CN220634273U - 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle - Google Patents
4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle Download PDFInfo
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- CN220634273U CN220634273U CN202322287284.4U CN202322287284U CN220634273U CN 220634273 U CN220634273 U CN 220634273U CN 202322287284 U CN202322287284 U CN 202322287284U CN 220634273 U CN220634273 U CN 220634273U
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- 238000005554 pickling Methods 0.000 title claims abstract description 60
- 239000002994 raw material Substances 0.000 title claims abstract description 31
- MLLIIHAKTPXMFF-UHFFFAOYSA-N (4-chlorophenyl)-(3,4-dimethoxyphenyl)methanone Chemical compound C1=C(OC)C(OC)=CC=C1C(=O)C1=CC=C(Cl)C=C1 MLLIIHAKTPXMFF-UHFFFAOYSA-N 0.000 title claims abstract description 26
- 150000002576 ketones Chemical class 0.000 title claims abstract description 16
- 239000007788 liquid Substances 0.000 claims abstract description 51
- 238000001514 detection method Methods 0.000 claims description 7
- 210000002421 cell wall Anatomy 0.000 claims description 4
- 238000013329 compounding Methods 0.000 claims description 2
- 239000002253 acid Substances 0.000 abstract description 11
- 238000005406 washing Methods 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 6
- 239000012535 impurity Substances 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000002699 waste material Substances 0.000 description 4
- 238000010586 diagram Methods 0.000 description 3
- 102000010970 Connexin Human genes 0.000 description 2
- 108050001175 Connexin Proteins 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 2
- 210000003976 gap junction Anatomy 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- RKIDDEGICSMIJA-UHFFFAOYSA-N 4-chlorobenzoyl chloride Chemical compound ClC(=O)C1=CC=C(Cl)C=C1 RKIDDEGICSMIJA-UHFFFAOYSA-N 0.000 description 1
- 238000005727 Friedel-Crafts reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
Abstract
The utility model relates to the technical field of pickling kettles, in particular to a 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle. The technical proposal comprises: the hydraulic telescopic rod is installed on the top of the hydraulic cylinder, the top plate is installed on the top of the hydraulic telescopic rod, the lower surface of the top plate is connected with the cover plate through the connecting plate, the first connecting rings are all installed on two sides of the lower surface of the cover plate, hooks are arranged on the first connecting rings, the hooks are installed on two ends of the connecting rope, and the hooks on the other end of the connecting rope are arranged on the second connecting rings. The utility model not only effectively improves the acid washing effect of the 4-chloro-3 ',4' -dimethoxy benzophenone raw material, but also can filter the acid washing liquid to remove impurities in the acid washing liquid, so that the acid washing liquid can be used continuously and has strong practicability.
Description
Technical Field
The utility model relates to the technical field of pickling kettles, in particular to a 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle.
Background
The 4-chloro-3 ',4' -dimethoxy benzophenone is white crystal. The preparation method is that p-chlorobenzoyl chloride and 1, 2-phenyldimethyl ether are subjected to Friedel-crafts reaction in the presence of anhydrous AlCl3 to prepare the 4-chloro-3 ',4' -dimethoxy benzophenone, and an acid pickling kettle is needed in the preparation and synthesis of the 4-chloro-3 ',4' -dimethoxy benzophenone.
Through retrieving, patent publication number CN209237940U discloses a pickling kettle with heating function, including the pickling kettle body, the internal agitating unit that is equipped with of pickling kettle, agitating unit includes rotatory inner ring and rotatory outer ring, and the magnetic pole of the outer convex surface of arc magnet No. one and the magnetic pole of the concave surface in arc magnet No. two are the synonym magnetic pole. According to the utility model, the motor drives the rotary outer ring to rotate, the second arc-shaped magnet in the rotary outer ring rotates, and the first arc-shaped magnet in the rotary inner ring is attracted to rotate through magnetic force, so that the stirring rod is driven to rotate, the liquid in the pickling kettle body is stirred, the pickling efficiency is improved, the stirring rod does not penetrate out of the pickling kettle body, and the problem that acid molecules leak due to difficulty in sealing of a shaft hole is solved. In addition, the heating half pipe heats the pickling kettle body, so that the temperature of the acid liquid is increased, the pickling time is shortened, and the working efficiency is improved.
When the conventional pickling kettle is in actual use, the mobility of the pickling solution is poor, the pickling effect on chemical raw materials is poor, and after the pickling of the raw materials is completed, staff directly discharges the pickling solution, so that unnecessary waste is easily caused, and the production cost is high.
Disclosure of Invention
The utility model aims to provide a 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle, which solves the problems in the prior art.
In order to achieve the above purpose, the present utility model provides the following technical solutions: the utility model provides a 4-chloro-3 ',4' -dimethoxy benzophenone compounding raw materials ketone pickling kettle, includes the base, hydraulic cylinder, the cauldron body, first pump body, filter bowl and second pump body are installed in proper order from left to right to the upper surface of base, hydraulic telescoping rod is installed on the top of hydraulic telescoping rod, the roof is installed on the top of hydraulic telescoping rod, the lower surface of roof passes through connecting plate and apron connection, first go-between is all installed to the lower surface both sides of apron, be provided with the couple on the first go-between, the couple is installed on the both ends of connecting rope, the couple on the connecting rope other end sets up on the second go-between, the second go-between sets up the top both sides at the raw materials standing groove.
Through the cooperation setting of a series of structures such as the first pump body, the second pump body, first connecting pipe, second connecting pipe, when the staff carries out the pickling to 4-chloro-3 ',4' -dimethoxy benzophenone raw materials, the staff starts first pump body and second pump body, first pump body and second pump body can make the pickling solution circulate, the mobility of pickling solution has been strengthened, thereby the utility model has effectively improved 4-chloro-3 ',4' -dimethoxy benzophenone raw materials pickling effect, through the cooperation setting of structures such as plate filter screen, filter vat, when first pump body and second pump body made the pickling solution circulate, the plate filter screen in the filter vat filters the pickling solution, get rid of pickling solution produced impurity, and PH value detection sensor detects the PH value of pickling solution in real time, thereby the staff of being convenient for judges whether the pickling solution needs to discharge, so that can continue to use, avoid causing unnecessary waste, manufacturing cost has been reduced.
Preferably, a PH value detection sensor is arranged on the inner rear end wall of the kettle body, and a PLC controller is arranged on the front end surface of the kettle body.
Preferably, a diversion block is arranged at the bottom end of the kettle body.
Preferably, a first liquid inlet pipe and a first liquid outlet pipe are respectively arranged above and below one side outer wall of the kettle body, the other end of the first liquid outlet pipe is connected with a liquid inlet end on one side outer wall of the first pump body through a pipe joint, the liquid outlet end on the top of the first pump body is connected with a second connecting pipe through a pipe joint, the other end of the second connecting pipe is connected with a second liquid inlet pipe through a pipe joint, the second liquid inlet pipe is arranged above one side outer wall of the filter tank, a second liquid outlet pipe is arranged below the other side outer wall of the filter tank, the other end of the second liquid outlet pipe is connected with a liquid inlet end on one side outer wall of the second pump body through a pipe joint, the liquid outlet end on the top of the second pump body is connected with the first connecting pipe through a pipe joint, and the other end of the first connecting pipe is connected with the first liquid inlet pipe through a pipe joint.
Preferably, valve bodies are arranged on the first liquid inlet pipe, the first liquid outlet pipe, the second liquid inlet pipe and the second liquid outlet pipe.
Preferably, the inside of filter vat is provided with board-like filter screen, the both ends of board-like filter screen are all installed in the U type inslot on the U type cardboard, and be gap connection between the cell wall in the both ends outer wall of board-like filter screen and the U type groove on the U type cardboard.
Preferably, the U-shaped clamping plates are arranged on the front end wall and the rear end wall inside the filter tank.
Compared with the prior art, the utility model has the beneficial effects that:
1. according to the utility model, through the matching arrangement of a series of structures such as the first pump body, the second pump body, the first connecting pipe, the second connecting pipe and the like, when a worker performs acid washing on the 4-chloro-3 ',4' -dimethoxy benzophenone raw material, the worker starts the first pump body and the second pump body, the first pump body and the second pump body can enable the acid washing liquid to circularly flow, and the mobility of the acid washing liquid is enhanced, so that the acid washing effect of the 4-chloro-3 ',4' -dimethoxy benzophenone raw material is effectively improved.
2. According to the utility model, through the cooperation arrangement of the structures such as the plate-type filter screen and the filter tank, when the first pump body and the second pump body enable the pickling solution to circularly flow, the plate-type filter screen in the filter tank filters the pickling solution to remove impurities generated by pickling, and the PH value detection sensor detects the PH value of the pickling solution in real time, so that a worker can conveniently judge whether the pickling solution needs to be discharged or not, the pickling solution can be used continuously, unnecessary waste is avoided, the production cost is reduced, and the practicability is high.
Drawings
FIG. 1 is a schematic diagram of the structure of the present utility model;
FIG. 2 is a schematic view of the internal structure of the present utility model;
FIG. 3 is a schematic diagram of a filter cell according to the present utility model;
fig. 4 is a schematic diagram of a connection structure between a cover plate and a raw material placing groove according to the present utility model.
In the figure: 1. a top plate; 2. a connecting plate; 3. a cover plate; 4. a hydraulic telescopic rod; 5. a PLC controller; 6. a kettle body; 7. a hydraulic cylinder; 8. a base; 9. a first liquid inlet pipe; 10. a tube-like joint; 11. a first connection pipe; 12. a first liquid outlet pipe; 13. a first pump body; 14. a second connection pipe; 15. a filter tank; 16. a U-shaped clamping plate; 17. a plate filter screen; 18. a second liquid outlet pipe; 19. a valve body; 20. a second pump body; 21. a first connection ring; 22. a hook; 23. a connecting rope; 24. a second connecting ring; 25. a raw material placing groove; 26. a flow guiding block; 27. a pH value detection sensor; 28. and a second liquid inlet pipe.
Detailed Description
The technical scheme of the utility model is further described below with reference to the attached drawings and specific embodiments.
Example 1
As shown in fig. 1-4, the 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle provided by the utility model comprises a base 8, wherein a hydraulic cylinder 7, a kettle body 6, a first pump body 13, a filter tank 15 and a second pump body 20 are sequentially arranged on the upper surface of the base 8 from left to right, a hydraulic telescopic rod 4 is arranged at the top end of the hydraulic cylinder 7, a top plate 1 is arranged at the top end of the hydraulic telescopic rod 4, the lower surface of the top plate 1 is connected with a cover plate 3 through a connecting plate 2, first connecting rings 21 are arranged on two sides of the lower surface of the cover plate 3, hooks 22 are arranged on the first connecting rings 21, the hooks 22 are arranged on two ends of a connecting rope 23, the hooks 22 on the other end of the connecting rope 23 are arranged on second connecting rings 24, and the second connecting rings 24 are arranged on two sides of the top of a raw material placing groove 25.
The working principle of the 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle based on the first embodiment is as follows: when the pickling tank is used, an external power supply is connected, when a worker performs pickling on the 4-chloro-3 ',4' -dimethoxy benzophenone raw material, the worker starts the first pump body 13 and the second pump body 20, the first pump body 13 and the second pump body 20 can enable the pickling solution to flow circularly, and the fluidity of the pickling solution is enhanced, so that the pickling tank effectively improves the pickling effect of the 4-chloro-3 ',4' -dimethoxy benzophenone raw material, and when the first pump body 13 and the second pump body 20 enable the pickling solution to flow circularly, the plate-type filter screen 17 in the filter tank 15 filters the pickling solution to remove impurities generated by pickling, and the PH value detection sensor 27 detects the PH value of the pickling solution in real time, so that the worker is convenient to judge whether the pickling solution needs to be discharged or not, the pickling tank can be used continuously, unnecessary waste is avoided, and the production cost is reduced.
Example two
As shown in fig. 1-4, the present utility model provides a 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle, which further comprises: a PH value detection sensor 27 is arranged on the inner rear end wall of the kettle body 6, a PLC controller 5 is arranged on the front end surface of the kettle body 6, a flow guide block 26 is arranged at the inner bottom end of the kettle body 6, a first liquid inlet pipe 9 and a first liquid outlet pipe 12 are respectively arranged above and below the outer wall of one side of the kettle body 6, the other end of the first liquid outlet pipe 12 is connected with the liquid inlet end on the outer wall of one side of a first pump body 13 through a pipe joint 10, the liquid outlet end on the top of the first pump body 13 is connected with a second connecting pipe 14 through a pipe joint 10, the other end of the second connecting pipe 14 is connected with a second liquid inlet pipe 28 through a pipe joint 10, the second liquid inlet pipe 28 is arranged above the outer wall of one side of a filter tank 15, a second liquid outlet pipe 18 is arranged below the outer wall of the other side of the filter tank 15, the other end of second drain pipe 18 is connected with the feed liquor end on the outer wall of one side of the second pump body 20 through pipe type joint 10, the drain end on the top of the second pump body 20 is connected with first connecting pipe 11 through pipe type joint 10, the other end of first connecting pipe 11 is connected with first feed liquor pipe 9 through pipe type joint 10, all be provided with valve body 19 on first feed liquor pipe 9, first drain pipe 12, second feed liquor pipe 28 and the second drain pipe 18, the inside of filter tank 15 is provided with plate filter screen 17, the U type inslot on U type cardboard 16 is all installed at the both ends of plate filter screen 17, and be gap junction between the cell wall of the U type groove on the plate filter screen 17 and the U type cardboard 16, the front end wall and the rear end wall of U type cardboard 16 are installed in the filter tank 15 inside.
In this embodiment, the setting of guide block 26, the guide block 26 can play the effect of water conservancy diversion to the pickling solution of raw materials standing groove 25, because of the inside of filter vat 15 is provided with board-like filter screen 17, the U type inslot on U type cardboard 16 is all installed at board-like filter screen 17's both ends, and be gap junction between the cell wall in the U type groove on board-like filter screen 17's both ends outer wall and the U type cardboard 16 to the staff of being convenient for dismouting change or clearance to board-like filter screen 17.
The above-described embodiments are merely a few preferred embodiments of the present utility model, and many alternative modifications and combinations of the above-described embodiments will be apparent to those skilled in the art based on the technical solutions of the present utility model and the related teachings of the above-described embodiments.
Claims (7)
1. The utility model provides a 4-chloro-3 ',4' -dimethoxy benzophenone compounding raw materials ketone pickling kettle, includes base (8), its characterized in that: the utility model discloses a hydraulic cylinder, cauldron body (6), first pump body (13), filter bowl (15) and second pump body (20) are installed in proper order from left to right to the upper surface of base (8), hydraulic telescoping rod (4) are installed on the top of hydraulic cylinder (7), roof (1) are installed on the top of hydraulic telescoping rod (4), the lower surface of roof (1) is connected with apron (3) through connecting plate (2), first go-between (21) are all installed to the lower surface both sides of apron (3), be provided with couple (22) on first go-between (21), couple (22) are installed on the both ends of connecting rope (23), couple (22) on connecting rope (23) other end set up on second go-between (24), second go-between (24) set up the top both sides at raw materials standing groove (25).
2. The 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle according to claim 1, wherein the kettle is characterized in that: the PH value detection sensor (27) is arranged on the inner rear end wall of the kettle body (6), and the front end face of the kettle body (6) is provided with the PLC (5).
3. The 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle according to claim 1, wherein the kettle is characterized in that: the inner bottom end of the kettle body (6) is provided with a flow guide block (26).
4. The 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle according to claim 1, wherein the kettle is characterized in that: the kettle comprises a kettle body (6), wherein a first liquid inlet pipe (9) and a first liquid outlet pipe (12) are respectively arranged above and below one side outer wall of the kettle body (6), the other end of the first liquid outlet pipe (12) is connected with a liquid inlet end on one side outer wall of a first pump body (13) through a pipe joint (10), the liquid outlet end on the top of the first pump body (13) is connected with a second connecting pipe (14) through a pipe joint (10), the other end of the second connecting pipe (14) is connected with a second liquid inlet pipe (28) through a pipe joint (10), the second liquid inlet pipe (28) is arranged above one side outer wall of a filter tank (15), a second liquid outlet pipe (18) is arranged below the other side outer wall of the filter tank (15), the other end of the second liquid outlet pipe (18) is connected with a liquid inlet end on one side outer wall of a second pump body (20) through a pipe joint (10), and the liquid outlet end on the top of the second pump body (20) is connected with the first connecting pipe (11) through a pipe joint (10), and the other end of the second liquid inlet pipe (11) is connected with the first connecting pipe (9).
5. The 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle according to claim 4, wherein the kettle is characterized in that: valve bodies (19) are arranged on the first liquid inlet pipe (9), the first liquid outlet pipe (12), the second liquid inlet pipe (28) and the second liquid outlet pipe (18).
6. The 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle according to claim 1, wherein the kettle is characterized in that: the inside of filter vat (15) is provided with board-like filter screen (17), the U type inslot on U type cardboard (16) is all installed at the both ends of board-like filter screen (17), and be gap connection between the cell wall in the both ends outer wall of board-like filter screen (17) and the U type groove on U type cardboard (16).
7. The 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle according to claim 6, wherein the kettle is characterized in that: the U-shaped clamping plates (16) are arranged on the front end wall and the rear end wall inside the filter tank (15).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322287284.4U CN220634273U (en) | 2023-08-24 | 2023-08-24 | 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322287284.4U CN220634273U (en) | 2023-08-24 | 2023-08-24 | 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220634273U true CN220634273U (en) | 2024-03-22 |
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ID=90283654
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202322287284.4U Active CN220634273U (en) | 2023-08-24 | 2023-08-24 | 4-chloro-3 ',4' -dimethoxy benzophenone mixed raw material ketone pickling kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220634273U (en) |
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2023
- 2023-08-24 CN CN202322287284.4U patent/CN220634273U/en active Active
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