CN220758013U - Distillation plant is used in production of hydrogen peroxide di-tert-butyl isopropyl benzene - Google Patents
Distillation plant is used in production of hydrogen peroxide di-tert-butyl isopropyl benzene Download PDFInfo
- Publication number
- CN220758013U CN220758013U CN202322378881.8U CN202322378881U CN220758013U CN 220758013 U CN220758013 U CN 220758013U CN 202322378881 U CN202322378881 U CN 202322378881U CN 220758013 U CN220758013 U CN 220758013U
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- distillation
- vat
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- fixed mounting
- heating
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- 238000004821 distillation Methods 0.000 title claims abstract description 72
- IQDYJTRQXOFUGA-UHFFFAOYSA-N 1,2-ditert-butyl-3-propan-2-ylbenzene hydrogen peroxide Chemical compound OO.CC(C)C1=CC=CC(C(C)(C)C)=C1C(C)(C)C IQDYJTRQXOFUGA-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 8
- 239000000463 material Substances 0.000 claims abstract description 52
- 238000003756 stirring Methods 0.000 claims abstract description 33
- 238000010438 heat treatment Methods 0.000 claims abstract description 24
- 238000001816 cooling Methods 0.000 claims description 35
- 239000002893 slag Substances 0.000 claims description 7
- 230000002146 bilateral effect Effects 0.000 claims description 3
- 239000003818 cinder Substances 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 4
- 238000002156 mixing Methods 0.000 description 7
- 238000009833 condensation Methods 0.000 description 5
- 230000005494 condensation Effects 0.000 description 5
- 239000007787 solid Substances 0.000 description 4
- 238000007599 discharging Methods 0.000 description 3
- 230000009977 dual effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
Classifications
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a distillation device for producing di-tert-butyl isopropyl benzene hydrogen peroxide, and relates to the technical field of distillation devices. This distillation plant is used in production of hydrogen peroxide di-tert-butyl isopropyl benzene through setting up heating vat, the distillation vat, material stirring subassembly and row's cinder notch, after throwing into the distillation vat with the material from the feed inlet, can open material stirring subassembly and heating vat, make material stirring subassembly can stir the material at heating vat heating in-process, with material evenly mix together, can look over the inside condition of distillation vat through setting up the observation window, so that in time handle the problem, the row's cinder notch sets up in the distillation vat bottom, can conveniently discharge unnecessary material, avoid the material to mix with the material that subsequently newly adds and influence material purity, thereby improve distillation efficiency, set up first splint and second splint in first standing groove and second standing groove, can hold the container, avoid the container to empty.
Description
Technical Field
The utility model relates to the technical field of distillation devices, in particular to a distillation device for producing di-tert-butylcumene hydroperoxide.
Background
Di-tert-butylcumene hydroperoxide is a white to pale yellow powder or solid having strong oxidizing properties and is subjected to a series of processing steps including distillation and purification of the material by distillation equipment during the production of the di-tert-butylcumene hydroperoxide.
At present, a high-strength distillation device is generally selected for distillation of the di-tert-butylcumene hydroperoxide, materials are required to be mixed and stirred uniformly before distillation, but the existing distillation device does not have a material stirring function, is not very convenient to clean, most of the materials are stirred uniformly and then poured into the distillation device, stirring and distillation cannot be combined together, meanwhile, some materials are deposited at the bottom, the subsequent cleaning is not very convenient, the purity of distillation can be affected to a certain extent, and the distillation efficiency is low.
Disclosure of Invention
Aiming at the defects of the prior art, the utility model provides a distillation device for producing hydrogen peroxide di-tert-butyl isopropyl benzene, which solves the problem of low distillation efficiency of the distillation device.
In order to achieve the above purpose, the utility model is realized by the following technical scheme: the utility model provides a distillation plant is used in production of hydrogen peroxide di-tert-butylcumene, includes the workstation, workstation upside fixed mounting has first backup pad, first backup pad upside fixed mounting has the heating vat, the inside fixed mounting of heating vat has the distillation vat, distillation vat downside fixed mounting has the slag tap, slag tap externally mounted has manual valve, the material mixing subassembly is installed to distillation vat upside, material mixing subassembly front side is provided with the feed inlet, first backup pad right side is provided with the second backup pad, second backup pad upside fixed mounting has the cooling sleeve, cooling sleeve upside installs radiator fan through the bolt, cooling sleeve outside fixed mounting has evenly distributed's fin, cooling sleeve upper end fixed mounting has the distillation tube, distillation tube lower extreme fixedly connected with spiral condensing duct, spiral condensing duct end fixedly connected with drain pipe, first standing groove internally mounted has first standing groove, first standing groove right side is provided with the feed inlet with the second backup pad corresponding, second standing groove and inside is provided with the second cooling sleeve, the inside is provided with the control panel, the inside is provided with the cooling sleeve on the cooling sleeve top, the cooling sleeve front side is provided with the cooling panel.
Preferably, the upper surface of the distillation barrel is fixedly provided with a connecting sleeve, and the end part of the distillation pipe is detachably arranged on the connecting sleeve.
Preferably, a fixing ring is fixedly arranged in the cooling sleeve, and the cooling fan is arranged on the upper side of the fixing ring.
Preferably, the material stirring assembly comprises a driving motor, and a first electric push rod is arranged on an output shaft of the driving motor.
Further, a stirring shaft is fixedly arranged at the lower end of the first electric push rod, and stirring paddles which are uniformly distributed are fixedly arranged on the stirring shaft.
Preferably, the first clamping plate and the second clamping plate are both provided with two groups, and the first clamping plate and the second clamping plate are both distributed in bilateral symmetry.
Preferably, the first clamping plate is fixedly provided with a second electric push rod, the second clamping plate is fixedly provided with a third electric push rod, and the second electric push rod and the third electric push rod are fixedly arranged inside the workbench.
Advantageous effects
The utility model provides a distillation device for producing di-tert-butylcumene hydroperoxide. Compared with the prior art, the method has the following beneficial effects:
1. this distillation plant is used in production of hydrogen peroxide di-tert-butyl isopropyl benzene through setting up heating vat, distillation vat, material stirring subassembly and row's cinder notch, drops into the distillation vat with the material from the feed inlet after, can open material stirring subassembly and heating vat for material stirring subassembly can stir the material at heating vat heating in-process, and evenly mix the material together, can look over the inside condition of distillation vat through setting up the observation window, so that in time handle the problem, arrange the cinder notch and set up in distillation vat bottom, can conveniently discharge unnecessary material, avoid material and follow-up newly added material to mix and influence material purity, thereby improve distillation efficiency.
2. This distillation plant is used in production of hydrogen peroxide di-tert-butyl isopropyl benzene through setting up cooling sleeve, radiator fan and fin, can play dual radiating effect for vapor material condensation in the spiral condensation pipeline has set up first splint and second splint in first standing groove and second standing groove simultaneously, can hold the container, avoids the container to empty.
Drawings
FIG. 1 is a schematic diagram of the structure of the present utility model;
FIG. 2 is a schematic view of a cooling jacket according to the present utility model;
FIG. 3 is a schematic view of the structure of the first clamping plate according to the present utility model;
FIG. 4 is a schematic view of a material stirring assembly according to the present utility model.
In the figure: 1. a work table; 2. a first support plate; 3. heating the barrel; 4. a distillation barrel; 5. a material stirring assembly; 501. a driving motor; 502. a first electric push rod; 503. a stirring shaft; 504. stirring paddles; 6. a feed inlet; 7. a second support plate; 8. cooling the sleeve; 9. a heat radiation fan; 10. a heat sink; 11. a distillation tube; 12. a first placement groove; 13. a first clamping plate; 14. a second placement groove; 15. a second clamping plate; 16. a second electric push rod; 17. a fixing ring; 18. a spiral condensing pipeline; 19. a liquid outlet pipe; 20. and an observation window.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Referring to fig. 1-4, the present utility model provides a technical solution: a distillation device for producing hydrogen peroxide di-tert-butylcumene comprises a workbench 1, a first supporting plate 2 is fixedly arranged on the upper side of the workbench 1, a heating barrel 3 is fixedly arranged on the upper side of the first supporting plate 2, the heating barrel 3 can be used for heating, a distillation barrel 4 is fixedly arranged in the heating barrel 3, a slag discharging port is fixedly arranged on the lower side of the distillation barrel 4, a manual valve is arranged outside the slag discharging port, the slag discharging port is arranged at the bottom of the distillation barrel 4, the unnecessary materials can be conveniently discharged, the influence on the purity of the materials caused by the mixing of the materials with the materials newly added materials is avoided, a material stirring assembly 5 is arranged on the upper side of the distillation barrel 4, a feed port 6 is arranged on the front side of the material stirring assembly 5, a second supporting plate 7 is arranged on the right side of the first supporting plate 2, a cooling sleeve 8 is fixedly arranged on the upper side of the second supporting plate 7, a cooling fan 9 is arranged on the upper side of the cooling sleeve 8 through bolts, the cooling sleeve 8 is fixedly provided with uniformly distributed cooling fins 10 outside, the upper end of the cooling sleeve 8 is fixedly provided with a distillation tube 11, the cooling sleeve 8 can play a role of dual heat dissipation by arranging a cooling fan 9 and the cooling fins 10, the vapor materials in a spiral condensation pipeline 18 are accelerated to be condensed, the lower end of the distillation tube 11 is fixedly connected with the spiral condensation pipeline 18, the tail end of the spiral condensation pipeline 18 is fixedly connected with a liquid outlet pipe 19, the surface of the workbench 1 is provided with a first placing groove 12, the inside of the first placing groove 12 is fixedly provided with a first clamping plate 13, the right side of the first placing groove 12 is provided with a second placing groove 14 corresponding to the second supporting plate 7, the inside of the second placing groove 14 is provided with a second clamping plate 15, the workbench 1 is provided with a control panel, the front sides of the heating barrel 3 and the distillation barrel 4 are provided with observation windows 20, the inside of the distillation barrel 4 can be checked through the observation windows 20, so as to deal with the problem in time.
The upper surface fixed mounting of distilling vat 4 has the adapter sleeve, distillation tube 11 tip detachable installs on the adapter sleeve, cooling sleeve 8 inside fixed mounting has solid fixed ring 17, through setting up solid fixed ring 17, can avoid radiator fan 9 to fall down, radiator fan 9 sets up in solid fixed ring 17 upside, material stirring subassembly 5 includes driving motor 501, driving motor 501's output shaft is provided with first electric putter 502, first electric putter 502 lower extreme fixed mounting has (mixing) shaft 503, can drive first electric putter 502 through driving motor 501 and rotate, first electric putter 502 can drive (mixing) shaft 503 reciprocates, evenly distributed's stirring paddle 504 on the (mixing) shaft 503, stirring paddle 504 can be in the rotation in-process with the material evenly mixed together, first splint 13 and second splint 15 all are provided with two sets of, and first splint 13 and second splint 15 all are bilateral symmetry and distribute, first splint 13 outside fixed mounting has second electric putter 16, second splint 15 outside fixed mounting has the third electric putter, second electric putter 16 and third electric putter fixed mounting are inside workstation 1, through setting up second electric putter 16 and third electric putter, can avoid the container to empty with the second electric putter, thereby it takes place to empty container to empty or loosen to empty with the second splint 15.
During operation, firstly throw into the material from feed inlet 6 distillation barrel 4, then open driving motor 501 and first electric putter 502 in the material stirring subassembly 5, open the heating element in the heating barrel 3 simultaneously and heat distillation barrel 4, driving motor 501 rotates and drives first electric putter 502 and rotate, thereby drive (mixing) shaft 503 and stirring paddle 504 and rotate, make stirring paddle 504 stir the material in the heating process of heating barrel 3, evenly mix the material together, can look over the inside condition of distillation barrel 4 through setting up viewing window 20, so that in time handle the problem, the sediment mouth sets up in distillation barrel 4 bottom, can conveniently discharge unnecessary material, avoid material and follow-up newly added material to mix and influence material purity, thereby improve distillation efficiency.
And all that is not described in detail in this specification is well known to those skilled in the art.
Claims (7)
1. The utility model provides a distillation plant is used in production of hydrogen peroxide di-tert-butyl isopropyl benzene, includes workstation (1), its characterized in that: the utility model discloses a cooling device, including workstation (1) and cooling sleeve (8), workstation (1) front side fixed mounting has first backup pad (2), first backup pad (2) upside fixed mounting has heating vat (3), inside fixed mounting of heating vat (3) has distillation vat (4), distillation vat (4) downside fixed mounting has the slag tap, slag tap externally mounted has manual valve, material stirring subassembly (5) are installed to distillation vat (4) upside, material stirring subassembly (5) front side is provided with feed inlet (6), first backup pad (2) right side is provided with second backup pad (7), second backup pad (7) upside fixed mounting has cooling sleeve (8), cooling sleeve (8) upside is through bolt mounting radiator fan (9), cooling sleeve (8) outside fixed mounting has evenly distributed's fin (10), cooling sleeve (8) upper end fixed mounting has distillation tube (11), distillation tube (11) lower extreme fixedly connected with spiral condensing duct (18), spiral condensing duct (18) end fixed connection has feed inlet (6), second backup pad (7) upside fixed mounting has cooling sleeve (8), cooling sleeve (8) upside passes through the bolt mounting has radiator fan (9), cooling sleeve (8) outside fixed mounting has evenly distributed fin (11), the novel heating device is characterized in that a second placing groove (14) corresponding to the second supporting plate (7) is formed in the right side of the first placing groove (12), a second clamping plate (15) is arranged in the second placing groove (14), a control panel is arranged on the workbench (1), and an observation window (20) is formed in the front sides of the heating barrel (3) and the distilling barrel (4).
2. The distillation apparatus for producing di-tert-butylcumene hydroperoxide as set forth in claim 1, wherein: the upper surface of the distillation barrel (4) is fixedly provided with a connecting sleeve, and the end part of the distillation tube (11) is detachably arranged on the connecting sleeve.
3. The distillation apparatus for producing di-tert-butylcumene hydroperoxide as set forth in claim 1, wherein: the cooling sleeve (8) is internally and fixedly provided with a fixing ring (17), and the cooling fan (9) is arranged on the upper side of the fixing ring (17).
4. The distillation apparatus for producing di-tert-butylcumene hydroperoxide as set forth in claim 1, wherein: the material stirring assembly (5) comprises a driving motor (501), and a first electric push rod (502) is arranged on an output shaft of the driving motor (501).
5. The distillation apparatus for producing di-tert-butylcumene hydroperoxide as defined in claim 4, wherein: the stirring shaft (503) is fixedly arranged at the lower end of the first electric push rod (502), and stirring paddles (504) which are uniformly distributed are fixedly arranged on the stirring shaft (503).
6. The distillation apparatus for producing di-tert-butylcumene hydroperoxide as set forth in claim 1, wherein: the first clamping plate (13) and the second clamping plate (15) are respectively provided with two groups, and the first clamping plate (13) and the second clamping plate (15) are respectively distributed in bilateral symmetry.
7. The distillation apparatus for producing di-tert-butylcumene hydroperoxide as set forth in claim 1, wherein: the first clamping plate (13) is fixedly provided with a second electric push rod (16) outside, the second clamping plate (15) is fixedly provided with a third electric push rod outside, and the second electric push rod (16) and the third electric push rod are fixedly arranged inside the workbench (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322378881.8U CN220758013U (en) | 2023-09-01 | 2023-09-01 | Distillation plant is used in production of hydrogen peroxide di-tert-butyl isopropyl benzene |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322378881.8U CN220758013U (en) | 2023-09-01 | 2023-09-01 | Distillation plant is used in production of hydrogen peroxide di-tert-butyl isopropyl benzene |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220758013U true CN220758013U (en) | 2024-04-12 |
Family
ID=90597768
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202322378881.8U Active CN220758013U (en) | 2023-09-01 | 2023-09-01 | Distillation plant is used in production of hydrogen peroxide di-tert-butyl isopropyl benzene |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220758013U (en) |
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2023
- 2023-09-01 CN CN202322378881.8U patent/CN220758013U/en active Active
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