CN2848878Y - Electrochemical electrolysis device - Google Patents

Electrochemical electrolysis device Download PDF

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Publication number
CN2848878Y
CN2848878Y CN 200520040819 CN200520040819U CN2848878Y CN 2848878 Y CN2848878 Y CN 2848878Y CN 200520040819 CN200520040819 CN 200520040819 CN 200520040819 U CN200520040819 U CN 200520040819U CN 2848878 Y CN2848878 Y CN 2848878Y
Authority
CN
China
Prior art keywords
reaction
cavity
base
electrolysis device
electrochemical electrolysis
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 200520040819
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Chinese (zh)
Inventor
樊春海
武海萍
周波
徐慧
宋世平
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Institute of Applied Physics of CAS
Original Assignee
Shanghai Institute of Applied Physics of CAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Institute of Applied Physics of CAS filed Critical Shanghai Institute of Applied Physics of CAS
Priority to CN 200520040819 priority Critical patent/CN2848878Y/en
Application granted granted Critical
Publication of CN2848878Y publication Critical patent/CN2848878Y/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model discloses an electrochemical electrolysis device capable of being magnetically controlled, which comprises a reacting device capable of containing working electrodes and also comprises a magnetic device acting on the working electrodes. The utility model can be used for magnetic-control electrochemical electrolysis, and the working electrodes are arranged beneath reaction cavities so as to be favorable to the collection of magnetic particles; the electrochemical electrolysis device comprises two reaction cavities, wherein a small reacting cavity is used for determining the reaction surfaces of the working electrodes so as to enhance the deposition efficiency of the magnetic particles and a large reaction cavity is favorable to carrying out electrochemical experiments needing more solutions after the magnetic particles are deposited.

Description

The electrochemical electrolysis device
Technical field
But the utility model relates to a kind of electrochemical electrolysis device of magnetic regulation and control.
Background technology
Common electrochemical cell is simple glass beaker, weighing bottle, glass or the Teflon cup-like container (as U.S. CH company, BAS company) that contains lid, and reaction volume is bigger, is not suitable for carrying out magnetic operator.Existing novel thin layer electrochemical cell is suitable for carrying out the electrochemical reaction (as CH company) of smaller size smaller (a few hectolambda), but is difficult to the magnetic particle location is deposited on the working electrode.
Summary of the invention
The purpose of this utility model provides a kind of electrochemical electrolysis device that can be used for the magnetic control electrochemical electrolysis.
The purpose of this utility model is achieved through the following technical solutions:
A kind of electrochemical electrolysis device comprises a reaction unit that can hold working electrode, also comprises a magnetic means that acts on this working electrode.
Wherein, this reaction unit comprises: a reaction cavity, and its inside is provided with at least one reaction chamber; A top cover that is located at this reaction cavity top, its top is provided with two electrode holes that are used for connection electrode, and respectively this electrode hole all communicates with this reaction chamber; A base that is located at this reaction cavity bottom, which is provided with one communicate with this reaction chamber base cavity pocket; A stick harness that links to each other with this base.
Wherein, this reaction cavity inside is provided with one first reaction chamber and second reaction chamber that communicates with this first reaction chamber, this reaction cavity bottom also is provided with a cavity sealing pit that is used to place sealing-ring, and the bottom of this reaction cavity also is provided with a groove that is used for extraction electrode.
Wherein, the top of this top cover also is provided with an air inlet port and a production well, and the bottom of this top cover is provided with a top cover pit, and the top of this reaction cavity is provided with a cavity projection with matching.
Wherein, the top of this base is provided with a base sealing pit that is used to install sealing-ring that communicates with this base cavity pocket, is provided with a pit that is connected that has internal thread that communicates with this base cavity pocket in the bottom of this base.
Wherein, this stick harness inside also is provided with a stick harness chamber, and the bottom in this stick harness chamber is provided with a through hole.
Wherein, this stick harness is provided with the outside screw that the internal thread that is connected pit with this matches.
Wherein, this reaction cavity is provided with a plurality of reaction cavity connecting holes, and this base is provided with and the corresponding base screw of this reaction cavity connecting hole.
Wherein, this magnetic means is a bar-shaped magnet that is arranged in this stick harness chamber.
This electrochemical electrolysis device also comprises a support that is set on this stick harness.
Positive progressive effect of the present utility model is: can be used in the magnetic control electrochemical electrolysis; Working electrode is arranged on reaction chamber and gets the below, helps the enrichment of magnetic particle; Comprise two reaction chambers, little reaction chamber is determined the reaction surface of working electrode, thereby has improved the adsorption efficiency of magnetic particle; Big reaction chamber needing to help the electrochemistry experiment of more solution.
Description of drawings
Fig. 1 is the decomposing schematic representation of analysing and observe of the utility model one embodiment.
Fig. 2 is the schematic top plan view of top cover among the utility model one embodiment.
Fig. 3 is the schematic top plan view of reaction cavity among the utility model one embodiment.
Fig. 4 is the elevational schematic view of reaction cavity among the utility model one embodiment.
Fig. 5 is the schematic top plan view of base among the utility model one embodiment.
Embodiment
Provide the utility model preferred embodiment below in conjunction with accompanying drawing, to describe the technical solution of the utility model in detail.
As shown in Figure 1, a kind of electrochemical electrolysis device comprises a reaction unit 1, wherein is provided with working electrode 2, and this electrochemical electrolysis device also comprises a magnetic means 3 that acts on this reaction electrode 2.
This reaction unit 1 comprises a top cover 11, reaction cavity 12, a base 13 and a stick harness 14.
The inside of this reaction cavity 12 is provided with first a bigger reaction chamber 121 and second a less reaction chamber 122 that communicates with it, be provided with a cavity sealing pit 123 that is used to lay first sealing-ring 4 in these reaction cavity 12 bottoms, this second reaction cavity 122 communicates with this cavity sealing pit 123.As shown in Figure 4, the bottom of this reaction cavity 12 is provided with a groove 124, is used to draw the wiring of this working electrode 2.The top of this reaction cavity 12 also is provided with one and is used for the cavity projection 125 that links to each other with this top cover 11.As Fig. 3, also be provided with four cavity connecting holes 126 on this reaction cavity 12, be used for being fixedly linked with this base 13.This second reaction chamber 122 is used to adsorb magnetic particle, can improve the adsorption efficiency of magnetic particle, adds electrolytic solution in this first reaction chamber 121, can be engaged in electrochemistry experiment.
As Fig. 2, the top of this top cover 11 is provided with two electrode holes 111, is respectively applied for reference electrode and supporting electrode are installed, and an air inlet port 112 and a production well 113 also can be set.These two electrode holes 111, this air inlet port 112 and this production well 113 all communicate with this first reaction chamber 121.This air inlet port 112 is used to connect the nitrogen needle tubing, is used for to discharge the air in the reaction chamber, avoiding airborne impurity that reaction is exerted an influence to reaction cavity 12 logical nitrogen, and air is discharged from this production well 113.The bottom of this top cover 11 is provided with a top cover pit 114 that matches with this cavity projection 125.
These base 13 inside are provided with a base cavity pocket 131, it communicates with this second reaction chamber 122, the top of this base 13 is provided with a base sealing pit 132 that is used to install second sealing-ring 5 that communicates with this base cavity pocket 131, be provided with in the bottom of this base 13 one with this base cavity pocket 131 communicate have an internal thread be connected pit 133.As Fig. 5, also be provided with on this base 13 four respectively with these cavity connecting hole 126 corresponding base screws 134 respectively.
These stick harness 14 inside are provided with a stick harness chamber 141, and the bottom in this stick harness chamber 141 is provided with a through hole 142.This stick harness 14 is provided with the outside screw that the internal thread that is connected pit 133 with this matches.
This magnetic means 3 is the existing bar-shaped magnets in the stick harness chamber that is arranged on this stick harness 14 141.
This electrochemical electrolysis device also comprises a support 6 that is set on this stick harness 14.

Claims (10)

1, a kind of electrochemical electrolysis device comprises a reaction unit that can hold working electrode, it is characterized in that, it also comprises a magnetic means that acts on this working electrode.
2, electrochemical electrolysis device according to claim 1 is characterized in that, this reaction unit comprises: a reaction cavity, and its inside is provided with at least one reaction chamber; A top cover that is located at this reaction cavity top, its top is provided with two electrode holes that are used for connection electrode, and respectively this electrode hole all communicates with this reaction chamber; A base that is located at this reaction cavity bottom, which is provided with one communicate with this reaction chamber base cavity pocket; A stick harness that links to each other with this base.
3, electrochemical electrolysis device according to claim 2, it is characterized in that, this reaction cavity inside is provided with one first reaction chamber and second reaction chamber that communicates with this first reaction chamber, this reaction cavity bottom also is provided with a cavity sealing pit that is used to place sealing-ring, and the bottom of this reaction cavity also is provided with a groove that is used for extraction electrode.
4, electrochemical electrolysis device according to claim 3, it is characterized in that, the top of this top cover also is provided with an air inlet port and a production well, and the bottom of this top cover is provided with a top cover pit, and the top of this reaction cavity is provided with a cavity projection with matching.
5, electrochemical electrolysis device according to claim 4, it is characterized in that, the top of this base is provided with a base sealing pit that is used to install sealing-ring that communicates with this base cavity pocket, is provided with a pit that is connected that has internal thread that communicates with this base cavity pocket in the bottom of this base.
6, electrochemical electrolysis device according to claim 5 is characterized in that, this stick harness inside also is provided with a stick harness chamber, and the bottom in this stick harness chamber is provided with a through hole.
7, electrochemical electrolysis device according to claim 6 is characterized in that, this stick harness is provided with the outside screw that the internal thread that is connected pit with this matches.
8, electrochemical electrolysis device according to claim 7 is characterized in that, this reaction cavity is provided with a plurality of reaction cavity connecting holes, and this base is provided with and the corresponding base screw of this reaction cavity connecting hole.
9, electrochemical electrolysis device according to claim 8 is characterized in that, this magnetic means is a bar-shaped magnet that is arranged in this stick harness chamber.
10, electrochemical electrolysis device according to claim 9 is characterized in that, it also comprises a support that is set on this stick harness.
CN 200520040819 2005-04-13 2005-04-13 Electrochemical electrolysis device Expired - Fee Related CN2848878Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 200520040819 CN2848878Y (en) 2005-04-13 2005-04-13 Electrochemical electrolysis device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 200520040819 CN2848878Y (en) 2005-04-13 2005-04-13 Electrochemical electrolysis device

Publications (1)

Publication Number Publication Date
CN2848878Y true CN2848878Y (en) 2006-12-20

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN 200520040819 Expired - Fee Related CN2848878Y (en) 2005-04-13 2005-04-13 Electrochemical electrolysis device

Country Status (1)

Country Link
CN (1) CN2848878Y (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102101205A (en) * 2009-12-21 2011-06-22 财团法人金属工业研究发展中心 Electrochemical processing device, processing method and electrode unit thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102101205A (en) * 2009-12-21 2011-06-22 财团法人金属工业研究发展中心 Electrochemical processing device, processing method and electrode unit thereof
CN102101205B (en) * 2009-12-21 2013-11-06 财团法人金属工业研究发展中心 Electrochemical processing device, processing method and electrode unit thereof

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C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20061220