CN220676758U - Rotary evaporator for producing octyl triazone - Google Patents

Rotary evaporator for producing octyl triazone Download PDF

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Publication number
CN220676758U
CN220676758U CN202321107424.9U CN202321107424U CN220676758U CN 220676758 U CN220676758 U CN 220676758U CN 202321107424 U CN202321107424 U CN 202321107424U CN 220676758 U CN220676758 U CN 220676758U
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fixedly connected
pipe
heat exchange
rotary evaporator
connecting pipe
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CN202321107424.9U
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梁栋梁
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Hubei Artec Biotechnology Co ltd
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Hubei Artec Biotechnology Co ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

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Abstract

The utility model discloses a rotary evaporator for octyl triazone production, which comprises a base, wherein the top of the base is fixedly connected with a mounting cylinder, a lifting cylinder is inserted in the mounting cylinder in a sliding manner, the top of the lifting cylinder is fixedly connected with an adjusting box, the top of the adjusting box is fixedly connected with a heat exchange box, one side of the heat exchange box is fixedly connected with a condensing pipe, the bottom of the condensing pipe is fixedly connected with a first connecting pipe, and the first connecting pipe is communicated with the inside of the condensing pipe; this a rotary evaporator for octyl triazinone production can use the circulating pump to circulate cooling water inside spiral pipe and coiled pipe through the heat transfer mechanism who sets up to cooling water in the coiled pipe is cooled down through the flabellum that sets up, thereby quickens the heat transfer effect of cooling water, improves the condensation efficiency to steam.

Description

Rotary evaporator for producing octyl triazone
Technical Field
The utility model relates to the technical field of rotary evaporators, in particular to a rotary evaporator for producing octyl triazone.
Background
Octyl triazone is a novel ultraviolet absorber, has a large molecular structure and high ultraviolet absorption efficiency, has a broad-spectrum sun-screening effect, can be used as an additive in sun-screening products, is an oil-soluble absorber with the strongest UVB absorption capacity in the market today, has high light stability, prevents UVB-induced immunosuppression, has strong water resistance, has better affinity to skin keratin, and can be used in a rotary evaporator in the production of octyl triazone.
The utility model discloses a rotary evaporator for producing paranitrochlorobenzene, which comprises an installation table, wherein a steaming bath device is fixedly arranged on the right side of the installation table, a steaming bath pot is arranged in the steaming bath device, a heat preservation part is arranged above the steaming bath pot, a mounting frame is fixedly arranged on the upper end face of the installation table, and a lifting seat is arranged on the mounting frame.
However, the rotary evaporator has the following defects that when the rotary evaporator is used for processing octyl triazone, octyl triazone steam generated by distillation can be cooled and condensed through a condensing pipe, and the condensing efficiency of the steam is low due to low heat exchange efficiency of cooling water in the cooling pipe, so that the production efficiency is influenced.
To this end, the present utility model provides a rotary evaporator for octyl triazone production to solve the above-mentioned problems.
Disclosure of Invention
Aiming at the defects of the prior art, the utility model provides a rotary evaporator for producing octyl triazone, which solves the problems.
In order to achieve the above purpose, the utility model is realized by the following technical scheme: the rotary evaporator comprises a base, wherein a mounting cylinder is fixedly connected to the top of the base, a lifting cylinder is inserted in the mounting cylinder in a sliding manner, an adjusting box is fixedly connected to the top of the lifting cylinder, a heat exchange box is fixedly connected to the top of the adjusting box, a condensing pipe is fixedly connected to one side of the heat exchange box, a first connecting pipe is fixedly connected to the bottom end of the condensing pipe, the first connecting pipe is communicated with the interior of the condensing pipe, a middle through pipe is fixedly connected to the bottom end of the first connecting pipe, the middle through pipe is communicated with the interior of the first connecting pipe, and a heat exchange mechanism capable of improving the heat exchange effect of cooling water and accelerating the condensation efficiency of steam is arranged in the heat exchange box;
the heat exchange mechanism comprises a spiral pipe arranged in the condensing pipe, two ends of the spiral pipe are all extended into the heat exchange box, a circulating pump is fixedly connected to the inner wall of the top of the heat exchange box, a water inlet of the circulating pump is fixedly connected with one end of the spiral pipe, a water outlet of the circulating pump is fixedly connected with a coiled pipe, one end of the coiled pipe is fixedly connected with one end of the spiral pipe, two rotating shafts are rotatably and penetratingly connected to the inner wall of one side of the heat exchange box, and one end of each rotating shaft is fixedly connected with a fan blade.
Preferably, one side outer wall fixedly connected with protection casing of heat exchange box, in the one end of pivot extends to the protection casing, fixed cover is equipped with the linkage gear in the pivot, one side inner wall fixedly connected with first motor of protection casing, the output shaft fixedly connected with drive gear of first motor, drive gear all meshes with two linkage gears, and protection casing, linkage gear, first motor and the drive gear collocation convenient to use through setting up drive two flabellums to can conveniently cool down the cooling water in the coiled pipe.
Preferably, the top fixedly connected with steam bath ware of base, fixedly connected with steam bath pot on the steam bath ware, be connected with the air duct through rotating the piece through on the regulating box, in the one end rotation of air duct extends to well siphunculus, the one end that well siphunculus was kept away from to the air duct has the distillation flask through thread bush threaded connection, the distillation flask is located steam bath pot top, carries out distillation processing through steam bath ware, steam bath pot, air duct and the convenient to use of distillation flask collocation that sets up.
Preferably, the bottom fixedly connected with second connecting pipe of well siphunculus, the bottom of second connecting pipe is through threaded sleeve threaded connection there being the collecting bottle, fixedly connected with first solenoid valve on the second connecting pipe, fixedly connected with third connecting pipe on the well siphunculus, fixedly connected with second solenoid valve on the third connecting pipe, the top fixedly connected with aspiration pump of base, the air inlet fixedly connected with flexible hose of aspiration pump, in flexible hose's top extends to the third connecting pipe, produce the negative pressure in the second connecting pipe, collecting bottle, first solenoid valve, third connecting pipe, second solenoid valve, aspiration pump and flexible hose collocation convenient to use through setting up in the siphunculus to can carry the condenser intraductal with steam, carry the drop of water after the condensation to the collecting bottle in simultaneously.
Preferably, the bottom inner wall fixedly connected with second motor of installation section of thick bamboo, the output shaft fixedly connected with threaded rod of second motor, the top screw thread of threaded rod extends to in the lift section of thick bamboo, and the second motor and the threaded rod collocation convenient to use through setting drive the lift section of thick bamboo and remove, conveniently adjust the distillation column height.
Preferably, the fixed cover is equipped with driven conical gear on the air duct, the fixedly connected with third motor in the regulating box, the output shaft fixedly connected with initiative conical gear of third motor, initiative conical gear and driven conical gear meshing drive the air duct through driven conical gear, third motor and the initiative conical gear collocation convenient to use that sets up and rotate to make the distillation flask can rotate at the uniform velocity, conveniently heat its inside solution.
Preferably, the spout has been seted up in the installation section of thick bamboo, the outer wall fixedly connected with gag lever post of lift section of thick bamboo, the one end of gag lever post slides and extends to in the spout that corresponds, and the spout and the gag lever post collocation convenient to use through setting up carry out spacingly to the lift section of thick bamboo, avoid it to take place to rotate or break away from with the installation section of thick bamboo.
Preferably, fixedly connected with filling tube on the air duct, fixedly connected with third solenoid valve on the filling tube, through the filling tube that sets up and the cooperation of third solenoid valve use can conveniently add octyl triazinone solution to the distillation flask inside, facilitate production.
Advantageous effects
The utility model provides a rotary evaporator for producing octyl triazone. Compared with the prior art, the method has the following beneficial effects:
(1) This a rotary evaporator for octyl triazinone production can use the circulating pump to circulate cooling water in spiral pipe and coiled pipe inside through the heat transfer mechanism who sets up to cooling water in the coiled pipe through the flabellum that sets up lowers the temperature, thereby quickens the heat transfer effect of cooling water, improves the condensation efficiency to steam.
(2) This a rotary evaporator for octyl triazinone production can be adjusted the height of distillation flask through the lift section of thick bamboo that sets up, and the air duct can drive the distillation flask simultaneously and rotate to can carry out even heating to inside solution, accelerate production efficiency.
Drawings
FIG. 1 is a perspective view of the external structure of the present utility model;
FIG. 2 is a schematic elevational cross-sectional view of the present utility model;
FIG. 3 is a schematic view of the structure of the shaft, fan blades, linkage gear, first motor and driving gear in the present utility model;
fig. 4 is an assembly view of a circulation pump, a serpentine tube, a rotating shaft, a fan blade, a shield, a linkage gear, a first motor and a driving gear according to the present utility model.
In the figure: 1. a base; 2. a mounting cylinder; 3. a lifting cylinder; 4. an adjusting box; 5. a heat exchange box; 6. a condensing tube; 7. a first connection pipe; 8. a middle through pipe; 9. a spiral tube; 10. a circulation pump; 11. a serpentine tube; 12. a rotating shaft; 13. a fan blade; 14. a protective cover; 15. a linkage gear; 16. a first motor; 17. a drive gear; 18. steaming and bathing device; 19. a steam bath pot; 20. an air duct; 21. a distillation flask; 22. a second connection pipe; 23. a collection bottle; 24. a first electromagnetic valve; 25. a third connection pipe; 26. a second electromagnetic valve; 27. an air extracting pump; 28. a flexible hose; 29. a second motor; 30. a threaded rod; 31. a driven bevel gear; 32. a third motor; 33. a driving bevel gear; 34. a chute; 35. a limit rod; 36. a liquid adding tube; 37. and a third solenoid valve.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Embodiment one:
referring to fig. 1, 3 and 4, a rotary evaporator for producing octyl triazone comprises a base 1, wherein the top of the base 1 is fixedly connected with a mounting cylinder 2, a lifting cylinder 3 is inserted in the mounting cylinder 2 in a sliding manner, the top of the lifting cylinder 3 is fixedly connected with an adjusting box 4, the top of the adjusting box 4 is fixedly connected with a heat exchange box 5, one side of the heat exchange box 5 is fixedly connected with a condensing tube 6, the bottom end of the condensing tube 6 is fixedly connected with a first connecting tube 7, the first connecting tube 7 is communicated with the interior of the condensing tube 6, the bottom end of the first connecting tube 7 is fixedly connected with a middle through tube 8, the middle through tube 8 is communicated with the interior of the first connecting tube 7, and a heat exchange mechanism capable of improving the heat exchange effect of cooling water and accelerating the condensing efficiency of steam is arranged in the heat exchange box 5;
the heat exchange mechanism comprises a spiral pipe 9 arranged in the condenser pipe 6, two ends of the spiral pipe 9 extend into the heat exchange box 5, a circulating pump 10 is fixedly connected to the inner wall of the top of the heat exchange box 5, a water inlet of the circulating pump 10 is fixedly connected with one end of the spiral pipe 9, a water outlet of the circulating pump 10 is fixedly connected with a coiled pipe 11, one end of the coiled pipe 11 is fixedly connected with one end of the spiral pipe 9, two rotating shafts 12 are rotatably and penetratingly connected to the inner wall of one side of the heat exchange box 5, and one end of each rotating shaft 12 is fixedly connected with a fan blade 13; one side outer wall fixedly connected with protection casing 14 of heat exchange box 5, in the one end of pivot 12 extends to protection casing 14, the fixed cover is equipped with linkage gear 15 on the pivot 12, and one side inner wall fixedly connected with first motor 16 of protection casing 14, the output shaft fixedly connected with drive gear 17 of first motor 16, drive gear 17 and two linkage gears 15 all mesh.
Embodiment two:
referring to fig. 1 to 4, the present embodiment provides a technical solution based on the first embodiment: the top of the base 1 is fixedly connected with a steam bath device 18, the steam bath device 18 is fixedly connected with a steam bath pot 19, the regulating box 4 is connected with an air duct 20 in a penetrating way through a rotating piece, one end of the air duct 20 extends into the middle through pipe 8 in a rotating way, one end of the air duct 20, which is far away from the middle through pipe 8, is connected with a distillation flask 21 through a thread sleeve in a threaded way, and the distillation flask 21 is positioned above the steam bath pot 19; the bottom end of the middle through pipe 8 is fixedly connected with a second connecting pipe 22, the bottom end of the second connecting pipe 22 is connected with a collecting bottle 23 through a thread sleeve thread, a first electromagnetic valve 24 is fixedly connected to the second connecting pipe 22, a third connecting pipe 25 is fixedly connected to the middle through pipe 8, a second electromagnetic valve 26 is fixedly connected to the third connecting pipe 25, the top of the base 1 is fixedly connected with an air pump 27, an air inlet of the air pump 27 is fixedly connected with a telescopic hose 28, and the top end of the telescopic hose 28 extends into the third connecting pipe 25; the bottom inner wall of the mounting cylinder 2 is fixedly connected with a second motor 29, an output shaft of the second motor 29 is fixedly connected with a threaded rod 30, and the top thread of the threaded rod 30 extends into the lifting cylinder 3; the air duct 20 is fixedly sleeved with a driven bevel gear 31, a third motor 32 is fixedly connected in the regulating box 4, an output shaft of the third motor 32 is fixedly connected with a driving bevel gear 33, and the driving bevel gear 33 is meshed with the driven bevel gear 31; a chute 34 is formed in the mounting cylinder 2, a limiting rod 35 is fixedly connected to the outer wall of the lifting cylinder 3, and one end of the limiting rod 35 slides and extends into the corresponding chute 34; the air duct 20 is fixedly connected with a liquid adding pipe 36, and the liquid adding pipe 36 is fixedly connected with a third electromagnetic valve 37.
And all that is not described in detail in this specification is well known to those skilled in the art.
Working principle: when in use, the steam bath 18 is started to heat the steam bath pot 19, then the third electromagnetic valve 37 is opened, octyl triazinone solution is poured into the distillation flask 21 through the liquid adding pipe 36 and the air duct 20, then the third electromagnetic valve 37 is closed, at the moment, the second motor 29 is started, the second motor 29 drives the lifting cylinder 3 to descend through the threaded rod 30, the lifting cylinder 3 drives the regulating box 4 to descend, at the moment, the distillation flask 21 descends along with the lifting cylinder until the distillation flask 21 is close to the steam bath pot 19, then the third motor 32 is started, the third motor 32 drives the driven bevel gear 31 meshed with the third motor 32 to rotate through the driving bevel gear 33, the driven bevel gear 31 drives the air duct 20 to rotate, at the moment, the distillation flask 21 rotates along with the driving bevel gear, the solution in the distillation flask 21 forms a film on the inner wall of the distillation flask 21 to accelerate evaporation efficiency, at the same time, the second electromagnetic valve 26 is opened to start the air sucking pump 27, the air sucking pump 27 sucks air into the middle through the telescopic hose 28 and the third connecting pipe 25, then the second electromagnetic valve 26 is closed to generate negative pressure in the distillation flask 21, at this time, the solution in the distillation flask 21 is vaporized at high temperature, steam enters the middle through pipe 8 through the air duct 20, then enters the condensation pipe 6 through the first connecting pipe 7, at this time, the circulating pump 10 and the first motor 16 are started, the first motor 16 drives the two linkage gears 15 meshed with the first motor to rotate through the driving gear 17, the linkage gears 15 drive the rotating shaft 12 to rotate, the rotating shaft 12 drives the fan blades 13 to rotate, the fan blades 13 cool cooling water in the coiled pipe 11, meanwhile, the circulating pump 10 enables the cooling water to circulate in the spiral pipe 9 and the coiled pipe 11, the cooling water in the spiral pipe 9 cools the steam to enable the steam to condense, then the first electromagnetic valve 24 is opened to enable condensed water drops to enter the collection bottle 23 through the second connecting pipe 22 to collect, the production work of the octyl triazone can be completed after continuous work.
It is noted that relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.

Claims (8)

1. A rotary evaporator for the production of octyl triazone comprising a base (1), characterized in that: the cooling water cooling device comprises a base (1), wherein the top of the base (1) is fixedly connected with a mounting cylinder (2), a lifting cylinder (3) is inserted in the mounting cylinder (2), the top of the lifting cylinder (3) is fixedly connected with a regulating box (4), the top of the regulating box (4) is fixedly connected with a heat exchange box (5), one side of the heat exchange box (5) is fixedly connected with a condensing pipe (6), the bottom of the condensing pipe (6) is fixedly connected with a first connecting pipe (7), the first connecting pipe (7) is communicated with the interior of the condensing pipe (6), the bottom of the first connecting pipe (7) is fixedly connected with a middle through pipe (8), the middle through pipe (8) is communicated with the interior of the first connecting pipe (7), and a heat exchange mechanism capable of improving the heat exchange effect of cooling water and accelerating the condensation efficiency of steam is arranged in the heat exchange box (5);
the heat exchange mechanism comprises a spiral pipe (9) arranged in a condensing pipe (6), two ends of the spiral pipe (9) are all extended into a heat exchange box (5), a circulating pump (10) is fixedly connected to the inner wall of the top of the heat exchange box (5), a water inlet of the circulating pump (10) is fixedly connected with one end of the spiral pipe (9), a water outlet of the circulating pump (10) is fixedly connected with a coiled pipe (11), one end of the coiled pipe (11) is fixedly connected with one end of the spiral pipe (9), two rotating shafts (12) are rotatably and penetratingly connected to the inner wall of one side of the heat exchange box (5), and fan blades (13) are fixedly connected to one end of the rotating shafts (12).
2. A rotary evaporator for the production of octyl triazone according to claim 1, characterized in that: one side outer wall fixedly connected with protection casing (14) of heat exchange box (5), in one end of pivot (12) extends to protection casing (14), fixed cover is equipped with linkage gear (15) on pivot (12), one side inner wall fixedly connected with first motor (16) of protection casing (14), the output shaft fixedly connected with driving gear (17) of first motor (16), driving gear (17) all mesh with two linkage gears (15).
3. A rotary evaporator for the production of octyl triazone according to claim 1, characterized in that: the top fixedly connected with steam bath ware (18) of base (1), fixedly connected with steam bath pot (19) on steam bath ware (18), be connected with air duct (20) through rotating the piece through on adjusting box (4), in the one end rotation of air duct (20) extends to well siphunculus (8), the one end that well siphunculus (8) was kept away from to air duct (20) has distillation flask (21) through thread bush threaded connection, distillation flask (21) are located steam bath pot (19) top.
4. A rotary evaporator for the production of octyl triazone according to claim 1, characterized in that: the bottom fixedly connected with second connecting pipe (22) of well siphunculus (8), threaded sleeve threaded connection has collecting bottle (23) in the bottom of second connecting pipe (22), fixedly connected with first solenoid valve (24) on second connecting pipe (22), fixedly connected with third connecting pipe (25) on well siphunculus (8), fixedly connected with second solenoid valve (26) on third connecting pipe (25), the top fixedly connected with aspiration pump (27) of base (1), the air inlet fixedly connected with flexible hose (28) of aspiration pump (27), the top of flexible hose (28) extends to in third connecting pipe (25).
5. A rotary evaporator for the production of octyl triazone according to claim 1, characterized in that: the bottom inner wall fixedly connected with second motor (29) of installation section of thick bamboo (2), the output shaft fixedly connected with threaded rod (30) of second motor (29), the top screw thread of threaded rod (30) extends to in the lift section of thick bamboo (3).
6. A rotary evaporator for the production of octyl triazone according to claim 3, characterized in that: the air duct (20) is fixedly sleeved with a driven bevel gear (31), a third motor (32) is fixedly connected in the adjusting box (4), an output shaft of the third motor (32) is fixedly connected with a driving bevel gear (33), and the driving bevel gear (33) is meshed with the driven bevel gear (31).
7. A rotary evaporator for the production of octyl triazone according to claim 1, characterized in that: a chute (34) is formed in the mounting cylinder (2), a limit rod (35) is fixedly connected to the outer wall of the lifting cylinder (3), and one end of the limit rod (35) slides and extends into the corresponding chute (34).
8. A rotary evaporator for the production of octyl triazone according to claim 3, characterized in that: the air duct (20) is fixedly connected with a liquid adding pipe (36), and the liquid adding pipe (36) is fixedly connected with a third electromagnetic valve (37).
CN202321107424.9U 2023-05-10 2023-05-10 Rotary evaporator for producing octyl triazone Active CN220676758U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202321107424.9U CN220676758U (en) 2023-05-10 2023-05-10 Rotary evaporator for producing octyl triazone

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202321107424.9U CN220676758U (en) 2023-05-10 2023-05-10 Rotary evaporator for producing octyl triazone

Publications (1)

Publication Number Publication Date
CN220676758U true CN220676758U (en) 2024-03-29

Family

ID=90409349

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202321107424.9U Active CN220676758U (en) 2023-05-10 2023-05-10 Rotary evaporator for producing octyl triazone

Country Status (1)

Country Link
CN (1) CN220676758U (en)

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