CN2555932Y - Hydrogen grinder for magnetic material - Google Patents

Hydrogen grinder for magnetic material Download PDF

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Publication number
CN2555932Y
CN2555932Y CN 02268466 CN02268466U CN2555932Y CN 2555932 Y CN2555932 Y CN 2555932Y CN 02268466 CN02268466 CN 02268466 CN 02268466 U CN02268466 U CN 02268466U CN 2555932 Y CN2555932 Y CN 2555932Y
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CN
China
Prior art keywords
hydrogen
magnetic material
valve
cylinder
cylindrical shell
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 02268466
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Chinese (zh)
Inventor
李康
崔巍
信应刚
贾秀山
宋跃育
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JIASHITE PURIFICATION EQUIPMENT CO Ltd TAIYUAN CITY
Original Assignee
JIASHITE PURIFICATION EQUIPMENT CO Ltd TAIYUAN CITY
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JIASHITE PURIFICATION EQUIPMENT CO Ltd TAIYUAN CITY filed Critical JIASHITE PURIFICATION EQUIPMENT CO Ltd TAIYUAN CITY
Priority to CN 02268466 priority Critical patent/CN2555932Y/en
Application granted granted Critical
Publication of CN2555932Y publication Critical patent/CN2555932Y/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Hard Magnetic Materials (AREA)

Abstract

The utility model relates to a grinder, a magnetic material, in particular to a hydrogen grinder for magnetic material. The grinder comprises a hydrogen absorption crushing cylinder with an electric heater. The outer layer of the hydrogen absorption crushing cylinder is provided with a water jacket and the bottom part of the hydrogen absorption crushing cylinder is connected with a dehydrogenating crushing cylinder with an electric heater through a valve. The bottom part of the dehydrogenating crushing cylinder is provided with a valve and the upper part of the dehydrogenating crushing cylinder is provided with a cooling cylinder that is actively and hermetically connected with the valve arranged at the bottom part of the dehydrogenating crushing cylinder. The hydrogen grinder for magnetic material accomplishes working procedures of hydrogen absorption, dehydrogenating and cooling in various containers and adopts a vertical structure that each container is mutually connected through a valve, thus being convenient for the transmission of each working procedure of the magnetic material and leading the hydrogen grinder to realized continuous manufacture and improve the manufacture efficiency of the grinder.

Description

The hydrogen reducing mechanism of magnetic material
Technical field
The utility model relates to a kind of reducing mechanism, is specially magnetic material, particularly the hydrogen reducing mechanism of neodymium-iron-boron magnetic material.
Background technology
Rare earth transition metal magnetic material, particularly neodymium-iron-boron magnetic material have invertibity and inhale the characteristic of putting hydrogen and disproportionation decomposition.Under certain hydrogen pressure, magnetic material low temperature is inhaled hydrogen generation efflorescence behavior, and middle temperature is inhaled the behavior of hydrogen generation disproportionation, then keeps the structure of former compound constant behind the high-temperature dehydrogenation.Utilize the above-mentioned characteristic of rare earth metal magnetic material, can be made into the hydrogen reducing mechanism of magnetic material.Existing magnetic material hydrogen reducing mechanism, processes such as the efflorescence of low temperature suction hydrogen, middle temperature suction hydrogen disproportionation, high-temperature dehydrogenation and cooling are all finished in single container, and this container needs input pressure hydrogen a little while, extracts hydrogen out a little while, heat a little while, cooling a little while, like this, not only structure, the performance to apparatus container has strict demand, and each operation can not be carried out simultaneously, because the inertia of vessel temp, pressure, the inefficiency that device hydrogen is pulverized is unfavorable for continuous production.
Summary of the invention
The utility model solves existing hydrogen reducing mechanism can not the quantity-produced problem, the magnetic material hydrogen reducing mechanism that provides a kind of each operation can be simultaneously, carry out continuously.
The utility model is to adopt following technical scheme to realize: magnetic material hydrogen reducing mechanism, comprise the suction hydrogen pulverization cylinder that has electric heater unit, the skin of inhaling the hydrogen pulverization cylinder is provided with water jacket, the bottom of inhaling the hydrogen pulverization cylinder links by valve and the dehydrogenation tube that has electric heater unit, the dehydrogenation tube bottom is fixed with valve, and dehydrogenation tube bottom is provided with the cooling cylinder with the activity of dehydrogenation tube bottom valve, sealed attachment.Dehydrogenation tube bottom valve can be fixed by cylindrical shell direct with bolt and the dehydrogenation tube.Cooling cylinder can rely between the two pressure realization activity, sealed attachment by an auxiliary last moving mechanism with cooling cylinder and dehydrogenation tube bottom valve dieback.This device is finished the container separately of the pulverizing of suction hydrogen, high-temperature dehydrogenation, refrigerating work procedure by setting and by valve it is coupled to each other, form and press the vertical structure that process sequence is arranged, the control respective valves, magnetic material enters in the cylindrical shell of each operation successively, each operation is finished in the container separately, realize that each operation carries out simultaneously, and then reach device quantity-produced purpose.
Inhale the electric heater unit of hydrogen pulverization cylinder, dehydrogenation tube, can adopt built-in or the external electric heating device, built-in structure is with electric heating element---electrically heated rod places tube inner chamber, and outlet structure is with electric heating element---, and resistive heater is wrapped in outside the cylindrical shell.The structure of heater can be selected as required.
The utility model is inhaled the valve of hydrogen pulverization cylinder, dehydrogenation tube bottom can adopt butterfly valve or slide valve.
Because the operating temperature of dehydrogenation tube is higher, cooling cylinder, inhale hydrogen pulverize by the valve tube directly and the dehydrogenation tube link, the dehydrogenation tube can be directly to cooling cylinder, suction hydrogen pulverization cylinder conduction heat, simultaneously, structure to cooling cylinder, suction hydrogen pulverization cylinder, particularly the valve on the cooling cylinder and the hear resistance of inhaling the valve between hydrogen pulverization cylinder and dehydrogenation tube have higher requirement, even this valve need adopt the high temperature resistant valve of special use, thereby can increase the manufacturing cost of cooling cylinder and whole device.For this reason, between suction hydrogen pulverization cylinder and dehydrogenation tube, have additional heat insulation cylindrical shell, heat insulation cylindrical shell links with inhaling hydrogen pulverization cylinder and dehydrogenation tube respectively through valve up and down, and the dehydrogenation tube links by its bottom valve and heat insulation cylindrical shell, movable, the sealed attachment of cooling cylinder and heat insulation cylindrical shell bottom.
Magnetic material hydrogen reducing mechanism described in the utility model, suction hydrogen, dehydrogenation, refrigerating work procedure that magnetic material hydrogen is pulverized are finished in different containers simultaneously, and adopt the vertical structure that is coupled to each other by valve between each container, be convenient to the transmission of each inter process of magnetic material, also make the hydrogen reducing mechanism realize producing continuously, improve the efficient that device is produced.
Description of drawings
Fig. 1 is a structural representation of the present utility model;
The specific embodiment
Magnetic material hydrogen reducing mechanism, comprise the suction hydrogen pulverization cylinder 1 that has electric heater unit, suction hydrogen pulverization cylinder has the loam cake 11 of sealed attachment and takes out, the mouth of pipe 12 of inflation body, the skin of inhaling the hydrogen pulverization cylinder is provided with water jacket 2, communicate with water jacket and to be provided with into, effluent pipe mouth, the electric heater unit of inhaling the hydrogen pulverization cylinder adopts electrically heated rod 7 to be fixed in the built-in structure of tube inner chamber, the bottom of inhaling the hydrogen pulverization cylinder links by valve 3 and heat insulation cylindrical shell 20, the bottom of heat insulation cylindrical shell links by valve 21 and the dehydrogenation tube 4 that has electric heater unit, the electric heater unit of dehydrogenation tube adopts resistive heater 10 to be wrapped in the outer outlet structure of cylindrical shell, the dehydrogenation tube is provided with to be taken out, aerating pipe port 13, the dehydrogenation tube bottom links by valve 5 and heat insulation cylindrical shell 8, cooling cylinder 6 and heat insulation cylindrical shell activity, sealed attachment.Valve 3,21,5 between each cylindrical shell all adopts butterfly valve, and be convenient fixing the employing to the folder butterfly valve, the end that is coupled to each other of each cylindrical shell is all managed orchid, will be clamped between the flange of cylindrical shell the folder butterfly valve with bolt, thereby realize connecting between each cylindrical shell and valve and cylindrical shell.Routinely, cooling cylinder 6 upper ends are provided with valve, are used for the switching of cooling cylinder, because the existence of heat insulation cylindrical shell 8, the valve on the cooling cylinder can adopt the common butterfly valve of nonrefractory structure, also be provided with on the cooling cylinder take out, aerating pipe port 14.Be to accelerate the cooling of cooling cylinder, be provided with water jacket 9,, accelerate the cooling of magnetic material in the cooling cylinder by the circulation of cooling water in the water jacket at the skin of cooling cylinder.Heat insulation cylindrical shell 8,20 also is provided with water jacket, increases the effect of heat insulation of heat insulation cylindrical shell.All water jackets in this device all have the water-in and water-out mouth of pipe, make the water circulation in the water jacket.
Open the loam cake of inhaling the hydrogen pulverization cylinder, magnetic material such as NdFeB material are added in the tube, the loam cake closure, at first by inhale taking out on hydrogen pulverization cylinder and the dehydrogenation tube, 12,13 pairs of cylinder lumens of aerating pipe port vacuumize, filling with inert gas, and the oxygen content of cylinder lumen is reached below the License Value.Then, input pressure hydrogen in inhaling the hydrogen pulverization cylinder, inhaling the hydrogen incipient stage, magnetic material carries out surface active needs certain environment temperature, and the electric heater unit of inhaling the hydrogen pulverization cylinder heats magnetic material, because inhaling the hydrogen process is an exothermic process, therefore, after suction hydrogen process formally began, electric heater unit quit work, inhale the outer field water jacket of hydrogen pulverization cylinder and play the cooling effect, make to inhale to keep inhaling the required environment temperature of hydrogen in the hydrogen pulverization cylinder.After suction hydrogen process is finished, open and inhale hydrogen pulverization cylinder, heat insulation cylindrical shell bottom valve, the magnetic material after the efflorescence of suction hydrogen enters the dehydrogenation tube through valve, the electric heater unit of dehydrogenation tube heats dehydrogenation tube inner chamber high temperature, simultaneously, the dehydrogenation tube is found time, the hydrogen in the magnetic material is removed.By cooling cylinder being pressed under heat insulation cylindrical shell with this matched with devices specific hydraulic rising mechanism, make sealing between the two, open the valve of cooling cylinder, by its take out, aerating pipe port 14 vacuumizes and filling with inert gas, the oxygen content of cooling cylinder inner chamber and heat insulation cylinder lumen is reached below the License Value, open the valve of dehydrogenation tube bottom, the finished product magnetic material falls in the cooling cylinder, cooling cylinder is filled the valve of closing dehydrogenation tube and cooling cylinder behind the finished product magnetic material, cooling cylinder separates with the dehydrogenation tube, the finished product magnetic material can be loaded on a plurality of cooling cylinders by said process.Magnetic material in the cooling cylinder cools off under the effect of outer water jacket.

Claims (5)

1, a kind of magnetic material hydrogen reducing mechanism, it is characterized by: comprise the suction hydrogen pulverization cylinder (1) that has electric heater unit, the skin of inhaling the hydrogen pulverization cylinder is provided with water jacket (2), the bottom of inhaling the hydrogen pulverization cylinder links by valve (3) and the dehydrogenation tube (4) that has electric heater unit, the dehydrogenation tube bottom is fixed with valve (5), and dehydrogenation tube bottom is provided with the cooling cylinder (6) with the activity of dehydrogenation tube bottom valve, sealed attachment.
2, magnetic material hydrogen reducing mechanism as claimed in claim 1, it is characterized by: between suction hydrogen pulverization cylinder and dehydrogenation tube, have additional heat insulation cylindrical shell (20), heat insulation cylindrical shell (20) links with suction hydrogen pulverization cylinder and dehydrogenation tube respectively through valve (3), (21) up and down, the dehydrogenation tube links by its bottom valve (5) and heat insulation cylindrical shell (8), cooling cylinder (6) and movable, the sealed attachment in heat insulation cylindrical shell bottom.
3, as claim 1,2 described magnetic material hydrogen reducing mechanisms, it is characterized by: the electric heater unit of inhaling the hydrogen pulverization cylinder adopts electrically heated rod (7) to place the built-in structure of tube inner chamber, and the electric heater unit employing of dehydrogenation tube adds thermal resistance wire (10) and is wrapped in the outer outlet structure of cylindrical shell.
4, as claim 1,2 described magnetic material hydrogen reducing mechanisms, it is characterized by: the skin at cooling cylinder is provided with water jacket (9).
5, magnetic material hydrogen reducing mechanism as claimed in claim 2, it is characterized by: heat insulation cylindrical shell (8), (20) also are provided with water jacket.
CN 02268466 2002-07-26 2002-07-26 Hydrogen grinder for magnetic material Expired - Fee Related CN2555932Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 02268466 CN2555932Y (en) 2002-07-26 2002-07-26 Hydrogen grinder for magnetic material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 02268466 CN2555932Y (en) 2002-07-26 2002-07-26 Hydrogen grinder for magnetic material

Publications (1)

Publication Number Publication Date
CN2555932Y true CN2555932Y (en) 2003-06-18

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CN 02268466 Expired - Fee Related CN2555932Y (en) 2002-07-26 2002-07-26 Hydrogen grinder for magnetic material

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014071707A1 (en) * 2012-11-08 2014-05-15 沈阳中北通磁科技股份有限公司 Continuous hydrogen decrepitation processing method for rare earth permanently magnetic alloy and production equipment therefor
CN103801700A (en) * 2012-11-08 2014-05-21 沈阳中北通磁科技股份有限公司 Rare earth permanent magnetic alloy flexible hydrogen breaking process method
CN103801702A (en) * 2012-11-08 2014-05-21 沈阳中北真空科技有限公司 Rare earth permanent magnetic alloy hydrogen decrepitation continuous production equipment
CN104624338A (en) * 2015-03-13 2015-05-20 苏州圣谱拉新材料科技有限公司 Heated and stimulated crusher
CN103801702B (en) * 2012-11-08 2016-11-30 沈阳中北真空科技有限公司 RE permanent magnetic alloy hydrogen breaks continuous producing apparatus
CN113649580A (en) * 2021-07-13 2021-11-16 杭州电子科技大学 Efficient hydrogen breaking device and rare earth alloy hydrogen breaking method

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014071707A1 (en) * 2012-11-08 2014-05-15 沈阳中北通磁科技股份有限公司 Continuous hydrogen decrepitation processing method for rare earth permanently magnetic alloy and production equipment therefor
CN103801703A (en) * 2012-11-08 2014-05-21 沈阳中北通磁科技股份有限公司 Rare earth permanent magnetic alloy continuous hydrogen decrepitation process method
CN103801700A (en) * 2012-11-08 2014-05-21 沈阳中北通磁科技股份有限公司 Rare earth permanent magnetic alloy flexible hydrogen breaking process method
CN103801702A (en) * 2012-11-08 2014-05-21 沈阳中北真空科技有限公司 Rare earth permanent magnetic alloy hydrogen decrepitation continuous production equipment
CN103801702B (en) * 2012-11-08 2016-11-30 沈阳中北真空科技有限公司 RE permanent magnetic alloy hydrogen breaks continuous producing apparatus
CN103801700B (en) * 2012-11-08 2016-12-21 沈阳中北通磁科技股份有限公司 RE permanent magnetic alloy flexibility hydrogen breaks process
CN103801703B (en) * 2012-11-08 2017-01-18 沈阳中北通磁科技股份有限公司 Rare earth permanent magnetic alloy continuous hydrogen decrepitation process method
CN104624338A (en) * 2015-03-13 2015-05-20 苏州圣谱拉新材料科技有限公司 Heated and stimulated crusher
CN113649580A (en) * 2021-07-13 2021-11-16 杭州电子科技大学 Efficient hydrogen breaking device and rare earth alloy hydrogen breaking method

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