CN2794624Y - High efficiency reactor for high viscosity material solid liquid heterogeneous reaction - Google Patents
High efficiency reactor for high viscosity material solid liquid heterogeneous reaction Download PDFInfo
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- CN2794624Y CN2794624Y CN 200520006044 CN200520006044U CN2794624Y CN 2794624 Y CN2794624 Y CN 2794624Y CN 200520006044 CN200520006044 CN 200520006044 CN 200520006044 U CN200520006044 U CN 200520006044U CN 2794624 Y CN2794624 Y CN 2794624Y
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Abstract
The utility model discloses a high efficiency reactor for high viscosity material solid liquid heterogeneous reaction. The utility model comprises a frame type stirrer (16) and a kettle body (18), wherein the frame type stirrer (16) is positioned at the upper part of the kettle body (18), and a frame type stirring paddle (15) is connected with an A motor (1) through a speed reducer (2). The utility model is characterized in that the bottom of the kettle body (18) is provided with a high shear stirring reactor (17), and a stator (9) of the high shear stirring reactor (17) is fixed on the kettle body (18) by a fixed frame (12). A plurality of holes are arranged at the top of the stator (9) and on the circumference of a side edge, and a rotating disk (8) of the high shear stirring reactor (17) is connected with a B motor (11). A gap is arranged between the rotating disk (8) and the stator (9) of the high shear stirring reactor (17). When the high viscosity material solid liquid heterogeneous reaction is carried out, the utility model can make heterogeneous reaction materials mixed evenly, the contact surfaces among reactant particles are increased and reaction time is shortened.
Description
Technical field
The utility model relates to a kind of reactor, relates in particular to a kind of high-viscosity material high efficiency reactor.
Background technology
High-viscosity material solid-liquid heterogeneous reaction is meant that reactant is one or more solids and one or more liquid, reacts under heterogeneous conditions, and reaction product is a high-viscosity material.When finishing this type of reaction, be high-viscosity material, hindered the further reaction of liquid phase reactor thing and solid-phase reactant, reaction is carried out slowly, thereby conversion ratio is not high because liquid phase contacts the product that generates with solid phase.Conventional at present reactor can't solve the problem that above-mentioned reaction exists, thereby be unfavorable for realizing large-scale industrial production as having the conventional electric heating reacting kettle of anchor agitator.
The utility model content
The purpose of this utility model be to overcome above-mentioned shortcoming and provide a kind of when carrying out high-viscosity material solid-liquid heterogeneous reaction, can promote that heterogeneous reaction mass mixes, increase contact-making surface between the reactant particle, shorten the high-viscosity material solid-liquid heterogeneous reaction high efficiency reactor in reaction time.
The purpose of this utility model and solve its technical problem underlying and realize by the following technical solutions: according to the high-viscosity material solid-liquid heterogeneous reaction high efficiency reactor that the utility model proposes, comprise gate stirrer, kettle, the housing of kettle is a chuck, charging aperture is positioned at the case top of kettle, discharging opening is positioned at the housing bottom of kettle, steam-gas inlet is positioned at the lower housing portion of kettle, and the condensation mouth of pipe is positioned at the case top of kettle; Gate stirrer is positioned at kettle top, its frame type agitating blade links to each other with motor by reductor, wherein autoclave body bottom is provided with the high shear stirred reactor, the stator of high shear stirred reactor is fixed on the kettle with fixed mount, have some holes on stator top and the side circumference, the rotating disk of high shear stirred reactor links to each other with motor, between rotating disk and the stator slit is arranged.
The purpose of this utility model and solve its technical problem and can also adopt following technical measures further to realize.
Big outer little bellmouth had the little bellmouth of outer imperial palace in the stator top of described high shear stirred reactor had on the stator side circumference.
The stirring piece that four symmetries are arranged on the rotating disk card of described high shear stirred reactor.
The scraping blade that the useful fixed clamping bar in described frame type agitating blade end is fixing.
Described frame type agitating blade is the Y type.
The utility model compared with prior art has tangible advantage and beneficial effect.By above technical scheme as can be known, after reaction mass dropped into the utility model, start gate stirrer and high shear stirred reactor, the rotating disk of high shear stirred reactor rotates at a high speed, produces huge suction the bellmouth of solid-liquid two phase materials from the stator top sucked, and fierce collision takes place in stator, allow solid-liquid fully contact mutually, reaction is carried out fast, and then sprayed, further add fast response from the bellmouth of stator side; Gate stirrer scrapes mixing to the high-viscosity material of reaction generation and the solid-liquid phase materials of adhesion thereof from the kettle edge, and then sucks the high shear stirred reactor, allows reaction carry out more thoroughly.Thereby have and promote heterogeneous reaction mass to mix, increase the reactant particle indirectly touching hit probability, shorten the characteristics in reaction time.
The specific embodiment of the present utility model is provided in detail by following examples and accompanying drawing thereof.
Description of drawings
Fig. 1 is a structural representation of the present utility model;
Fig. 2 is the A-A cutaway view of Fig. 1;
Fig. 3 is the B-B schematic diagram of the high shear stirred reactor among Fig. 1;
Fig. 4 is the vertical view of high shear stirred reactor of the present utility model;
Fig. 5 is the C-C cutaway view of Fig. 4;
Mark among the figure:
1, A motor; 2, reductor; 3, charging aperture; 4, the condensation mouth of pipe; 5, vapor outlet port; 6, fixed clamping bar; 7, scraping blade; 8, rotating disk; 9, stator; 10, discharging opening; 11, B motor; 12, fixed mount; 13, steam-gas inlet; 14, chuck; 15, frame stirring arm; 16, gate stirrer; 17, high shear stirred reactor; 18, kettle; 19, stir piece; 20, A bellmouth; The 21:B bellmouth.
The specific embodiment
Below in conjunction with accompanying drawing and preferred embodiment, to according to the high-viscosity material solid-liquid heterogeneous reaction that the utility model proposes with the high efficiency reactor specific embodiment, structure, feature and effect thereof, describe in detail as after.
Referring to Fig. 1-5, high-viscosity material solid-liquid heterogeneous reaction high efficiency reactor, form by gate stirrer 16, high shear stirred reactor 17, kettle 18, the housing of kettle 18 is a chuck 14, charging aperture 3 is positioned at the case top of kettle 18, discharging opening 10 is positioned at the housing bottom of kettle 18, and steam-gas inlet 13 is positioned at the lower housing portion of kettle 18, and the condensation mouth of pipe 4 is positioned at the case top of kettle 18;
Gate stirrer 16 is positioned at kettle 18 tops, and its frame type agitating blade 15 links to each other with A motor 1 by reductor 2, the silicon rubber scraping blade 7 that the useful fixed clamping bar 6 in frame type agitating blade 15 ends is fixed, and frame type agitating blade 15 is the Y type;
Kettle 18 bottoms are provided with high shear stirred reactor 17, the stator 9 usefulness fixed mounts 12 of high shear stirred reactor 17 are fixed on the kettle 18, the rotating disk 8 of high shear stirred reactor 17 links to each other with B motor 11, the slit is 1.5mm between rotating disk 8 and the stator 9, and the stirring piece 19 of four symmetries is arranged on rotating disk 8 cards.Big outer little A bellmouth 20 in stator 9 tops have, the aperture is: interior 3.5mm, outer 2.0mm has the little B bellmouth 21 of outer imperial palace on the stator 9 side circumference, and the aperture is: interior 2.0mm, outer 3.5mm.
Make use-case: produce the humic acid sodium salt with high efficiency reactor with high-viscosity material solid-liquid heterogeneous reaction of the present utility model:
Primary raw material and inventory
Name of an article inventory (kg)
Weathered coal (, containing humic acid 67.52%) 100 in butt
30% NaOH 40
NPE 0.2
Water 200
Water and NPE are added in the foregoing description, be warming up to 60 ℃, start stirring, adding is crushed to 80～100 purpose weathered coals, stirs 15min; Add 30% sodium hydroxide solution, be controlled in the 10min and add, keep 60～65 ℃ of reactions of temperature 30min, stop reaction, discharging, drying is crushed to 100 orders, measures wherein that solubility humic acid content is 65.16%, and conversion ratio reaches 96.5%.
Comparative example: produce the humic acid sodium salt with conventional electric heating reacting kettle
Primary raw material and inventory
Name of an article inventory (kg)
Weathered coal (, containing humic acid 67.52%) 100 in butt
30% NaOH 40
NPE 0.2
Water 200
Water and NPE adding are equipped with in the conventional electric heating reacting kettle of anchor agitator, are warming up to 60 ℃, start stirring, adding is crushed to 80～100 purpose weathered coals, stirs 15min; Add 30% sodium hydroxide solution, be controlled in the 10min and add, keep 60～65 ℃ of reactions of temperature 4h, stop reaction, discharging, drying is crushed to 100 orders, measures wherein that solubility humic acid content is 42.47%, and conversion ratio only is 62.9%.
Claims (5)
1, a kind of high-viscosity material solid-liquid heterogeneous reaction high efficiency reactor, comprise gate stirrer (16), kettle (18), the housing of kettle (18) is chuck (14), charging aperture (3) is positioned at the case top of kettle (18), discharging opening (10) is positioned at the housing bottom of kettle (18), steam-gas inlet (13) is positioned at the lower housing portion of kettle (18), and the condensation mouth of pipe (4) is positioned at the case top of kettle (18); Gate stirrer (16) is positioned at kettle (18) top, its frame type agitating blade (15) links to each other with A motor (1) by reductor (2), it is characterized in that: kettle (18) bottom is provided with high shear stirred reactor (17), the stator (9) of high shear stirred reactor (17) is fixed on the kettle (18) with fixed mount (12), have some holes on stator (9) top and the side circumference, the rotating disk (8) of high shear stirred reactor (17) links to each other with B motor (11), between the rotating disk (8) of high shear stirred reactor (17) and the stator (9) slit is arranged.
2, high-viscosity material solid-liquid heterogeneous reaction high efficiency reactor as claimed in claim 1, it is characterized in that: big outer little A bellmouth (20) in stator (9) top of high shear stirred reactor (17) has has the little B bellmouth (21) of outer imperial palace on stator (9) the side circumference.
3, high-viscosity material solid-liquid heterogeneous reaction high efficiency reactor as claimed in claim 1 or 2 is characterized in that: the stirring piece (19) that four symmetries are arranged on rotating disk (8) card of high shear stirred reactor (17).
4, high-viscosity material solid-liquid heterogeneous reaction high efficiency reactor as claimed in claim 3 is characterized in that: the scraping blade (7) that the useful fixed clamping bar in frame type agitating blade (15) end (6) is fixing.
5, high-viscosity material solid-liquid heterogeneous reaction high efficiency reactor as claimed in claim 4, it is characterized in that: frame type agitating blade (15) is the Y type.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200520006044 CN2794624Y (en) | 2005-03-17 | 2005-03-17 | High efficiency reactor for high viscosity material solid liquid heterogeneous reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200520006044 CN2794624Y (en) | 2005-03-17 | 2005-03-17 | High efficiency reactor for high viscosity material solid liquid heterogeneous reaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2794624Y true CN2794624Y (en) | 2006-07-12 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200520006044 Expired - Fee Related CN2794624Y (en) | 2005-03-17 | 2005-03-17 | High efficiency reactor for high viscosity material solid liquid heterogeneous reaction |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102688623A (en) * | 2012-06-14 | 2012-09-26 | 长沙中联重科环卫机械有限公司 | Material heating device |
| CN104147995A (en) * | 2014-06-23 | 2014-11-19 | 南阳师范学院 | High-shear-force grinding reactor |
| CN105771856A (en) * | 2016-04-28 | 2016-07-20 | 庆丰鞋业（江苏）有限公司 | Reaction kettle with porous media |
| TWI563019B (en) * | 2015-05-05 | 2016-12-21 | Yang Min Hsiang | New process for producing humic acid salts with fluidizing solid phase reaction |
| CN106582359A (en) * | 2015-10-20 | 2017-04-26 | 上海寰球工程有限公司 | High efficient heterogeneous stirring equipment |
| CN108660061A (en) * | 2017-11-13 | 2018-10-16 | 陈城 | A kind of novel fermentation equipment |
| CN114477116A (en) * | 2022-01-24 | 2022-05-13 | 上海弗鲁克科技发展有限公司 | Method for preparing phosphoric acid by using high-shear reactor |
-
2005
- 2005-03-17 CN CN 200520006044 patent/CN2794624Y/en not_active Expired - Fee Related
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102688623A (en) * | 2012-06-14 | 2012-09-26 | 长沙中联重科环卫机械有限公司 | Material heating device |
| CN104147995A (en) * | 2014-06-23 | 2014-11-19 | 南阳师范学院 | High-shear-force grinding reactor |
| CN104147995B (en) * | 2014-06-23 | 2015-06-17 | 南阳师范学院 | High-shear-force grinding reactor |
| TWI563019B (en) * | 2015-05-05 | 2016-12-21 | Yang Min Hsiang | New process for producing humic acid salts with fluidizing solid phase reaction |
| CN106582359A (en) * | 2015-10-20 | 2017-04-26 | 上海寰球工程有限公司 | High efficient heterogeneous stirring equipment |
| CN105771856A (en) * | 2016-04-28 | 2016-07-20 | 庆丰鞋业（江苏）有限公司 | Reaction kettle with porous media |
| CN108660061A (en) * | 2017-11-13 | 2018-10-16 | 陈城 | A kind of novel fermentation equipment |
| CN114477116A (en) * | 2022-01-24 | 2022-05-13 | 上海弗鲁克科技发展有限公司 | Method for preparing phosphoric acid by using high-shear reactor |
| CN114477116B (en) * | 2022-01-24 | 2023-11-28 | 上海弗鲁克科技发展有限公司 | Method for preparing phosphoric acid by using high shear reactor |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee |
Owner name: WENGFU (GROUP) CO. Free format text: FORMER NAME OR ADDRESS: GUANGZHOU HONGFU INDUSTRIAL DEVELOPMENT CO., LTD. |
|
| CP03 | Change of name, title or address |
Address after: 57, South Road, Guiyang, Nanming District, Guizhou, China (550002) Patentee after: Wengfu (Group) Co., Ltd. Address before: Guizhou Fuquan racecourse, zip code: 550501 Patentee before: Hongfu Industry Development Gen. Co., Ltd., Guizhou |
|
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20060712 Termination date: 20140317 |