CN2493270Y - Multi-function crystallizer - Google Patents
Multi-function crystallizer Download PDFInfo
- Publication number
- CN2493270Y CN2493270Y CN 01245026 CN01245026U CN2493270Y CN 2493270 Y CN2493270 Y CN 2493270Y CN 01245026 CN01245026 CN 01245026 CN 01245026 U CN01245026 U CN 01245026U CN 2493270 Y CN2493270 Y CN 2493270Y
- Authority
- CN
- China
- Prior art keywords
- airtight container
- screen pack
- seal container
- guide shell
- chuck
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model relates to a multi-functional crystallization device for producing and manufacturing chemical products (such as fine chemicals, pharmaceutical, food, petrochemicals, etc.). The utility model is a seal container consisting of a jacket and a tank; one end of the seal container is provided with a guide cylinder inside; the guide cylinder is provided with a blade inside; the blade extending out of the seal container through a mixing shaft is connected with a motor; an inlet pipe through the seal container is communicated with the lower end of the internal cavity of the guide cylinder; one end of an outlet pipe is communicated with the upper end of the internal cavity of the guide cylinder and the other end with the internal cavity of the jacket; the other end of the seal container is provided with a screen; the corresponding end of the seal container to the screen is provided with a discharge port and a movable cover; the seal container is rotationally connected with a rotary bracket; and a dry washing vacuum tube and a heating cooled liquid inlet and outlet pipes communicated with the seal container are all out of the seal container trough the axes of the rotary bracket.
Description
Technical field:
The utility model relates to the multi-functional crystallization apparatus that a kind of chemical products (as fine chemistry industry, pharmacy, food, petrochemical industry etc.) are manufactured usefulness.
Background technology:
When human society entered the new century of kownledge economy, the development of sharp skill made social progress, industry innovation, has quickened economic development.Follow development of science and technology, just continuing to bring out out the new and high technology that some promote production development in industry-by-industry, field.And at chemical field, especially the low fine chemistry industry that drops into high production, the pharmaceutical industry of costly medicine, food, petrochemical industry, and be accompanied by poisonous, inflammable, explosive production operation process in producing and also wait to improve, need constantly employ new technology and high efficiency equipment replaces backward outmoded device.Though developed " three-in-one " equipment of some crystallizations, filtration, drying abroad, but its filter area is little, speed is slow, and drying is a rake formula Rotary drying, the destructible crystal, and discharging is difficulty, labour intensity is big, crystallization yield, product quality aspect are affected, and the cost height, every about 40-50 ten thousand U.S. dollars of overseas equipment introduced.
Summary of the invention:
The purpose of this utility model is exactly in order to address the above problem, and provides a kind of filter area big, and speed is fast, can not destroy crystal, and discharging is easy, the crystallization yield height, and reliable product quality and cost are low, multiple functional multi-functional crystallization apparatus.
Technical solution of the present utility model:
A kind of multi-functional crystallization apparatus, it includes the airtight container that is combined by chuck, tank body, it is characterized in that the end in the airtight container is provided with guide shell, be provided with blade in the guide shell, blade pass is crossed shaft and is stretched out airtight container and link to each other with motor, feed tube passes airtight container and is connected with guide shell inner chamber lower end, and drain pipe one end is connected with guide shell inner chamber upper end, and its other end is connected with the chuck inner chamber; The other end is established and is seen screen pack in the airtight container, the corresponding end of the airtight container of corresponding screen pack one end is provided with discharging opening and movable cap thereof, airtight container is rotatably connected on the swinging mounting, and the drying that is communicated with airtight container is washed vacuum tube and heated cooling fluid import and export Guan Jun draws outside the airtight container by the axle center of crossing swinging mounting.
The utility model is " five in one " multi-functional crystallization apparatus, has remedied the deficiency of domestic and international same category of device preferably.The utility model makes many production technologies link, effectively makes up by its characteristics, will concentrate well, several unit operations such as vacuum (cooling) crystallization, vacuum (pressurization) suction filtration, washing, drying are connected in the same table apparatus and finish.Not only reduce investment, the floor space of equipment, and stopped the run, drip, leak phenomenon of danger poisonous substance product in the production operation process.Simultaneously shortened the production operation cycle again.What is more important, the utility model can obtain higher yield and improve the quality of products, and reduces production costs, thereby increases economic benefit.
Description of drawings:
Fig. 1 is a structural representation of the present utility model.
The specific embodiment:
As Fig. 1, the utility model includes the airtight container 3 that is combined by chuck 1, tank body 2, end in the airtight container 3 is provided with guide shell 4, be provided with blade 5 in the guide shell 4, blade 5 stretches out airtight container 3 link to each other with motor 7 (motor 7 is connected on the chuck 1 by support) by shaft 6, feed tube 8 passes airtight container 3 and is connected with guide shell 4 inner chamber lower ends, and drain pipe 9 one ends are connected with guide shell 4 inner chambers upper end, and its other end is connected with chuck 1 inner chamber; The other end is provided with screen pack 10 in the airtight container 3, the corresponding end of the airtight container 3 of corresponding screen pack 10 1 ends is provided with discharging opening 11 and movable cap 12 thereof, airtight container 3 is rotatably connected on the swinging mounting 13, and the drying that is communicated with airtight container 3 is washed vacuum tube 14 and heated cooling fluid import and export pipe 15 is all drawn outside the airtight container 3 by the axle center of swinging mounting 13.
Guide shell 4 of the present utility model can be a cylinder barrel shaped, also can cone barrel, be provided with guide plate 16 in its sidewall inner chamber, and rise to guarantee the liquid spirals in the guide shell 4.Blade 5 in the guide shell 4 should be helical blade, is generally the 4-5 sheet.
Screen pack 10 in the utility model airtight container 3 can be a plane net, its two ends and tank body 2 inwall correspondence positions are connected, screen pack 10 is preferably the taper net, and its big opening end edge and tank body 2 correspondence position inwalls are connected, and its osculum end is positioned at discharging opening 11 places of airtight container 3.Be provided with center screen pack 17 at the middle part of screen pack 10, this center screen pack 17 is a cylinder, and it is connected discharging opening 11 places of airtight container 3 by connecting plate 18.Movable cap 12 is arranged on discharging opening 11 ports of airtight container 3, it links to each other with airtight container 3 by runing rest 19, runing rest 19 is made of straight-bar 20 and cross bar 21, straight-bar 20 1 ends are connected on chuck 1 end face, its other end and cross bar 21 1 ends are hinged, and cross bar 21 other ends are fixedlyed connected with the tube wall of suction filtration liquid vacuum tube 22 on being installed in movable cap 12.
Swinging mounting 13 of the present utility model is by two a upright bearing 23 and left sides, right two turning cylinders 24,25 constitute, two upright bearing 23 lower ends and ground are connected, their upper end by sliding bearing 26 separately respectively with a left side, right-hand rotation moving axis 24,25 link to each other, a left side, right-hand rotation moving axis 24,25 is hollow shaft, the inner of it all fixedlyed connected with 1 liang of middle side part outer wall of airtight container chuck, left-hand rotation moving axis 24 links to each other with drive motors by worm and gear 27, dry washing vacuum tube 14 the inners are positioned at airtight container 3, which is provided with shower nozzle 28, its pipeline passes left-hand rotation moving axis 24 and draws airtight container 3; Heated cooling fluid is imported and exported pipe 15 the inners and is connected with chuck 1 inner chamber, and its pipeline passes right-hand rotation moving axis 25 and draws airtight container 3.
The course of work of the present utility model is as follows:
1, when shaft 6 is positioned at airtight container 3 lower ends and airtight container 3 and leaves standstill, carry out the reactive crystallization unit operations, at this moment, open suction filtration liquid vacuum tube 22 valves, make processed material (as chemical industry, food, materials such as medicine) enter in the airtight container 3 by suction filtration liquid vacuum tube 22 and screen pack 10, starter motor 7 rotates shaft 6 then, shaft 6 drives 5 pairs of materials of helical blade and stirs, for different materials, different treatment temperature requirements is arranged, add hot water or cold water by feed tube 8 and drain pipe 9 this moment as required, makes material finish reaction crystallization process.If when some material needs to concentrate in reaction crystallization process, then the suction filtration liquid vacuum tube 22 on the movable cap 12 is connected with the vacuum machine, material is carried out vacuum concentrate.
When 2, after the material crystallization, changing filter operation over to, start earlier drive motors by worm and gear 27 and turn left and right axle 24,25 airtight container 3 Rotate 180 degree are stopped, this moment, the screen pack 10 and the discharging opening 11 of airtight container 3 were positioned at the lower end, then the suction filtration liquid vacuum tube on the movable cap 12 22 is connected the vacuum machine, material after the crystallization is carried out suction filtration, liquid in the material is drawn out of by screen pack 10 and center screen pack 17, and the crystal in the material is stayed in the airtight container 3.
3, filter operation is promptly carried out washing operation after finishing, and cleaning solution enters in the airtight container 3 by drying washing vacuum tube 14, and from its shower nozzle 28 ejections crystallized stock is washed.
4, washing is carried out drying process again after finishing, open drive motors again, by worm and gear 27 and turn left and right axle and 24,25 make airtight container 3 be in continuous rotation status, simultaneously, open dry washing vacuum tube 14, the steam in the airtight container 3 is drawn out of, stop operating after crystallized stock drying in airtight container 3 is qualified, should make simultaneously airtight container 3 still stop at discharging opening 11 under the position, this moment can open movable cap 12, take out qualified finished product materials.
Claims (6)
1, a kind of multi-functional crystallization apparatus, it includes the airtight container that is combined by chuck, tank body, it is characterized in that the end in the airtight container is provided with guide shell, be provided with blade in the guide shell, blade pass is crossed shaft and is stretched out airtight container and link to each other with motor, feed tube passes airtight container and is connected with guide shell inner chamber lower end, and drain pipe one end is connected with guide shell inner chamber upper end, and its other end is connected with the chuck inner chamber; The other end is provided with screen pack in the airtight container, the corresponding end of the airtight container of corresponding screen pack one end is provided with discharging opening and movable cap thereof, airtight container is rotatably connected on the swinging mounting, and the drying that is communicated with airtight container is washed vacuum tube and heated cooling fluid import and export Guan Jun draws outside the airtight container by the axle center of swinging mounting.
2, by the described multi-functional crystallization apparatus of claim 1, it is characterized in that described guide shell or cylinder barrel shaped, or cone barrel, being provided with guide plate in its sidewall inner chamber, the blade in the guide shell should be helical blade, and its sheet number is the 4-5 sheet.
3, by the described multi-functional crystallization apparatus of claim 1, it is characterized in that screen pack or plane net in the described airtight container, its two ends and inner tank wall correspondence position are connected.
4, by the described multi-functional crystallization apparatus of claim 1, it is characterized in that the screen pack in the described airtight container is the taper net, its big opening end edge and tank body correspondence position inwall are connected, its osculum end is positioned at the discharging opening place of airtight container, be provided with the center screen pack at the middle part of screen pack, this center screen pack is a cylinder, and it is connected the discharging opening place of airtight container by connecting plate.
5, by the described multi-functional crystallization apparatus of claim 1, it is characterized in that described movable cap is arranged on the discharging opening port place of airtight container, it links to each other with airtight container by runing rest, runing rest is made of straight-bar and cross bar, straight-bar one end is connected on the chuck end face, its other end and cross bar one end are hinged, and the cross bar other end is fixedlyed connected with the tube wall that is installed in the suction filtration liquid vacuum tube that moveable cap covers.
6, by the described multi-functional crystallization apparatus of claim 1, it is characterized in that described swinging mounting is by two a upright bearing and left sides, right two turning cylinders constitute, two upright bearing lower ends and ground are connected, their upper end by sliding bearing separately respectively with a left side, the right-hand rotation moving axis links to each other, a left side, the right-hand rotation moving axis is a hollow shaft, the inner of it all fixedlyed connected with airtight container chuck two middle side part outer walls, the left-hand rotation moving axis links to each other with drive motors by worm and gear, dry washing vacuum tube the inner is positioned at airtight container, which is provided with shower nozzle, its pipeline passes the left-hand rotation moving axis and draws airtight container; Heated cooling fluid is imported and exported pipe the inner and is connected with the chuck inner chamber, and its pipeline passes the right-hand rotation moving axis and draws airtight container.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 01245026 CN2493270Y (en) | 2001-07-25 | 2001-07-25 | Multi-function crystallizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 01245026 CN2493270Y (en) | 2001-07-25 | 2001-07-25 | Multi-function crystallizer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2493270Y true CN2493270Y (en) | 2002-05-29 |
Family
ID=33656342
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 01245026 Expired - Fee Related CN2493270Y (en) | 2001-07-25 | 2001-07-25 | Multi-function crystallizer |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2493270Y (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100393419C (en) * | 2002-04-10 | 2008-06-11 | 佳能株式会社 | Method for disintegrating container containing powder and disintegrator |
| CN102085423A (en) * | 2010-04-29 | 2011-06-08 | 杨志勇 | Totally-enclosed multifunctional crystallization product producing device |
| CN102614698A (en) * | 2012-02-06 | 2012-08-01 | 张家兴 | Four-in-one multifunctional machine |
| CN103949083A (en) * | 2014-05-07 | 2014-07-30 | 无锡市张华医药设备有限公司 | Crystallization tank |
-
2001
- 2001-07-25 CN CN 01245026 patent/CN2493270Y/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100393419C (en) * | 2002-04-10 | 2008-06-11 | 佳能株式会社 | Method for disintegrating container containing powder and disintegrator |
| CN102085423A (en) * | 2010-04-29 | 2011-06-08 | 杨志勇 | Totally-enclosed multifunctional crystallization product producing device |
| CN102614698A (en) * | 2012-02-06 | 2012-08-01 | 张家兴 | Four-in-one multifunctional machine |
| CN103949083A (en) * | 2014-05-07 | 2014-07-30 | 无锡市张华医药设备有限公司 | Crystallization tank |
| CN103949083B (en) * | 2014-05-07 | 2016-04-20 | 无锡市张华医药设备有限公司 | A kind of crystallizing tank |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20020529 Termination date: 20100725 |