CN2657780Y - Ultrasonic disintegrator - Google Patents

Ultrasonic disintegrator Download PDF

Info

Publication number
CN2657780Y
CN2657780Y CN 200320106324 CN200320106324U CN2657780Y CN 2657780 Y CN2657780 Y CN 2657780Y CN 200320106324 CN200320106324 CN 200320106324 CN 200320106324 U CN200320106324 U CN 200320106324U CN 2657780 Y CN2657780 Y CN 2657780Y
Authority
CN
China
Prior art keywords
ultrasonic wave
ultrasonic
tube
takes place
pulverizer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN 200320106324
Other languages
Chinese (zh)
Inventor
郑少华
王平
任振
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jinan University
University of Jinan
Original Assignee
University of Jinan
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by University of Jinan filed Critical University of Jinan
Priority to CN 200320106324 priority Critical patent/CN2657780Y/en
Application granted granted Critical
Publication of CN2657780Y publication Critical patent/CN2657780Y/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Abstract

The utility model relates to a pulverizer, in particular to an ultrasonic pulverizer which integrates ultrasonic pulverization and mechanical agitation pulverization and is used for pulverization of metal or non-metal materials. An ultrasonic generating cylinder is fixed around an agitation cylinder; the bottom of the ultrasonic generating cylinder has a water inlet pipe, and the upper part of the ultrasonic generating cylinder has a water outlet pipe; the periphery of the ultrasonic generating cylinder is provided with uniformly distributed ultrasonic emitters. With the advantages of simple structure and convenient manufacture, the utility model integrates ultrasonic pulverization and mechanical agitation pulverization and can pulverizes metal and non-metal materials into particles of nanometer grades.

Description

The ultrasonic wave pulverizer
(1) technical field under
The utility model relates to a kind of pulverizer, particularly a kind of ultrasonic wave the pulverizing and ultrasonic wave pulverizer that the mechanical agitation pulverizing combines.
(2) background technology
Along with science and technology development, the required powder granularity of people is more and more littler, and the needs that have reach nano level powder.Particularly along with the intensification that nano material is understood, the performance of the various excellences of nano material is found, and the application of nano material is more and more wider.The function of the stirring pulverizer that uses is limit at present, and made powder granularity is relatively too big, does not reach the demand under people's particular case.Be 87213972 Chinese patent as the patent No.: " supersonic cell pulverizer " discloses a kind of ultrasonic wave that utilizes and pulverized organic cell pulverization machine.Because organic matter hardness is little, to pulverize than being easier to, above-mentioned grinder can reach the requirement that nanoscale is pulverized.But, use above-mentioned cell pulverization machine then not reach desirable effect for some metals and inorganic non-metallic thing, particularly silicates.
(3) utility model content
The utility model provides a kind of and has utilized ultrasonic wave pulverizing and mechanical agitation pulverizing to combine in order to overcome above deficiency, inorganic matter can be crushed to nano level ultrasonic wave pulverizer.
The technical solution of the utility model realizes by following measure:
A kind of ultrasonic wave pulverizer comprises motor, electric machine support, is used for churned mechanically stirring rod, is used to hold mixing drum, the cylinder stent of crushed material; Fix a ultrasonic wave in the periphery of mixing drum tube takes place, a water inlet pipe is arranged at the bottom that tube takes place ultrasonic wave, and an outlet pipe is arranged at top; The peripheral symmetry that tube takes place ultrasonic wave is evenly equipped with ultrasonic transmitter.
Ultrasonic wave pulverizer of the present utility model is installed ultrasonic wave for convenience tube is taken place, and improves hyperacoustic crush efficiency, and tube takes place described ultrasonic wave is the positive multiedge cylinder of even number face.
Tube takes place in order to protect ultrasonic wave, and is used for the support fixation pulverizer in ultrasonic wave pulverizer of the present utility model, sends out the periphery of tube at ultrasonic wave and fixes a urceolus.
Ultrasonic wave pulverizer of the present utility model, described ultrasonic frequency are 20KHz~50KHz.
Architectural feature of the present utility model: tube takes place and is preferably multiple edge body configuration (being generally the even number face) in ultrasonic wave, on its each face ultrasonic transmitter is installed, and evenly distributes at an angle between the ultrasonic transmitter.Because even number face polyhedron is configured as symmetrical structure, assemble thereby make the ultrasonic transmitter ultrasonic waves transmitted transmit to the center.Utilize hyperacoustic cavitation blast effect and microjet effect, material is done further pulverizing and dispersion.
Frequency of ultrasonic is very high, generally between 20KHz~50KHz.Have stronger cavitation shock effect and microjet effect.Material had stronger percussion.Combine by ultrasonic wave pulverizing and mechanical crushing, can play a multiplier role.
The utility model can crushing metal and inorganic non-metallic material, particularly silicate compound.With ESEM the material after pulverizing is carried out grain size analysis, find that it has reached nanoscale, that is to say that the utility model can produce nano-powder fully in a large number.
The utility model can be crushed to nanoscale with metal and Inorganic Non-metallic Materials, can select different abrasive medias and decentralized medium for use according to the character of the powder produced of require.Be applied to chemical industry, metallurgy, building materials, electronics etc. and need a large amount of industries of producing nano-powder.
The utility model is pulverized ultrasonic wave and stir to pulverize to combine and also metal and non-metallic material pulverizing can be nanoscale, has advantage simple in structure, easily manufactured.
(4) description of drawings
Below in conjunction with the drawings and specific embodiments the utility model is further described.
Fig. 1 is a structural representation of the present utility model
Fig. 2 is the A-A cutaway view of Fig. 1
Fig. 3 is for pulverizing the electromicroscopic photograph of MgO material
Fig. 4 is for pulverizing the size distribution histogram of MgO material
Fig. 5 is the electromicroscopic photograph of crushing metal copper material
Fig. 6 is the size distribution histogram of crushing metal copper material
Among Fig. 1,2,1 motor, 2 stirring rod, 3 mixing drums, tube takes place in 4 ultrasonic waves, 5 ultrasonic transmitters, 6 urceolus, 7 cylinder stents, 8 perpendicular stent support seats, 9 perpendicular supports, 10 electric machine supports, 11 outlet pipes, 12 water inlet pipes.
(5) specific embodiment
Accompanying drawing 1 and Fig. 2 are a kind of specific embodiment of the present utility model.
Tube 3 takes place described ultrasonic wave is positive eight rib builds, and each side that tube 3 takes place ultrasonic wave is evenly distributed with upper and lower 2 ultrasonic transmitters 5, and the bottom that tube takes place ultrasonic wave is evenly distributed with 3 ultrasonic transmitters 5 that are the equilateral triangle symmetry.The bottom that tube 4 takes place ultrasonic wave is provided with a water inlet pipe 12, and the top that the tube side takes place ultrasonic wave is provided with an outlet pipe 11.
The mixing drum 3 of this embodiment is enclosed within ultrasonic wave and takes place in the tube 6, ultrasonic generation tube 6 is enclosed within the urceolus, the flange that tube and urceolus take place for mixing drum 3, ultrasonic wave passes through bolted on connection together, and a seal cover is arranged on the mixing drum 3, and urceolus 6 is by being bolted on the cylinder stent 7.Be useful on churned mechanically stirring rod 2 in the mixing drum 3, and the abrasive body of making by the corundum ball.Stirring rod 2 is driven by motor 1.Described buncher 1 is fixed on the electric machine support 10, and electric machine support 10 is fixed on the perpendicular support 9 and can slides up and down along perpendicular support 9, and perpendicular support 9 is enclosed within the perpendicular stent support seat 8, and by set lever locking, the perpendicular support 9 of release handle can rotate freely.
Two ultrasonic transmitters (vibration frequency 20KHz) are installed on each side of ultrasonic wave launching tube, and the bottom symmetry is installed three ultrasonic transmitters, amounts to 19 ultrasonic transmitters, and general power is 1500W; The mixing drum volume is 4500L, and the entire machine apparent size is long 760mm * wide 550mm * high 1400mm, and used abrasive body is the corundum ball, and decentralized medium is a water.
The material that present embodiment is pulverized is MgO, average grain diameter: D Flat=5.39 μ m, meta particle diameter D In=11.06 μ m, maximum particle diameter is D Max=45 μ m.
Concrete operations are: material is contained in the mixing drum 3, and buncher 1 drives stirring rod 2 stirring abrasive medias material is pulverized.Take place in the tube 4 because mixing drum 3 is enclosed within ultrasonic wave,, utilized cavitation effect of ultrasonic waves and microjet effect that material is done further pulverizing and peptizaiton, reunite to prevent material so simultaneously it is applied ultrasonic wave in that material is pulverized.The water circulation takes place to be provided with between tube in mixing drum and ultrasonic wave, and its bottom is provided with water inlet pipe 12, and top is provided with outlet pipe 11, and water circulates the effect of playing cooling from lower to upper.
With ESEM the material after pulverizing is carried out grain size analysis, find that it has reached nanoscale, that is to say that the utility model can produce nano-powder fully in a large number.
Material after the pulverizing carries out grain size analysis with ESEM (25000 times of multiplication factors), its electromicroscopic photograph as shown in Figure 3, size distribution such as table 1, shown in Figure 4.
Table 1 granulometry is table (powder granule number 524) as a result
Project name Minimum of a value Maximum Mean value Standard variance
Feature area (μ m 2) 0.000 0.020 0.003 0.005
Girth (μ m) 0.040 0.740 0.216 0.139
0 degree direction particle diameter (μ m) 0.020 0.200 0.065 0.037
90 degree direction particle diameters (μ m) 0.020 0.250 0.071 0.041
2. embodiment 2
The present embodiment ultrasonic frequency is 45KHz, and general power is 1500W.Comminuting matter is a metallic copper.Average grain diameter: D Flat=2.07 μ m, meta particle diameter D In=2.86 μ m, maximum particle diameter is D Max=30 μ m.Other is substantially the same manner as Example 1.
Material after the pulverizing carries out grain size analysis with ESEM (15000 times of multiplication factors), its electromicroscopic photograph as shown in Figure 5, size distribution such as table 2, shown in Figure 6.
Table 2 granulometry is table (powder granule number 524) as a result
Project name Minimum of a value Maximum Mean value Standard variance
Feature area (μ m 2) 0.000 0.010 0.005 0.005
Girth (μ m) 0.070 0.860 0.304 0.164
0 degree direction particle diameter (μ m) 0.030 0.210 0.091 0.042
90 degree direction particle diameters (μ m) 0.030 0.260 0.086 0.037

Claims (6)

1. ultrasonic wave pulverizer, comprise motor (1), electric machine support (10), be used for churned mechanically stirring rod (2), be used to hold the mixing drum (3) of crushed material, it is characterized in that: fix a ultrasonic wave in the periphery of mixing drum (3) tube (4) takes place, one water inlet pipe (12) is arranged at the bottom that tube takes place ultrasonic wave, and an outlet pipe (11) is arranged at top; The peripheral symmetry that tube (4) takes place ultrasonic wave is evenly equipped with ultrasonic transmitter (5).
2. ultrasonic wave pulverizer according to claim 1 is characterized in that: tube (4) takes place described ultrasonic wave is the positive multiedge cylinder of even number face.
3. ultrasonic wave pulverizer according to claim 1 and 2 is characterized in that: ultrasonic wave is sent out the periphery of tube (4) and is fixed a urceolus (6).
4. ultrasonic wave pulverizer according to claim 2, it is characterized in that: tube (4) takes place and is positive eight prisms in described ultrasonic wave, be fixed with upper and lower two ultrasonic transmitters (5) on each side, the bottom of ultrasonic wave generation tube is fixed with the ultrasonic transmitter (5) of three symmetries.
5. ultrasonic wave pulverizer according to claim 3 is characterized in that: described ultrasonic frequency is 20KHz~50KHz.
6. ultrasonic wave pulverizer according to claim 3 is characterized in that: connected as one by bolt between the flange of described mixing drum (3), ultrasonic wave generation tube (4) and urceolus (6).
CN 200320106324 2003-10-20 2003-10-20 Ultrasonic disintegrator Expired - Lifetime CN2657780Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 200320106324 CN2657780Y (en) 2003-10-20 2003-10-20 Ultrasonic disintegrator

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 200320106324 CN2657780Y (en) 2003-10-20 2003-10-20 Ultrasonic disintegrator

Publications (1)

Publication Number Publication Date
CN2657780Y true CN2657780Y (en) 2004-11-24

Family

ID=34341614

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 200320106324 Expired - Lifetime CN2657780Y (en) 2003-10-20 2003-10-20 Ultrasonic disintegrator

Country Status (1)

Country Link
CN (1) CN2657780Y (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103203265A (en) * 2012-01-13 2013-07-17 谢小飞 Ultrasonic high-energy density bead mill for biological cell wall breaking
CN103785511A (en) * 2014-03-04 2014-05-14 湖南大学 Microwave and ultrasound combined assisted ball-milling device and process for preparing high-performance nanopowder
CN105728149A (en) * 2014-12-08 2016-07-06 苏州珀西瓦尔实验设备有限公司 Ultrasonic wave fragmentation all-in-one machine
CN106269150A (en) * 2016-08-08 2017-01-04 太仓市双凤镇薄彩工艺品厂 A kind of high temperature resistant gypsum grinding powder craft
CN108043553A (en) * 2017-11-27 2018-05-18 重庆市合川区金星玻璃制品有限公司 The breaker of quartz glass
EP3261770A4 (en) * 2015-02-24 2018-10-24 Liquitab Systems Limited Improved apparatus for disintegration of a solid and method
CN110756312A (en) * 2019-10-21 2020-02-07 大同新成新材料股份有限公司 Intelligent crushing method for irregular semiconductor material
CN114260088A (en) * 2021-12-27 2022-04-01 上交赛孚尔(包头)新材料有限公司 Drum-type material grinding machine

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103203265A (en) * 2012-01-13 2013-07-17 谢小飞 Ultrasonic high-energy density bead mill for biological cell wall breaking
CN103785511A (en) * 2014-03-04 2014-05-14 湖南大学 Microwave and ultrasound combined assisted ball-milling device and process for preparing high-performance nanopowder
CN103785511B (en) * 2014-03-04 2016-02-24 湖南大学 A kind of microwave ultrasound associating auxiliary ball mill apparatus and technique preparing high-performance nano powder
CN105728149A (en) * 2014-12-08 2016-07-06 苏州珀西瓦尔实验设备有限公司 Ultrasonic wave fragmentation all-in-one machine
EP3261770A4 (en) * 2015-02-24 2018-10-24 Liquitab Systems Limited Improved apparatus for disintegration of a solid and method
AU2016224136B2 (en) * 2015-02-24 2019-12-12 Liquitab Systems Limited Improved apparatus for disintegration of a solid and method
CN106269150A (en) * 2016-08-08 2017-01-04 太仓市双凤镇薄彩工艺品厂 A kind of high temperature resistant gypsum grinding powder craft
CN108043553A (en) * 2017-11-27 2018-05-18 重庆市合川区金星玻璃制品有限公司 The breaker of quartz glass
CN110756312A (en) * 2019-10-21 2020-02-07 大同新成新材料股份有限公司 Intelligent crushing method for irregular semiconductor material
CN114260088A (en) * 2021-12-27 2022-04-01 上交赛孚尔(包头)新材料有限公司 Drum-type material grinding machine

Similar Documents

Publication Publication Date Title
CN1270829C (en) Supersonic disintegrator
US6991189B2 (en) Process for micronizing materials
CN2657780Y (en) Ultrasonic disintegrator
AU2002336425A1 (en) Process for micronizing materials
CN102284326B (en) Ultrasonic ball mill pulverizer
CN109954542A (en) Noble metal intelligence recyclable device during a kind of automobile dismounting
CN111804393A (en) Automatic sand making machine capable of circularly crushing
CN2376334Y (en) Agitating mill for producing submicrometer grade graphite microparticle
EP1333929B1 (en) Grinding of particulate material
CN212441381U (en) Reducing mechanism for building
CN114682353A (en) Multistage granulation reducing mechanism for architectural ceramics
CN114162817A (en) Graphite powder balling and shaping system
WO2020155429A1 (en) High-performance crusher for sample preparation
CN101643215B (en) Preparation method of attapulgite used for mammalian cell culture
JP3138115B2 (en) Wet grinding method
CN114307791B (en) Dispersing system of carbon nano tube
CN2299661Y (en) Wet-type cyclic-stirring mill
CN210411034U (en) Rubbing crusher for waste treatment
CN211099378U (en) Automatic pneumatic pulverizer
CN210386172U (en) Powder material boiling device
CN214262056U (en) Dog grain production is with hierarchical breaker
CN219596796U (en) Grinding device for lithium iron phosphate precursor
CN209049533U (en) A kind of cement block dispersing device
CN214732930U (en) Accurate phosphogypsum powder feeding bin for adding cement chromium removing agent
CN214974583U (en) Raw material crushing device for processing plastic foam of automobile lining pad

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
AV01 Patent right actively abandoned

Effective date of abandoning: 20031020

C25 Abandonment of patent right or utility model to avoid double patenting