacxoAa oxnasAatomeM boam πρκ adcopd-Phh ra3oodpa3Hoň padoneíř cpeAH b shskhx adcopdmioHHbix cpesaxπρκ BHaejieoH Tenna adcopdpo.Cnocod pereHepauww Tenna η θκοηοιζο oxnarKAaiomeíiboah πρκ npopeccax odweHa BemecTB H3odpeTeHHe KacaeTca cnocoda peicynepapHíi Tenna πρκοΛΗΟΒρεωεΗΗΟι, ι coKpameHHH pacxoAa oxnasAatomeM boam πρκ adcopd PhH ra3oodpa3Hoň padoneíř cpeAH b shskhx adcopdmioHHbix cpesaxπρκ BHaejieoH Tenna adcopdpo.

CymHOCTB Η30ύρβΤ6ΗΗΗ COCTOHT B TOM, HTO ΠΟΑΒΟΑΗΜΗβ pa3daBJíeHHHft pacTBop pa37iejiHfOT Ha ABa qacTHqHHx ποτοκη. 3th nac-THHHbie ποτοκη pasdaBneHHoro pacTBopa ποαβοαητοη k adcopdepy hnapannenBHO BKmoneHHOuy adcopdepy nacinnHoro ηοτοκβ h odora-lUaioTCH H3BecTHUM odpa3OM b odowx annapaTax padoneiř cpenoft.Bbixosfluwe H3 odowx adcopdepoB KOHireHTpHposaHHbie pacTBopuodjeahhhbtch h wcnonB3yioTCH b KanecTEe oxnaKAaiomeiř cpesu ahhadcopdepa naCTHWHoro ποτοκθ. Adeopdep oxnasAaeTCH η3βθοτηημodpa3OM oxnasAawfi boaoíí. OxnaKAenne adcopdepa n adcopdepa^βοτηηηογο noTOKa ocyuieCTBnfleTCH no npHHpuny προτιίΒοτοκθ.CymHOCTB Η30ύρβΤ6ΗΗΗ COCTOHT B TOM, HTO ΠΟΑΒΟΑΗΜΗβ pa3daBJiHHHft pacTBop pa37iejiHfOT Ha ABa qacTHqHHx ποτοκη. 3th nac-THHHbie ποτοκη pasdaBneHHoro pacTBopa ποαβοαητοη to adcopdepy hnapannenBHO BKmoneHHOuy adcopdepy nacinnHoro ηοτοκβ h odora-lUaioTCH H3BecTHUM odpa3OM b odowx annapaTax padoneiř cpenoft.Bbixosfluwe H3 odowx adcopdepoB KOHireHTpHposaHHbie pacTBopuodjeahhhbtch h wcnonB3yioTCH b KanecTEe oxnaKAaiomeiř CPEs ahhadcopdepa naCTHWHoro ποτοκθ. Adeopdep oxnasAaeTCH η3βθοτηημodpa3OM oxnasAawfi boaoíí. OxnaKAenne adcopdepa n adcopdepa ^ βοτηηηογο noTOKa ocyuieCTBnfleTCH no npHHpuny προτιίΒοτοκθ.

Il3odpeT0HKe mokst dtiTB npraeHeHO b adcopdííHOHHbix xono-AOBHblX 3'CTaHOBKaX.The method of the present invention relates to the use of HOHHbix xono-AOBHblX 3'CTaHOBKaX.

Aanee 03o<5peTeHne nose τ npHMeHHTLCfl b Apyrax pHpKynn-hhohhux npou,eccax απη npeodpa3OBaHHH Tenna (Hanpwuep, HacocucopdpHM Tenna), a τηκκθ b npou,eccax mipKynHUO snn nonyneHunBHepro H3 oTxoAHinero Tenna. Φηγ. I. 237765Aanee 03o <5peTeHne nose τ npHMeHHTLCfl b Apyrax pHpKynn-hhohhux npou, eccax απη npeodpa3OBaHHH Tenna (Hanpwuep, HacocucopdpHM Tenna), and τηκκθ b npou, eccax mipKynHUO snn nonyneHunBHepro H3 oTxoAHinero Tenna. Φηγ. I. 237765

Claims (2)

10 237765 PŘEDMĚT VYNÁLEZU t. Způsob regenerace tepla a ekonomie chladicí vody při abaorbci snadno absorbovatel-ných plynů nebo par kapalinou, provázené oddělením absorbčního tepla, při regeneračnímvyužití podle možnosti největší části absorbčního teple, při použití zavlažovaných ab-sorbentů, vyznačující se tím, že nasycovaný zředěný roztok 1 se dělí na dva dílčí proudy,které paralelně jeden k druhému procházejí absorbérem 3 a absorbér dílčího proudu 2, kterýje přitom známým způsobem obohacován pracovním prostředím (6), a dílčí proud roztoku,vycházející z absorbéru dílčího proudu (2) se znovu mísí se základním proudem vySSl kon-centrace a společný proud koncentrovaného roztoku (5) se potom přivádí do absorbéru dílčíhoproudu (2) jako chladicí prostředí, přičemž oba absorbéry (3, 2) pracují známým způsobem,v režimu zpětného proudu nebo v podobném režimu.BACKGROUND OF THE INVENTION t. A method for recovering heat and cooling water economics when absorbing readily absorbable gases or vapors through a liquid, accompanied by the dissipation of absorbent heat, in regenerative use as much of the heat absorbed as possible, using irrigated absorbents, characterized in that the saturated dilute solution 1 is divided into two partial streams which, in parallel, pass through the absorber 3 and the partial flow absorber 2, which in the known manner is enriched with the working environment (6), and the partial flow of the solution exiting the partial flow absorber (2) is again mixes the base stream with the higher concentration and the common stream of concentrated solution (5) is then fed to the partial flow absorber (2) as a cooling medium, both absorbers (3, 2) operating in a known manner, in reverse flow or similar mode . 2. Způsob podle bodu 1, vyznačující setím, že dílčí proud koncentrovaného roztoku,opouštějící absorbér dílčího proudu (2) se opět směSuje se základním proudem v absorbéru (3) před posledním prvkem absorbéru (3, 4). Uznáno vynálezem na. základě výsledků expertizy, provedené Úřadem pro vynálezectvía patentnictví, Berlín, DD. 2 výkresy2. A method according to claim 1, wherein the partial flow of the concentrated solution exiting the partial flow absorber (2) is again mixed with the base stream in the absorber (3) upstream of the last absorber element (3, 4). Recognized by the Invention. on the basis of the results of the expertise carried out by the Patent Inventory Office, Berlin, DD. 2 drawings
CS811826A 1980-04-08 1981-03-10 Method of heat regeneration and saving of cooling water in substances exchange processes CS237765B1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DD80220268A DD161077A3 (en) 1980-04-08 1980-04-08 METHOD FOR THE GRINDING OF CHEESE AND COOLING WATER SAVINGS IN STOCK EXCHANGE PROCESSES

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US8192530B2 (en) * 2007-12-13 2012-06-05 Alstom Technology Ltd System and method for regeneration of an absorbent solution

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US4198387A (en) * 1978-02-14 1980-04-15 Bethlehem Steel Corporation Maintaining the selective removal of H2 S from a variably flowing gas stream containing H2 S and CO2
FR2427117A1 (en) * 1978-06-01 1979-12-28 Mo I Khim Counterflow heat and mass exchange appts. - with gas flow split into several side streams contacting liquid flow

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