CN2774634Y - Finned tube cooling type single bed layer tube type reactor - Google Patents

Finned tube cooling type single bed layer tube type reactor Download PDF

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Publication number
CN2774634Y
CN2774634Y CN 200520078309 CN200520078309U CN2774634Y CN 2774634 Y CN2774634 Y CN 2774634Y CN 200520078309 CN200520078309 CN 200520078309 CN 200520078309 U CN200520078309 U CN 200520078309U CN 2774634 Y CN2774634 Y CN 2774634Y
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China
Prior art keywords
tube
finned tube
reactor
reaction
utility
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Expired - Lifetime
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CN 200520078309
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Chinese (zh)
Inventor
郭新峰
赵仕哲
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Xian Aerospace Huawei Chemical and Biologic Engineering Co Ltd
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Xian Aerospace Huawei Chemical and Biologic Engineering Co Ltd
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Priority to CN 200520078309 priority Critical patent/CN2774634Y/en
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Publication of CN2774634Y publication Critical patent/CN2774634Y/en
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Abstract

The utility model relates to a finned tube cooling type single bed layer tubular reactor. In China, in the production techniques of producing acrolein and acrylic acid in a two-step method by taking propylene as raw materials, a two-segment reactor with a middle tube plate is adopted, but because the two reaction segments have heat media with different temperatures, the reactor has the stress problem due to the temperature difference of a tube between the sagging plate and a reactor housing body and the connection problem which normally is a hydraulic expanding connection problem of the middle tube plate and a reaction tube; because the distance between the sagging plate and a fixed tube pipe is long, the expanding connection technology is complicated; if the treatment is improper, the two reaction segments are mixed with each other to affect the normal proceed of the reaction. The reactor of the utility model is a segment of reaction bed, a finned tube cooler is arranged in a tube box under a lower tube pipe; thus, the utility model is a finned tube cooling type single bed layer tubular reactor having the advantages of reasonable structure, simple fabrication and high heat-transfer efficiency.

Description

Finned tube cooled list bed tubular reactor
One, technical field:
The utility model relates to a kind of finned tube cooled list bed tubular reactor.
Two, technical background:
Be raw material at home with the propylene, all adopt the two section reactor that sagging plate is arranged in two-step method oxidation system third rare aldehyde, the acrylic acid production technology, its reaction tube is that the many vertical pipes of placing constitute, sagging plate is divided into two reative cells with different temperatures section with reaction tube, finish from the corresponding reaction of section each chamber, but because two hot medias that conversion zone has different temperatures, there is following problem in this reactor: 1, the stress problem that causes owing to the pipe temperature difference between sagging plate and reactor shell; 2, sagging plate is connected (being generally the hydraulic pressure account connects) problem with reaction tube; Because sagging plate is longer apart from fixed tube sheet, make account connect complex process, loaded down with trivial details, to deal with improperly and cause two conversion zone hot medias to be gone here and there mutually, the influence reaction is normally carried out.
Three, summary of the invention:
The purpose of this utility model be to provide a kind of rational in infrastructure, make the finned tube cooled list bed tubular reactor simple, that heat transfer efficiency is high.
For achieving the above object, the technical solution adopted in the utility model is:
A kind of finned tube cooled list bed tubular reactor, comprise housing 1, upper perforated plate 2, lower perforated plate 3, conversion zone, heating agent EGR that a plurality of reaction tubes 4 form, its special character is: described reactor is one section reaction bed 5, and finned tube cooling device 6 is set in the bobbin carriage below lower perforated plate 3.
Above-mentioned one-part form reactor shell 1 is outer to be provided with hot media equivalent, radially enter cocircuit 7 and following circuit 8 between pipe.
Above-mentioned conversion zone heating agent EGR comprises axial-flow pump 9, the steam generator 10 that directly links to each other with upper and lower circuit.
Finned tube cooling device 6 in the above-mentioned lower tube box comprises finned tube 11, hot media delivery pump 12 and steam generator 13.
The utility model is with respect to prior art, and its advantage is as follows:
1, reactor of the present utility model is one section reaction bed, and only needing to finish propylene oxidation through one section bed is acrolein reaction;
2, the utility model does not have sagging plate, cancels a large amount of account plumber's prefaces, saves cost; Need not solve exhaust, the discharge opeing difficult problem at sagging plate place;
3, the utility model has been cancelled the swollen account joint between sagging plate and housing;
4, there is not the mutual string phenomenon that sagging plate both sides hot media produces owing to the account pipe is bad in the utility model;
5, the utility model adopts fintube cooler, improves heat-transfer effect;
Four, description of drawings:
Fig. 1 is the structural representation of existing many bed reactors;
Fig. 2 is the utility model overall structure schematic diagram;
Five, the specific embodiment:
Referring to Fig. 1, be raw material with the propylene at home, all adopt the two section reactor that sagging plate is arranged in two-step method oxidation system third rare aldehyde, the acrylic acid production technology.
Referring to Fig. 2, reactor of the present utility model is one section reaction bed 5, and one section (single bed) shell and tube reactor of its no sagging plate is finished the reaction that propylene oxidation is a methacrylaldehyde.Finned tube cooling device 6 is set in the bobbin carriage below lower perforated plate 3, and it comprises finned tube 11, hot media delivery pump 12 and steam generator 13.In order to cooling reaction back gas, to reduce the side reaction of gas.Hot media equivalent is set outside one-part form reactor shell 1, radially enters cocircuit 7 and following circuit 8 between pipe.Conversion zone heating agent EGR of the present utility model comprises axial-flow pump 9, the steam generator 10 that directly links to each other with upper and lower circuit.
During use, enter the reaction tube 4 of reactor after propylene, oxygen (air), water vapour mix, by the beds in managing, propylene oxidation generates methacrylaldehyde and a small amount of acrylic acid.This is exothermic reaction, reaction heat reaches the hot media outside the pipe outside reaction tube 4, hot media is squeezed into down circuit 8 by axial-flow pump 9, through the perforate equivalent on the reactor, entering between reaction tube radially, take away reaction heat, return axial-flow pump 9 inlets after flowing into cocircuit 7, steam generator 10 again.Hot media and reaction tube 4 can be axially parallel stream or cross-flow passes.The hot media that flows in the pipe of fintube cooler 11, medium can be fused salt, conduction oil or boiler feedwater, hot media is squeezed into finned tube 11 through pump 12 and is taken away heat, through steam generator 13 heat is moved on to outside the circulatory system.The finned tube outer wall arrives reacted gas cooled the temperature that needs.

Claims (4)

1, a kind of finned tube cooled list bed tubular reactor, comprise housing (1), upper perforated plate (2), lower perforated plate (3), conversion zone, heating agent EGR that a plurality of reaction tubes (4) form, it is characterized in that: described reactor is one section reaction bed (5), and finned tube cooling device (6) is set in the bobbin carriage below lower perforated plate (3).
2, finned tube cooled list bed tubular reactor according to claim 1 is characterized in that: described one-part form reactor shell (1) is outer to be provided with hot media equivalent, radially enter cocircuit (7) and following circuit (8) between pipe.
3, finned tube cooled list bed tubular reactor according to claim 1 and 2, it is characterized in that: described conversion zone heating agent EGR comprises axial-flow pump (9), the steam generator (10) that directly links to each other with upper and lower circuit.
4, finned tube cooled list bed tubular reactor according to claim 3 is characterized in that: the finned tube cooling device (6) in the described lower tube box comprises finned tube (11), hot media delivery pump (12) and steam generator (13).
CN 200520078309 2005-01-31 2005-01-31 Finned tube cooling type single bed layer tube type reactor Expired - Lifetime CN2774634Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 200520078309 CN2774634Y (en) 2005-01-31 2005-01-31 Finned tube cooling type single bed layer tube type reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 200520078309 CN2774634Y (en) 2005-01-31 2005-01-31 Finned tube cooling type single bed layer tube type reactor

Publications (1)

Publication Number Publication Date
CN2774634Y true CN2774634Y (en) 2006-04-26

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Family Applications (1)

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CN 200520078309 Expired - Lifetime CN2774634Y (en) 2005-01-31 2005-01-31 Finned tube cooling type single bed layer tube type reactor

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CN (1) CN2774634Y (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102641712A (en) * 2012-02-29 2012-08-22 大庆志飞生物化工有限公司 Novel reaction kettle for producing methylamino avermectin benzoate
CN115738921A (en) * 2022-11-29 2023-03-07 东方电气集团东方锅炉股份有限公司 Tube array type maleic anhydride reactor system with uniformly cooled reactor inlet and outlet multi-cavity
CN116272686A (en) * 2023-01-03 2023-06-23 东方电气集团东方锅炉股份有限公司 Mixed flow tubular fixed bed reactor

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102641712A (en) * 2012-02-29 2012-08-22 大庆志飞生物化工有限公司 Novel reaction kettle for producing methylamino avermectin benzoate
CN115738921A (en) * 2022-11-29 2023-03-07 东方电气集团东方锅炉股份有限公司 Tube array type maleic anhydride reactor system with uniformly cooled reactor inlet and outlet multi-cavity
CN116272686A (en) * 2023-01-03 2023-06-23 东方电气集团东方锅炉股份有限公司 Mixed flow tubular fixed bed reactor

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee

Owner name: HUAWEI PRESSURE CONTAINER MANUFACTURING CO., LTD.,

Free format text: FORMER NAME OR ADDRESS: XI AN AEROSPACE HUAWEI PRESSURE VESSEL MANUFACTURING CO., LTD.

CP01 Change in the name or title of a patent holder

Patentee after: Huawei Chemical Bioengineering Co., Ltd., Xi'an Aerospace

Patentee before: Xi'an Huawei Huawei Pressure Vessel Manufacturing Co., Ltd.

C17 Cessation of patent right
CX01 Expiry of patent term

Expiration termination date: 20150131

Granted publication date: 20060426