CN2213998Y - Pre-treatment device of gas analyse instrument - Google Patents

Pre-treatment device of gas analyse instrument Download PDF

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Publication number
CN2213998Y
CN2213998Y CN 94241427 CN94241427U CN2213998Y CN 2213998 Y CN2213998 Y CN 2213998Y CN 94241427 CN94241427 CN 94241427 CN 94241427 U CN94241427 U CN 94241427U CN 2213998 Y CN2213998 Y CN 2213998Y
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CN
China
Prior art keywords
jar
stabilivolt
gas
sampling
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 94241427
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Chinese (zh)
Inventor
宋传庠
肖吉刚
刘征强
许江南
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WEIFANG PURE ALKALI FACTORY SHANDONG PROV
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WEIFANG PURE ALKALI FACTORY SHANDONG PROV
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Publication date
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Priority to CN 94241427 priority Critical patent/CN2213998Y/en
Application granted granted Critical
Publication of CN2213998Y publication Critical patent/CN2213998Y/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model relates to the pre-treatment device of gas analyse instrument, which comprises a sampling probe, a liquid scrubbing implement, a condenser, a drying pot, a flow regulating valve, and a filter paper which are connected parallelly and orderly; the sampling probe comprises a sampling flange, a sampling pipe and a heat tracing steam pipe; the outlet of the heat tracing steam pipe is inserted into the inlet of the sampling pipe; the liquid scrubbing implement is provided with an inner pot, an outer pot and a T-shaped stabilivolt; the outer pot is an open type; one end of the upper part of the T-shaped stabilivolt is communicated with an air outlet duct; the other end of the T-shaped stabilivolt is a liquid level measuring hole; the bottom of the T-shaped stabilivolt is inserted under the liquid surface. The utility model can not be plugged easily, and the voltage regulation effect is good. The utility model can be used for the pre-treatment aspect before the gas with harmful substances is analysed.

Description

Pre-treatment device of gas analyse instrument
The utility model relates to the pretreatment unit of being washed the gas analysis instrument that device, condenser, drying chamber, throttling valve, filter paper form by sampling probe, liquid.
The QGS-08 infrared analyzer pretreatment unit that Beijing Analytical Instrument Factory produces comprises that sampling probe, the liquid of series connection are washed device, condenser, drying chamber, throttling valve, filter paper successively, sampling probe is with steam tracing by stopple coupon, stopple coupon periphery on sampling flange, the sampling flange and forms, this sampling probe can not guarantee the temperature of sample gas, easily make sample gas in stopple coupon, separate out crystallization, thereby cause sampling line to stop up.The sample tracheae that liquid is washed device has three branch roads, and first branch road connects U-tube manometer, the stabilivolt in second branch road is provided in a side of between jar and the outer jar, jar interior draft tube in the 3rd branch road is provided in a side of.The degree of depth that stabilivolt inserts in the washing lotion is darker than draft tube, and the stabilivolt bottom is mutually concordant with the discharging tube bottom, and interior tank top is provided with the outlet of sample gas, and the outer jar that this liquid is washed device seals.When analytic system pressure increases, sample gas is still discharged from draft tube in a large number, the sample gas of walking from stabilivolt seldom, the sample gas that comes out by stabilivolt enter the lotion pipeline drag-out wash device just still less, the pressure of this all gas outlet just increases along with the increase of system pressure, and stabilivolt does not play pressure stabilization function.Again because outer jar is sealed, the gas of being discharged by stabilivolt concentrates at outer tank top and air pressure is constantly risen, for reaching pressure equilibrium, and outer jar liquid level is descended, in jar liquid level rise, cause the sample gas carrying liquid or washing lotion is pressed onto the outlet of sample gas and can't supplies gas, though again through measures such as a series of condensation, dryings, part moisture is taken in the analysis meter, cause damage.
The pretreatment unit of the gas analysis instrument that the purpose of this utility model is exactly a kind of difficult obstruction of design, voltage regulation result is good.
The utility model comprises that successively sampling probe, the liquid of series connection washes device, condenser, exsiccator, throttling valve, filter paper, the closed circuit of measurement and control that this condenser comprises semiconductor condensation piece, lean against condenser pipe on the semiconductor condensation piece, form with semiconductor condensation piece; Drying chamber comprises that sample gas outlet is established on tank body, tank body top, the import of sample gas is established in the tank body bottom, it is characterized in that sampling probe comprises that the outlet of be fixedly connected on sampling flange, the sampling flange stopple coupon and steam tracing, steam tracing inserts in the import of stopple coupon; Liquid wash device comprise be provided with in the middle of outer jar, outer jar interior jar, outer jar top be provided with leakage fluid dram, outer jar bottom be provided with survey under the liquid level mouthful, outside jar and space one side of interior jar be provided with draft tube, opposite side be provided be connected to feed tube on T shape stabilivolt, the interior tank deck and escape pipe, T shape stabilivolt top one end communicate with escape pipe, the other end be survey mouth on the liquid level, below the bottom insertion liquid level.Enter the draft tube that liquid is washed device after the temperature and humidity of sample gas and steam raising sample gas, gas in interior jar with the washing lotion counter current contacting, remove harmful gas and impurity, sample gas after the purification, arrive condenser through escape pipe, make sample air cooling but and make the most of moisture in the sample gas be condensed into water, condensate water is in time discharged from the condenser pipe bottom, in drying chamber, further remove small amount of moisture through condensed sample gas, arrive the required flow of analysis meter through throttle valve control, by arriving analysis meter behind the filter paper elimination trace impurity.The utility model directly mixes with steam owing to sample gas, sample gas temperature and humidity improves fast and even, make sample gas avoid separating out crystallization, assurance stopple coupon and liquid are washed the draft tube of device and can not stopped up, the steam that is added is washed to cool off in the device at liquid and is become water, and the sample gas water cut after the purification can satisfy requirement of the present utility model.When analyzed system pressure raises, interior jar upper space and escape pipe, stabilivolt internal pressure also raise, and when it was increased to setting, a part of sample gas was discharged to the washing lotion from stabilivolt, after the washing lotion washing, enter atmosphere, be limited in the setting thereby use atmospheric pressure.The size of setting is inserted the degree of depth decision of washing lotion by stabilivolt.
So the utlity model has be difficult for to stop up, voltage regulation result is good, Failure analysis instrument not, the advantage that life cycle is long can be widely used in carrying out the pre-service aspect before the gas analysis that contains hazardous substance.
Fig. 1 is a block flow diagram of the present utility model;
Fig. 2 is the structural representation of sampling probe among Fig. 1 (1);
Fig. 3 is the structural representation that liquid is washed device (2) among Fig. 1;
Fig. 4 is the structural representation of condenser among Fig. 1 (3);
Fig. 5 is the structural representation of drying chamber among Fig. 1 (4).
Embodiment 1
The utility model comprises that successively sampling probe (1), the liquid of series connection washes device (2), condenser (3), drying chamber (4), throttling valve (5), filter paper (6), the closed circuit of measurement and control (9) that this condenser (3) comprises semiconductor condensation piece (7), lean against condenser pipe (8) on the semiconductor condensation piece (7), form with semiconductor condensation piece (7); Drying chamber (4) comprises that sample gas outlet (11) is established on tank body (10), tank body (10) top, sample gas import (12) is established in tank body (10) bottom, it is characterized in that sampling probe (1) comprises in the import of outlet insertion stopple coupon (14) of be fixedly connected on sampling flange (13), the sampling flange (13) stopple coupon (14) and steam tracing (15), steam tracing (15); Liquid is washed device (2) and is comprised outer jar (16), be provided with interior jar (17) in the middle of outer jar (16), outer jar (16) top is provided with leakage fluid dram (18), outer jar (a 16) bottom is provided with and surveys mouthful (19) under the liquid level, space one side of jar (16) and interior jar (17) is provided with draft tube (20) outside, opposite side is provided with T shape stabilivolt (21), be connected to feed tube (22) and escape pipe (23) on interior jar of (17) top, top one end of T shape stabilivolt (21) communicates with escape pipe (23), the other end is to survey mouthful (24) on the liquid level, insert below the liquid level bottom.Being fixedly connected to welding or screw connects of the utility model sampling flange (13) and stopple coupon (14) and steam tracing (15), washing lotion select for use sample gas do not allow therein to separate or hold separate less, harmful gas and impurity therein fully appearance separate or the washing lotion of Rong Xieda (can have chemical reaction).Drying agent is selected the solid drier that does not play physics or chemical reaction with sample gas for use.Drying chamber (4) is looked analysis meter and can be adopted two or more to the requirement of moisture.Throttling valve (5) requires gas of anti-sample the and washing lotion corrosion.Filter paper (6) can be selected common filter paper for use.Circuit of measurement and control (9) is regulated condensation number by the temperature of platinum resistance (25) perception semiconductor condensation piece (7) by control circuit (26).
Embodiment 2
Aforesaid outer jar (16) are open type.Outer jar (16) can also can establish a lid that has aperture by uncovered, are convenient to unnecessary sample gas and enter atmosphere, and keeping outer jar (16) middle liquid level pressure is atmospheric pressure, guarantees voltage regulation result of the present utility model.All the other are with described in the embodiment 1.
Embodiment 3
Aforesaid steam tracing (15) is L shaped.Steam is consistent with the flow direction of sample gas like this, the pressure of sample gas and the pressure of combination gas are proportional, and the mixture pressure that obtains is big, and impurity is free settling not, bring liquid at an easy rate into and wash in the device (2), guarantee that stopple coupon (14) and draft tube (20) are difficult for stopping up.All the other are with described in the embodiment 1.
Embodiment 4
Aforesaid draft tube (20) is L shaped.Air inlet and washing lotion counter current contacting guarantee that the objectionable impurities in the gas is all removed like this, avoid the Failure analysis instrument.All the other are with described in the embodiment 1

Claims (4)

1, a kind of pretreatment unit of gas analysis instrument, it comprises that successively sampling probe (1), the liquid of series connection washes device (2), condenser (3), drying chamber (4), throttling valve (5), filter paper (6), the closed circuit of measurement and control (9) that this condenser (3) comprises semiconductor condensation piece (7), lean against condenser pipe (8) on the semiconductor condensation piece (7), form with semiconductor condensation piece (7); Drying chamber (4) comprises that sample gas outlet (11) is established on tank body (10), tank body (10) top, sample gas import (12) is established in tank body (10) bottom, it is characterized in that sampling probe (1) comprises in the import of outlet insertion stopple coupon (14) of be fixedly connected on sampling flange (13), the sampling flange (13) stopple coupon (14) and steam tracing (15), steam tracing (15); Liquid is washed device (2) and is comprised outer jar (16), be provided with interior jar (17) in the middle of outer jar (16), outer jar (16) top is provided with leakage fluid dram (18), outer jar (a 16) bottom is provided with and surveys mouthful (19) under the liquid level, space one side of jar (16) and interior jar (17) is provided with draft tube (20) outside, opposite side is provided with T shape stabilivolt (21), be connected to feed tube (22) and escape pipe (23) on interior jar of (17) top, top one end of T shape stabilivolt (21) communicates with escape pipe (23), the other end is to survey mouthful (24) on the liquid level, insert below the liquid level bottom.
2, jar (16) were open type outside the pretreatment unit of gas analysis instrument according to claim 1, its feature also were.
3, the pretreatment unit of gas analysis instrument according to claim 1, its feature are that also steam tracing (15) is for L shaped.
4, the pretreatment unit of gas analysis instrument according to claim 1, its feature are that also draft tube (20) is for L shaped.
CN 94241427 1994-09-16 1994-09-16 Pre-treatment device of gas analyse instrument Expired - Fee Related CN2213998Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 94241427 CN2213998Y (en) 1994-09-16 1994-09-16 Pre-treatment device of gas analyse instrument

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 94241427 CN2213998Y (en) 1994-09-16 1994-09-16 Pre-treatment device of gas analyse instrument

Publications (1)

Publication Number Publication Date
CN2213998Y true CN2213998Y (en) 1995-11-29

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN 94241427 Expired - Fee Related CN2213998Y (en) 1994-09-16 1994-09-16 Pre-treatment device of gas analyse instrument

Country Status (1)

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CN (1) CN2213998Y (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102445367A (en) * 2010-10-13 2012-05-09 中国石油化工股份有限公司 Pretreatment system used for gas on-line analysis

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102445367A (en) * 2010-10-13 2012-05-09 中国石油化工股份有限公司 Pretreatment system used for gas on-line analysis

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GR01 Patent grant
C19 Lapse of patent right due to non-payment of the annual fee
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