CN2335976Y - High purity metallic magnesium distillator - Google Patents
High purity metallic magnesium distillator Download PDFInfo
- Publication number
- CN2335976Y CN2335976Y CN 98237570 CN98237570U CN2335976Y CN 2335976 Y CN2335976 Y CN 2335976Y CN 98237570 CN98237570 CN 98237570 CN 98237570 U CN98237570 U CN 98237570U CN 2335976 Y CN2335976 Y CN 2335976Y
- Authority
- CN
- China
- Prior art keywords
- distiller
- housed
- magnesium
- tube
- loam cake
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a high-purity metallic magnesium distiller. The utility model is characterized in that a shell body forms a cylinder shape; the bottom of the interior of the shell body is provided with a magnesium loading basket and a support frame; the upper part of the support frame is provided with the magnesium loading basket; the outside of the upper part of the shell body is provided with a support ring; an upper cover is provided with a vacuum-pumping pipe and two sleeve pipes; the middle sleeve pipe is a cooling water inlet pipe of a crystallizer; the outer sleeve pipe is a cooling water outlet pipe of the crystallizer; the ends of the water inlet pipe and the water outlet pipe are provided with circular cooling cavities; the lower parts of the cooling cavities are provided with circular crystallizers. The utility model has the advantages of simple structure, low manufacture cost, good sealing effect, high vacuum degree, uniform temperature, automatable operation and labor saving.
Description
The utility model relates to the light metal purifying plant, particularly a kind of producing high purity metal magnesium distiller.
The zirconium sponge of atomic level, hafnium sponge need to make reductive agent with producing high purity metal magnesium (99.99%) in purification process.Adopt the vacuum-sublimation method magnesium of purifying metals, crucial device is a vacuum distilling apparatus.The purify metals distiller of magnesium is not seen the report of pertinent data at present, and general distiller all is direct heating or indirect heating type, then with the material of purifying through distillation tower, cut product at condensation point.But the purification distillation of producing high purity metal magnesium, crystallization are finished in a distiller.
The purpose of this utility model is for the vacuum-sublimation method magnesium of purifying metals, and a kind of producing high purity metal magnesium distiller is provided.
The technical solution of the utility model summary.
A kind of producing high purity metal magnesium distiller, it is characterized in that: the distiller housing is the cylinder body, at distiller housing inner bottom part the magnesium holding basket ring holder is housed, the magnesium holding basket of skeleton construction is housed above the bracing frame, a basket hook is equipped with in the central position of magnesium holding basket, a screen cloth is put in the upper end of magnesium holding basket, the upper outside of distiller housing is provided with support ring, flange is equipped with in the upper end of distiller housing, and flange connects the distiller loam cake by bolt, and the top outside of flange is provided with sealing groove, sealing groove is built-in with rubber seal, the back side of flange is provided with cooling water channel down, and is provided with the turnover water-cooled tube in the corresponding position of rubber seal; The corresponding position of distiller loam cake and rubber seal is provided with annular and goes up cooling water channel, and the turnover water-cooled tube is arranged, and in the centre of the cooling water channel of water inlet pipe and water outlet pipe dividing plate is housed; Cover on distiller vacuum-pumping tube is housed, vacuum-pumping tube communicates with distiller, and below the distiller loam cake, " mountain " type baffle plate is equipped with in the below of vacuum-pumping tube; In the centre of distiller loam cake two-layer sleeve pipe is housed, intermediate casing is the cooling water inlet pipe of crystallizer, and outer tube is the cooling rising pipe of crystallizer, and circular cooling chamber is housed in the end of inlet tube and outlet tube, the distiller, circular crystallizer is housed below the cooling chamber; The loam cake of distiller also is provided with handle.When distiller was packed the distilling furnace internal heating into, support ring was stuck on the sealing rubber ring of distillation electric furnace, the unanimity of the inside and outside vacuum tightness of distiller can be realized in the space of sealing distiller and distillation electric furnace, had guaranteed distiller indeformable under the condition of high temperature.
Characteristics of the present utility model are collection distillers and crystallizer is integrated, simple in structure, cost of manufacture is low, good sealing effect, the vacuum tightness height, the good cooling results of crystallizer, temperature is even, but and automated operation, saved the labor force.
Fig. 1 is a producing high purity metal magnesium distiller structural front view.
Fig. 2 is a producing high purity metal magnesium distiller structure vertical view
Embodiment
Embodiment (see figure 1) of the present utility model, distiller housing 1 is the cylinder body, at distiller housing 1 inner bottom part magnesium holding basket ring holder 21 is housed, above the magnesium holding basket bracing frame 21, the magnesium holding basket 2 of skeleton construction is housed, basket hook 3 is equipped with in the central position of magnesium holding basket 2, a screen cloth 4 is put in the upper end of magnesium holding basket 2, and the upper outside of distiller housing 1 is provided with support ring 9, and flange 22 is equipped with in the upper end of distiller housing 1, flange 22 connects distiller loam cake 15 by bolt 13, the top outside of flange 22 is provided with sealing groove, and sealing groove is built-in with rubber seal 12, the back side of flange, be provided with cooling water channel 10 down in the corresponding position of rubber seal, and be provided with the turnover water-cooled tube; The corresponding position of distiller loam cake 15 and rubber seal 12 is provided with annular and goes up cooling water channel 14, and turnover water-cooled tube 17,18 is arranged, and in the centre of the cooling water channel 14 of water inlet pipe and water outlet pipe dividing plate 20 is housed; (see figure 2); Vacuum-pumping tube 16 is housed on distiller loam cake 15, and vacuum-pumping tube 16 communicates with distiller, and below distiller loam cake 15, " mountain " type baffle plate 11 is equipped with in the below of vacuum-pumping tube 16; In the centre of distiller loam cake 15 two-layer sleeve pipe is housed, intermediate casing is the cooling water inlet pipe 8 of crystallizer, outer tube is the cooling rising pipe 7 of crystallizer, in inlet tube and outlet tube 8,7 ends, the distiller circular cooling chamber 6 is housed, and circular crystallizer 5 is housed below the cooling chamber 6; The loam cake 15 of distiller also is provided with handle 19.When distiller was packed the distilling furnace internal heating into, support ring 9 was stuck on the sealing rubber ring of distilling furnace, the unanimity of vacuum tightness inside and outside the distiller can be realized in the space of sealing distiller and distilling furnace, had guaranteed distiller indeformable under the condition of high temperature.
Claims (1)
1. producing high purity metal magnesium distiller, it is characterized in that: the distiller housing is the cylinder body, at distiller housing inner bottom part the magnesium holding basket ring holder is housed, the magnesium holding basket of skeleton construction is housed above the bracing frame, a basket hook is equipped with in the central position of magnesium holding basket, a screen cloth is put in the upper end of magnesium holding basket, the upper outside of distiller housing is provided with support ring, flange is equipped with in the upper end of distiller housing, and flange connects the distiller loam cake by bolt, and the top outside of flange is provided with sealing groove, sealing groove is built-in with rubber seal, the back side of flange is provided with cooling water channel down, and is provided with the turnover water-cooled tube in the corresponding position of rubber seal; The corresponding position of distiller loam cake and rubber seal is provided with annular and goes up cooling water channel, and the turnover water-cooled tube is arranged, and in the centre of the cooling water channel of water inlet pipe and water outlet pipe dividing plate is housed; Cover on distiller vacuum-pumping tube is housed, vacuum-pumping tube communicates with distiller, and below the distiller loam cake, " mountain " type baffle plate is equipped with in the below of vacuum-pumping tube; In the centre of distiller loam cake two-layer sleeve pipe is housed, intermediate casing is the cooling water inlet pipe of crystallizer, and outer tube is the cooling rising pipe of crystallizer, and circular cooling chamber is housed in the end of inlet tube and outlet tube, the distiller, circular crystallizer is housed below the cooling chamber; The loam cake of distiller also is provided with handle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 98237570 CN2335976Y (en) | 1998-05-12 | 1998-05-12 | High purity metallic magnesium distillator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 98237570 CN2335976Y (en) | 1998-05-12 | 1998-05-12 | High purity metallic magnesium distillator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2335976Y true CN2335976Y (en) | 1999-09-01 |
Family
ID=33985361
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 98237570 Expired - Fee Related CN2335976Y (en) | 1998-05-12 | 1998-05-12 | High purity metallic magnesium distillator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2335976Y (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101386919B (en) * | 2008-10-24 | 2011-12-28 | 贵阳铝镁设计研究院有限公司 | High-pure magnesium preparation method and apparatus |
| CN102766769A (en) * | 2012-07-12 | 2012-11-07 | 东莞宜安科技股份有限公司 | Method for high-vacuum low-temperature purification of high-purity magnesium and purification device |
| CN109536709A (en) * | 2019-01-02 | 2019-03-29 | 北京科技大学 | A kind of improved metal magnesium, calcium smelt the cooling section for using reductive jar |
| CN109957654A (en) * | 2019-03-12 | 2019-07-02 | 济源市中亿科技有限公司 | A kind of steaming arsenic tank |
-
1998
- 1998-05-12 CN CN 98237570 patent/CN2335976Y/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101386919B (en) * | 2008-10-24 | 2011-12-28 | 贵阳铝镁设计研究院有限公司 | High-pure magnesium preparation method and apparatus |
| CN102766769A (en) * | 2012-07-12 | 2012-11-07 | 东莞宜安科技股份有限公司 | Method for high-vacuum low-temperature purification of high-purity magnesium and purification device |
| CN102766769B (en) * | 2012-07-12 | 2014-08-06 | 东莞宜安科技股份有限公司 | Method for high-vacuum low-temperature purification of high-purity magnesium and purification device |
| CN109536709A (en) * | 2019-01-02 | 2019-03-29 | 北京科技大学 | A kind of improved metal magnesium, calcium smelt the cooling section for using reductive jar |
| CN109957654A (en) * | 2019-03-12 | 2019-07-02 | 济源市中亿科技有限公司 | A kind of steaming arsenic tank |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |