CN2889552Y - Continuous preparation device for big block amorphous alloy - Google Patents
Continuous preparation device for big block amorphous alloy Download PDFInfo
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- CN2889552Y CN2889552Y CN 200620081264 CN200620081264U CN2889552Y CN 2889552 Y CN2889552 Y CN 2889552Y CN 200620081264 CN200620081264 CN 200620081264 CN 200620081264 U CN200620081264 U CN 200620081264U CN 2889552 Y CN2889552 Y CN 2889552Y
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- crucible
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- amorphous
- water conservancy
- conservancy diversion
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Abstract
The utility model provides a continuous production device of blocky amorphous alloy. The device includes a traction device, an amorphous dummy bar, a cooling device, a casting mould, a crucible, a pressing block, a servomotor, a feeding mechanism, several heaters, a vacuum container, a guiding/standing container; the casting mould, the crucible, the guiding/standing container, and the independent heaters are all arranged in the vacuum container, two ends of the guiding/standing container are respectively hermetically connected with the crucible and the casting mould, the amorphous dummy bar hermetically penetrates the vacuum container and enters to the casting mould, the feeding mechanism driven by the servomotor penetrates the vacuum container and has its bottom connected with the pressing block. The working process comprises allowing the amorphous dummy bar to hermetically penetrate the vacuum container and enter into mould, evacuating the vacuum container, starting the electrical heating system to melt alloy into liquid in the crucible, maintaining temperature of the liquid and standing in the guiding/standing container, filling the casting mould with the alloy liquid, cooling and solidifying in cooling device to obtain amorphous structure, and starting traction device to produce amorphous rod continuously.
Description
Affiliated technical field
The utility model provides a kind of continuous preparation device of bulk amorphous alloys, belongs to metallurgy, material forming and preparing technical field.
Background technology
Compare with common polycrystalline metal material, amorphous alloy (being called glassy metal again) has high strength, high rigidity, high elastic limit, excellent properties such as corrosion-resistant, wear-resistant.Enter twentieth century nineties, people find that in succession some palladiums, zirconium, lanthanum alloy are 10
7Cooling can form glassy metal under the speed of K/ second-time.Adopt common foundry engieering just can obtain the glassy metal block materials, encouraging prospects have been showed in the application of glassy metal.In in the past 10 years, the research of block metal glass has caused numerous scientists' interest in the world, and new achievement in research is not emerged in large numbers absolutely.Developing low cost, being easy to cast the novel alloy that becomes the blocks of large material is target of greatest concern all the time, also is the key that has the final practicability intellectual property of material simultaneously.
1991, Akihisa Inoue seminar of northeastern Japan university adopted 4 millimeters " magnesium-copper-yttrium " ternary alloy three-partalloy glass of copper mold casting forming diameter pole.June nineteen ninety-five, the Korea S scientist prepared the magnesium alloy glass that diameter reaches 14 millimeters (see J.Mater.Res.vol.20,2005, p.1465).The fracture strength of magnesium-base metal glass can reach the 800-900 MPa, is 2 ~ 3 times of common commercial magnesium alloy.Metal research Shenyang material science country (associating) of Chinese Academy of Sciences laboratory development goes out magnesium alloy Mg
54Cu
26.5Ag
8.5Gd
11Copper mould casting obtains the amorphous alloy pole of diameter 25mm, magnesium alloy Mg
54Cu
26.5Ag
8.5Gd
11The glassy metal pole diameter of copper mold casting can reach 25 millimeters, and about 1000 MPas of fracture strength (" Applied Physics wall bulletin ", AIP sponsors, publish October 31 nineteen ninety-five).Zr
55Al
10Ni
5Cu
30The critical non-crystaline amorphous metal size that alloy obtains can reach diameter 30mm (Mater.Trans.JlM, 1996 (37), P181).At present, the amorphous alloy of the relative low price that some glass forming abilities are very strong is seen in report in succession.For example zirconium base, the critical amorphous size of magnesium base alloy can reach more than the 10mm, and critical cooling rate has been reduced to 10~100K/s.
The main method of laboratory bulk amorphous alloy preparation has: die cast, wedge-shaped die casting, negative pressure casting (suction pouring), casting forming, shrend, directional solidification, jet are shaped or the like.
The preparation of disclosed bulk amorphous alloys has in patented technology at present: granted patent CN99250780.4 has introduced vacuum pressure casting bulk amorphous alloys device, utilizes gas pressure that the alloy of fusing is cast at a high speed in the copper film, forms bulk amorphous alloys; Granted patent CN02111709.8 has introduced and has utilized cyclone that the zirconium-base alloy of fusing is separated into fine drop, and the droplets fall process is at first pre-cooled by inert gas, enters in the condenser (casting mold) that is forced to cool off again and finishes the preparation method of solidifying; Patent CN03121418.5 has introduced and has utilized gas pressure to spray and negative pressure of vacuum suction casting measure, the alloy that melts is injected water cooled copper mould at a high speed obtain non-crystal method and apparatus; The method that patent CN03128762.X introduces is, alloy liquid is poured into form in the slit of a water-cooled roll noncrystal.
The common ground of these technology is, alloy liquid is cooled and solidified in casting mold (copper mold, roll etc.), and alloy liquid contacts closely with the casting mold wall.According to classical liquid alloy crystallization theory, it is the process that a nucleus forms, grows up that liquid alloy is solidified as crystal, and the wall of cooling casting mold can promote the formation of nucleus well and grow up, and is unfavorable for that alloy transforms to amorphous.Secondly, be seen in the reported method, except the method that patent CN03121418.5 introduces, the size of non-crystaline amorphous metal is subjected to the limitation of casting mold three-dimensional dimension.
The utility model content
The purpose of this utility model provides a kind of continuous preparation method and device that can overcome above-mentioned defective, bulk amorphous alloys that efficient is high, and its technical scheme is:
A kind of continuous preparation device of bulk amorphous alloys, comprise draw-gear, the amorphous dummy bar, cooling device, casting mold, crucible, briquetting, servomotor, feed mechanism and some heaters, it is characterized in that: set up vacuum tank and water conservancy diversion and leave standstill container, casting mold wherein, crucible and water conservancy diversion and leave standstill container and separately independently heater all be arranged in the vacuum tank, water conservancy diversion and the two ends of leaving standstill container be tightly connected respectively crucible and casting mold, amorphous dummy bar hermetically passing vacuum tank is inserted casting mold, by the feed mechanism hermetically passing vacuum tank of driven by servomotor, its bottom is connected with briquetting.
The continuous preparation device of described bulk amorphous alloys, water conservancy diversion and the cross section that leaves standstill container are 2~100 times of casting mold cross section.
The continuous preparation device of described bulk amorphous alloys, crucible, water conservancy diversion and leave standstill container and casting mold all adopts high purity graphite to make.
The continuous preparation device of described bulk amorphous alloys is provided with a plurality of casting molds in the vacuum tank, respectively with water conservancy diversion with leave standstill seal of vessel and be connected; Perhaps be provided with a plurality of water conservancy diversion in the vacuum tank and leave standstill container, be tightly connected with crucible respectively.
Its operation principle is: earlier amorphous dummy bar hermetically passing vacuum tank is inserted casting mold, then to evacuating atmosphere in vacuum vessel, restart electric heating system alloy is molten into liquid state in crucible, alloy liquid is introduced into water conservancy diversion and leaves standstill in the container under the briquetting extruding and is incubated, leaves standstill, promptly be full of casting mold, start cooling device alloy liquid and be solidified as amorphous structure, start draw-gear, liquid alloy continuously becomes non-crystalline style.
The utility model compared with prior art, have following advantage: 1, liquid alloy does not solidify in casting mold, help alloy to noncrystal transformation, the injection chilling action of dependence cooling medium changes into solid-state noncrystal, obtains the bar-shaped noncrystal of lengthwise dimension very big (in theory can be infinitely great); 2, water conservancy diversion and leave standstill the setting of container, the introducing of computer controlled automatic device has improved the success rate and the quantity-produced ability of dummy ingot operation.
Description of drawings
Fig. 1 is the structural representation of the utility model embodiment.
The specific embodiment
1, valve 2, draw-gear 3, amorphous dummy bar 4, vacuum tank 5, cooling device 6, casting mold 7, heater 8, water conservancy diversion and leave standstill container 9, alloy liquid 10, computer controlled automatic device 11, crucible 12, briquetting 13, feed mechanism 14, servomotor
In the embodiment shown in fig. 1: alloy adopts magnesium base alloy Mg
65Cu
20Zn
5Y
10Casting mold 6, crucible 11 and water conservancy diversion and leave standstill container 8 and all adopt high purity graphite to make, together be arranged in the vacuum tank 4 with cooling device 5, and each have the heater 7 that is subjected to 10 controls of computer controlled automatic device, water conservancy diversion and the two ends of leaving standstill container 8 be tightly connected respectively crucible 11 and casting mold 6, wherein water conservancy diversion and the cross section that leaves standstill container 8 are 10 times of casting mold 6 cross sections, amorphous dummy bar 3 hermetically passing vacuum tanks 4 are inserted casting mold 6, feed mechanism 13 hermetically passing vacuum tanks 4 by servomotor 14 drivings, its bottom is connected with briquetting 12, and the side ancient piece of jade, round, flat and with a hole in its centre of vacuum tank 4 is provided with the valve 1 that connects vacuum extractor or aerating device.
Adopt the utility model, can prepare the complete amorphous pole of diameter 5mm, length 10000mm.
For enhancing productivity, be provided with a plurality of casting molds 6 in the vacuum tank 4, respectively with water conservancy diversion with leave standstill container 8 and be tightly connected, perhaps be provided with a plurality of water conservancy diversion in the vacuum tank 4 and leave standstill container 8, be tightly connected with crucible 11 respectively, computer controlled automatic device 10 can be controlled and coordinate draw-gear 3, servomotor 14, cooling device 5 and a plurality of heater 7, in order to improve the success rate of dummy ingot operation, guarantees to produce continuously.
As required, cooling device 5 also can be arranged on outside the vacuum tank 4.
Claims (5)
1, a kind of continuous preparation device of bulk amorphous alloys, comprise draw-gear (2), amorphous dummy bar (3), cooling device (5), casting mold (6), crucible (11), briquetting (12), servomotor (14), feed mechanism (13) and some heaters (7), it is characterized in that: set up vacuum tank (4) and water conservancy diversion and leave standstill container (8), casting mold (6) wherein, crucible (11) and water conservancy diversion and leave standstill container (8) and all be arranged in the vacuum tank (4), and each have independently heater (7), water conservancy diversion and the two ends of leaving standstill container (8) be tightly connected respectively crucible (11) and casting mold (6), amorphous dummy bar (3) hermetically passing vacuum tank (4) is inserted casting mold (6), by feed mechanism (13) the hermetically passing vacuum tank (4) that servomotor (14) drives, its bottom is connected with briquetting (12).
2, the continuous preparation device of bulk amorphous alloys as claimed in claim 1 is characterized in that: water conservancy diversion and the cross section that leaves standstill container (8) are 2~100 times of casting mold (6) cross section.
3, the continuous preparation device of bulk amorphous alloys as claimed in claim 1 is characterized in that: crucible (11), water conservancy diversion and leave standstill container (8) and casting mold (6) all adopts high purity graphite to make.
4, the continuous preparation device of bulk amorphous alloys as claimed in claim 1 is characterized in that: be provided with a plurality of casting molds (6) in the vacuum tank (4), respectively with water conservancy diversion with leave standstill container (8) and be tightly connected.
5, the continuous preparation device of bulk amorphous alloys as claimed in claim 1 is characterized in that: be provided with a plurality of water conservancy diversion in the vacuum tank (4) and leave standstill container (8), be tightly connected with crucible (11) respectively.
Priority Applications (1)
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CN 200620081264 CN2889552Y (en) | 2006-02-24 | 2006-02-24 | Continuous preparation device for big block amorphous alloy |
Applications Claiming Priority (1)
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CN 200620081264 CN2889552Y (en) | 2006-02-24 | 2006-02-24 | Continuous preparation device for big block amorphous alloy |
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CN2889552Y true CN2889552Y (en) | 2007-04-18 |
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CN 200620081264 Expired - Fee Related CN2889552Y (en) | 2006-02-24 | 2006-02-24 | Continuous preparation device for big block amorphous alloy |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102641999A (en) * | 2012-04-24 | 2012-08-22 | 王东 | Device and method for continuously preparing bulk amorphous alloy ingots |
CN107496050A (en) * | 2017-07-10 | 2017-12-22 | 许昌锦荣食品有限公司 | A kind of non-crystaline amorphous metal intravascular stent manufacturing equipment |
-
2006
- 2006-02-24 CN CN 200620081264 patent/CN2889552Y/en not_active Expired - Fee Related
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102641999A (en) * | 2012-04-24 | 2012-08-22 | 王东 | Device and method for continuously preparing bulk amorphous alloy ingots |
CN107496050A (en) * | 2017-07-10 | 2017-12-22 | 许昌锦荣食品有限公司 | A kind of non-crystaline amorphous metal intravascular stent manufacturing equipment |
CN107496050B (en) * | 2017-07-10 | 2019-08-20 | 孟庆燕 | A kind of amorphous alloy intravascular stent manufacturing equipment |
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Legal Events
Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C17 | Cessation of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20070418 Termination date: 20100224 |