CN2918414Y - Autoclave for zinc diethyl - Google Patents
Autoclave for zinc diethyl Download PDFInfo
- Publication number
- CN2918414Y CN2918414Y CNU2006200914719U CN200620091471U CN2918414Y CN 2918414 Y CN2918414 Y CN 2918414Y CN U2006200914719 U CNU2006200914719 U CN U2006200914719U CN 200620091471 U CN200620091471 U CN 200620091471U CN 2918414 Y CN2918414 Y CN 2918414Y
- Authority
- CN
- China
- Prior art keywords
- ingress pipe
- reaction vessel
- kettle body
- reaction kettle
- zinc
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model belongs to a chemical processing equipment technology field, in particular to a reaction vessel for the diethyl zinc, comprising a reaction vessel body, a heater, a solution storage pot, a condenser, a product outlet valve, a blending machine and a flange. The reaction vessel body is provided with a hydrogen gas ingress pipe; the hydrogen gas ingress pipe is connected with the reaction vessel body in a threaded joint manner; the hydrogen gas ingress pipe is provided with a caulk; the size of the caulk is the same as that of the screw neck. The utility model has the advantages that the application of one reaction vessel enables both the activation and dryness of the zinc powder and the building-up reactions of the diethyl zinc, therefore, the cost is reduced and the efficiency is improved.
Description
Technical field
The utility model belongs to technical field of chemical, particularly a kind of reactor of zinc ethyl.
Background technology
At present, known Chemical Manufacture reaction unit generally comprises: reaction kettle body, stirring, heating muff and condenser etc.By to being connected of these basic elements of character, constitute the reaction unit of Chemical Manufacture.For organometallics, the building-up reactions of zinc ethyl particularly, general reaction kettle body can only satisfy feed intake and react in the carrying out of links such as stirring, heating, cooling, then have certain difficulty for the drying activation of zinc powder before the reaction, can not accomplish that a still is general.
Summary of the invention
Can not both finish the drying activation of the preceding zinc powder of reaction in order to overcome existing reaction unit, can carry out the weak point of normal zinc ethyl building-up reactions again, the purpose of this utility model provides a kind of reactor of zinc ethyl, this reactor can not only be finished general zinc ethyl building-up reactions, and can finish zinc powder is activated and drying treatment fully.
The technical scheme that its technical problem that solves the utility model adopts is: a kind of zinc ethyl reactor, form by reaction kettle body 2, well heater 3, container for storing liquid 4, condenser 5, products export valve 6, agitator 7 and flange 8, reaction kettle body 2 is provided with hydrogen ingress pipe 1, between hydrogen ingress pipe 1 and the reaction kettle body 2 by being threaded, be connected with plug 9 on the hydrogen ingress pipe 1, plug 9 is measure-alike with the screw thread mouth of hydrogen ingress pipe 1.Hydrogen ingress pipe 1 is actually to be threaded in reactor one side utilization and does one and extend along reaction kettle body 2 inwalls and to answer the kettle bottom insert canal at 2 ends, feed exsiccant hydrogen by the bottom insert canal external tapping, can before reaction, carry out abundant effective dry and activation treatment zinc powder.Activation can be taken out bottom insert canal after finishing very easily, and with screw plug plug 9 capping stills, carries out normal zinc ethyl building-up reactions, thereby realizes that a still is general, and reduces the complicacy of operation.
The beneficial effects of the utility model are, can both realize the activation and the drying of zinc powder with a reactor, carry out the building-up reactions of zinc ethyl again, reduce cost and raise the efficiency.
Description of drawings
Below in conjunction with drawings and Examples the utility model is further specified.
Fig. 1 is a structural representation of the present utility model.
Among the figure 1, hydrogen ingress pipe, 2, reaction kettle body, 3, well heater, 4, container for storing liquid, 5, condenser, 6, the products export valve, 7, agitator, 8, flange, 9, plug.
Embodiment
As shown in the figure, reaction kettle body 2 is provided with hydrogen ingress pipe 1, by being threaded, is connected with plug 9 on the hydrogen ingress pipe 1 between hydrogen ingress pipe 1 and the reaction kettle body 2, and plug 9 is measure-alike with the screw thread mouth of hydrogen ingress pipe 1.By hydrogen ingress pipe 1 dry hydrogen is fed in the reaction kettle body 2, well heater 3 corresponding kettlies 2 heat, thereby reach the purpose of zinc powder in the dry activation still.Container for storing liquid 4, condenser 5 are the necessary component of carrying out the zinc ethyl building-up reactions, and reaction is collected by the zinc ethyl product that 6 pairs of distillations of products export valve obtain after finishing.Agitator 7 controls are to the stirring of material, and flange 8 is solid materials charging openings.Hydrogen ingress pipe 1 and reaction kettle body 2 closely are connected by screw thread, and plug 9 can finish in the zinc powder activation, be used for the shutoff screw thread mouth after hydrogen ingress pipe 1 unloads.
Claims (2)
1, a kind of zinc ethyl reactor, form by reaction kettle body (2), well heater (3), container for storing liquid (4), condenser (5), products export valve (6), agitator (7) and flange (8), it is characterized in that, reaction kettle body (2) is provided with hydrogen ingress pipe (1), by being threaded, be connected with plug (9) on the hydrogen ingress pipe (1) between hydrogen ingress pipe (1) and the reaction kettle body (2).
2, a kind of zinc ethyl reactor according to claim 1 is characterized in that, described plug (9) is measure-alike with the screw thread mouth of hydrogen ingress pipe (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2006200914719U CN2918414Y (en) | 2006-06-06 | 2006-06-06 | Autoclave for zinc diethyl |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2006200914719U CN2918414Y (en) | 2006-06-06 | 2006-06-06 | Autoclave for zinc diethyl |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2918414Y true CN2918414Y (en) | 2007-07-04 |
Family
ID=38216228
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNU2006200914719U Expired - Fee Related CN2918414Y (en) | 2006-06-06 | 2006-06-06 | Autoclave for zinc diethyl |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2918414Y (en) |
-
2006
- 2006-06-06 CN CNU2006200914719U patent/CN2918414Y/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: KELIDE CHEMICAL TECH DEVELOPMENT CO., LTD., DALIAN Free format text: FORMER OWNER: JINGYUAN ELECTRONIC GASEOUS RESEARCH CENTER CO., LTD., DALIAN Effective date: 20111213 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20111213 Address after: 116600 storage processing zone IE-33, Dalian Free Trade Zone, Liaoning Patentee after: Dalian Free Trade Zone Credit Chemical Technology Development Co., Ltd. Address before: 116600 storage processing zone IE-33, Dalian Free Trade Zone, Dalian, Liaoning Patentee before: Jingyuan Electronic Gaseous Research Center Co., Ltd., Dalian |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20070704 Termination date: 20150606 |
|
| EXPY | Termination of patent right or utility model |