CN220633076U - Medicament evaporation crystallization tank - Google Patents

Abstract

The utility model relates to an evaporation crystallization tank technical field specifically is a medicament evaporation crystallization tank, including the inlayer jar body, the outside of inlayer jar body is provided with outer jar body, the bottom of outer jar body is provided with first support column, the inside of inlayer jar body is provided with rabbling mechanism to the inside of inlayer jar body is provided with the backup pad, the first through-hole has been seted up on the surface of outer jar body, and be provided with the pipeline of giving vent to anger on the surface of outer jar body, the pipeline of giving vent to anger runs through outer jar body to outside through the first through-hole of seting up, and the top of the pipeline of giving vent to anger is provided with the valve of giving vent to anger; the below of the outer jar body is provided with the condensation jar body, and the inside of the condensation jar body is provided with the diversion pipe to the bottom of the condensation jar body is provided with the choke valve, and then has realized the continuous stirring to the inside medicament of evaporating dish in the evaporation process, thereby has guaranteed that the inside medicament of evaporating dish can not take place to precipitate in the evaporation process, reaches the purpose that the medicament evaporation crystallization detected.

Description

Medicament evaporation crystallization tank

Technical Field

The application relates to the technical field of evaporative crystallization tanks, in particular to a medicament evaporative crystallization tank.

Background

Evaporation is known to be a process of removing a solvent from a solution by heating the solvent, and a process of polymerizing the solvent into crystals, which are used for detecting components of substances, and a method of evaporating and crystallizing a chemical is also used for detecting the chemical, so that a chemical evaporating and crystallizing tank is required.

Through retrieval, the utility model patent with the Chinese publication number of CN202638034U discloses a lysine hydrochloride evaporation crystallization tank, which comprises an evaporation chamber, a circulating pipe, an axial flow type circulating pump, a heating chamber, a collector and a scrubber, wherein the evaporation chamber comprises an upper sealing head, a straight barrel and a lower cone, the circulating pipe is connected with the side surface of the lower cone bottom of the evaporation chamber, the other end of the circulating pipe is connected with an inlet of the axial flow type circulating pump, the pump is connected with the heating chamber, an outlet of the heating chamber is connected with the evaporation chamber, the collector is positioned at the lower cone bottom of the evaporation chamber, the scrubber is positioned below the collector, the scrubber is arranged below the crystal collector, crystals can be washed and classified, the product quality is improved, the discharging pipe is connected with the bottom of the scrubber, the mother liquor carried by the crystals can be reduced and discharged, and the mother liquor circulation after the crystals are separated is reduced.

Although the above technical scheme solves the problems of washing and classifying crystals, improving the product quality, discharging pipes are connected at the bottom of the washer, reducing the amount of mother liquor carried by the discharged crystals and reducing the mother liquor circulation after the separation of the crystals, in the above technical scheme, the substances to be detected are easy to precipitate in a high-temperature environment in the process of evaporating and detecting the substances, so that the evaporated crystals do not meet the detection requirements.

Disclosure of Invention

Technical problem to be solved

To the not enough of prior art, this application provides a medicament evaporation crystallizer to solve the problem that proposes among the above-mentioned background art.

In order to achieve the above purpose, the present application provides the following technical solutions: the utility model provides a medicament evaporation crystallization jar, includes the inlayer jar body, its characterized in that: the outer layer tank body is arranged outside the inner layer tank body, a first supporting column is arranged at the bottom of the outer layer tank body, a stirring mechanism is arranged inside the inner layer tank body, a supporting plate is arranged inside the inner layer tank body, a first through hole is formed in the surface of the outer layer tank body, an air outlet pipeline is arranged on the surface of the outer layer tank body, the air outlet pipeline penetrates through the outer layer tank body to the outside through the first through hole, and an air outlet valve is arranged above the air outlet pipeline;

the condensing tank is arranged below the outer tank, a diversion pipe is arranged in the condensing tank, a throttle valve is arranged at the bottom of the condensing tank, a crystallization container is arranged below the throttle valve, a base plate is arranged on the lower surface of the crystallization container, a bottom plate is arranged on the right side of the outer tank, a second supporting column is arranged on the lower surface of the bottom plate, an electric heater is arranged on the upper surface of the second supporting column, and a heat-conducting pipeline is arranged on the left side of the electric heater;

the inside of the inner tank body is provided with a placement block, and an evaporation dish is arranged above the placement block.

Preferably, the stirring mechanism comprises a fixed block, the fixed block sets up the upper surface at the backup pad, the upper surface of fixed block is provided with the motor, the output of motor is connected with first conical gear, the meshing has second conical gear on the first conical gear, the bottom of second conical gear is connected with the axis of rotation, the bottom of axis of rotation is connected with the connecting block, the connecting hole has been seted up to the both sides of connecting block, through-connection has the connecting rod in the connecting hole, the both sides of connecting rod all are provided with the stirring rod to stir the medicament in the evaporation process, prevent that it from taking place to precipitate.

Further, the second through holes are formed in two sides of the top of the inner tank body, a circulating pipeline is arranged in the inner tank body, the circulating pipeline penetrates to the outside of the inner tank body through the second through holes, and the diameter of the second through holes is matched with the diameter of the circulating pipeline, so that the thermal steam in the evaporation process can be recycled.

Still further, the surface of the condensation tank body is opened and is set up the spacing groove, the lateral surface of diversion pipe is provided with the gag lever post, the shape of spacing groove is "L" shape, plays restriction diversion pipe position and removes the effect.

Further scheme, the back of the condensation tank body is provided with the cold air case, the top of cold air case is provided with adjusts the commentaries on classics handle to cold air case and air conditioning shower nozzle electric connection, the air conditioning shower nozzle sets up on the inner wall of the condensation tank body, the surface of adjusting the commentaries on classics handle is provided with the temperature regulation scale, carries out condensation cooling to the crystallization that evaporates.

On the basis of the scheme, the output end of the electric heater is provided with a control valve, one end of the control valve is communicated with a heat-conducting pipeline, and the top of the control valve is provided with a handle for controlling the temperature inside the inner tank body.

On the basis of the scheme, the surface of the outer layer tank body is provided with a temperature display, the temperature display is electrically connected with a temperature sensor, and the temperature sensor is arranged in an interlayer of the inner layer tank body and the outer layer tank body and is used for observing the ambient temperature in the evaporation process of the medicament.

Compared with the prior art, the application provides a medicament evaporation crystallization tank, possesses following beneficial effect:

this medicament evaporation crystallization tank, through set up rabbling mechanism in the top of evaporating dish, because the torsion of the motor in the rabbling mechanism for thereby the axis of rotation rotates the stirring rod on the connecting rod stirs, and then has realized the continuous stirring to the inside medicament of evaporating dish in the evaporation process, thereby guaranteed that the inside medicament of evaporating dish can not take place to precipitate in the evaporation process, reaches the purpose that medicament evaporation crystallization detected.

Drawings

FIG. 1 is a schematic structural diagram of the present application;

FIG. 2 is a schematic view of a partial vertical section of the present application;

FIG. 3 is a schematic diagram of an exploded structure of the stirring mechanism of the present application;

fig. 4 is a schematic partial structure of the present application.

In the figure: 1. an inner tank body; 2. an outer layer tank body; 3. a first support column; 4. a stirring mechanism; 401. a fixed block; 402. a motor; 403. a first bevel gear; 404. a second bevel gear; 405. a rotating shaft; 406. a connecting block; 407. a connection hole; 408. a connecting rod; 409. stirring rod; 5. a support plate; 6. a first through hole; 7. an air outlet pipe; 8. an air outlet valve; 9. a condensing tank; 10. a diverting tube; 11. a throttle valve; 12. a crystallization vessel; 13. a backing plate; 14. a bottom plate; 15. a second support column; 16. an electric heater; 17. a heat transfer pipe; 18. a second through hole; 19. a circulation pipe; 20. a limit groove; 21. a limit rod; 22. a cold air box; 23. adjusting a rotating handle; 24. a control valve; 25. a temperature display; 26. placing a block; 27. an evaporation dish; 28. a cold air spray head.

Detailed Description

The following description of the embodiments of the present application will be made clearly and fully with reference to the accompanying drawings, in which it is evident that the embodiments described are only some, but not all, of the embodiments of the present application. All other embodiments, which can be made by one of ordinary skill in the art without undue burden from the present disclosure, are within the scope of the present disclosure.

Examples

Referring to fig. 1-4, a medicament evaporating and crystallizing tank comprises an inner tank body 1, wherein an outer tank body 2 is arranged outside the inner tank body 1, first support columns 3 are arranged at the bottom of the outer tank body 2, the number of the first support columns 3 is four, the inner tank body 1 and the outer tank body 2 are both arranged at the tops of the four groups of first support columns 3, a stirring mechanism 4 is arranged inside the inner tank body 1, a supporting plate 5 is arranged inside the inner tank body 1, part of the stirring mechanism 4 is arranged on the upper surface of the supporting plate 5, a first through hole 6 is formed in the surface of the outer tank body 2, an air outlet pipeline 7 is arranged on the surface of the outer tank body 2, the size diameter of the air outlet pipeline 7 is matched with the size diameter of the first through hole 6, the air outlet pipeline 7 penetrates through the outer tank body 2 to the outside through the first through hole 6, and a valve 8 is arranged above the air outlet pipeline 7 and is used for controlling the outflow of steam inside the outer tank body 2;

the lower part of the outer layer tank body 2 is provided with a condensation tank body 9, the inside of the condensation tank body 9 is provided with a diversion pipe 10, the bottom of the condensation tank body 9 is provided with a throttle valve 11 for controlling the outflow of evaporative crystals, the lower part of the throttle valve 11 is provided with a crystallization container 12 for containing the evaporative crystals, the lower surface of the crystallization container 12 is provided with a backing plate 13, the crystallization container 12 is fixedly arranged on the backing plate 13, the right side of the outer layer tank body 2 is provided with a bottom plate 14, the lower surface of the bottom plate 14 is provided with second support columns 15, the number of the second support columns 15 is four, the bottom plate 14 is fixedly arranged on the four groups of the second support columns 15, the upper surface of the second support columns 15 is fixedly provided with an electric heater 16, the left side of the electric heater 16 is provided with a heat-passing pipeline 17, and one end of the heat-passing pipeline 17 passes through the outer layer tank body 2 to the inside;

the inner tank 1 is internally provided with a placing block 26, and an evaporation dish 27 is arranged above the placing block 26.

By the above embodiment, the following effects can be obtained: through setting up the steam heat that pipeline 7 and valve 8 of giving vent to anger are used for controlling the inlayer jar body 1, through the last fixed surface mounting electric heater 16 at bottom plate 14 to be connected with logical hot pipe 17 through outer jar body 2, guaranteed the inside continuous heat supply of jar body, guarantee its inside evaporation environment, through setting up condensation jar body 9 in the below of outer jar body 2, realized carrying out final condensation cooling to the crystal after evaporating, make the crystal flow into crystallization container 12 through choke valve 11 at last.

Referring to fig. 3, in this embodiment, the stirring mechanism 4 includes a fixed block 401, the fixed block 401 is fixedly mounted on the upper surface of the supporting plate 5, a motor 402 is fixedly mounted on the upper surface of the fixed block 401, an output end of the motor 402 is fixedly connected with a first bevel gear 403, a second bevel gear 404 is meshed on the first bevel gear 403, a rotating shaft 405 is fixedly connected with a bottom of the second bevel gear 404, a connecting block 406 is fixedly connected with the bottom of the rotating shaft 405, connecting holes 407 are formed in two sides of the connecting block 406, connecting rods 408 are connected in the connecting holes 407 in a penetrating manner, diameters of the connecting holes 407 are matched with diameters of the connecting rods 408, stirring rods 409 are arranged on two sides of the connecting rods 408, and the stirring rods 409 are spirally arranged.

By the above embodiment, the following effects can be obtained: through setting up rabbling mechanism 4, because the torsion of motor 402 makes first conical gear 403 rotate, because first conical gear 403 meshes with second conical gear 404 to make second conical gear 404 rotate, again because the bottom of second conical gear 404 is connected with axis of rotation 405, and install connecting block 406 in the bottom of axis of rotation 405, and be connected with puddler 409 in connecting hole 407 that connecting block 406 offered, thereby make puddler 409 constantly stir in evaporation dish 27, through carrying out continuous stirring to the medicament at the evaporation in-process, the effectual medicament that prevents takes place to precipitate at the in-process of evaporation.

Next, referring to fig. 2 and 4, in the present embodiment, second through holes 18 are formed on two sides of the top of the inner tank 1, a circulation pipe 19 is disposed inside the inner tank 1, the circulation pipe 19 penetrates to the outside of the inner tank 1 through the second through holes 18, and the diameter of the second through holes 18 is adapted to the diameter of the circulation pipe 19.

By the above embodiment, the following effects can be obtained: through the second through holes 18 matched with the diameters of the circulating pipelines 19 are formed in the two sides of the inner tank body 1, the circulating pipelines 19 are firmly arranged in the formed second through holes 18, so that the hot steam in the evaporation process is recycled, the working efficiency is improved, and the resources are saved.

Referring to fig. 1 again, in the present embodiment, a limiting groove 20 is formed on the surface of the condensation tank 9, and a limiting rod 21 is fixedly mounted on the outer side surface of the diversion pipe 10, and the limiting groove 20 is L-shaped.

By the above embodiment, the following effects can be obtained: by forming the limit groove 20 into an L shape, an operator can conveniently control the up-and-down movement of the diversion pipe 10, so that the outflow of the evaporative crystals is controlled.

It should be noted that, referring to fig. 4, in the embodiment, a cold air box 22 is fixedly mounted on the back of the condensation tank 9, an adjusting handle 23 is fixed above the cold air box 22, the cold air box 22 is electrically connected with a cold air spray head 28, the cold air spray head 28 is fixed on the inner wall of the condensation tank 9, and a temperature adjustment scale is provided on the surface of the adjusting handle 23.

By the above embodiment, the following effects can be obtained: through with air conditioning shower nozzle 28 and air conditioning case 22 electric connection to realize the inside air conditioning temperature control of condensation tank body 9, through being provided with the temperature scale with the surface of adjusting the twist grip 23, thereby make things convenient for the accurate regulation of operating personnel.

It should be further noted that, referring to fig. 1, in the present embodiment, the output end of the electric heater 16 is connected to a control valve 24, one end of the control valve 24 is connected to a heat pipe 17, and a handle is disposed at the top of the control valve 24 for controlling the outflow of hot gas and thus controlling the temperature in the inner tank 1.

By the above embodiment, the following effects can be obtained: the control valve 24 is communicated with the middle position of the electric heater 16 and the heat-conducting pipeline 17, so that the temperature environment of the medicament evaporation can be controlled.

It should be further noted that, referring to fig. 1, in the present embodiment, a temperature display 25 is mounted on a surface of the outer tank 2, the temperature display 25 is electrically connected to a temperature sensor, and the temperature sensor is disposed in an interlayer between the inner tank 1 and the outer tank 2.

By the above embodiment, the following effects can be obtained: through being provided with temperature display 25 to the inside condition of inlayer jar body 1 is known more conveniently, for the purpose of medicament evaporation crystallization, thereby can more scientifically make corresponding judgement.

When the chemical evaporation crystallization tank is used, the chemical evaporation crystallization tank is firstly placed at a position required to be used, the chemical is placed in the evaporation pan 27, and the electric heater 16 is started. The hot air enters the inner tank body 1 through the heat-conducting pipeline 17, meanwhile, the motor 402 is started, the first conical gear 403 rotates due to the torque force of the motor 402, the second conical gear 404 rotates due to the meshing of the first conical gear 403 and the second conical gear 404, the bottom of the second conical gear 404 is connected with the rotating shaft 405, the connecting block 406 is arranged at the bottom of the rotating shaft 405, and the stirring rod 409 is connected in the connecting hole 407 formed in the connecting block 406, so that the stirring rod 409 is continuously stirred in the evaporation dish 27 to prevent precipitation, and the hot steam circulates between the inner tank body 1 and the outer tank body 2 due to the fact that the second through hole 18 is formed in the surface of the inner tank body 1;

when evaporation is in place, the limiting rod 21 moves through the limiting groove 20, so that the limiting rod 21 drives the diversion pipe 10 to move, evaporation crystals in the evaporation dish 27 flow into the condensation tank 9 through the diversion pipe 10, high-temperature crystals in the condensation tank 9 can be condensed and cooled by starting the cold air box 22, finally, the evaporation crystals flow into the bottom of the condensation tank 9, the throttle valve 11 is opened, and the cooled evaporation crystals flow into the crystallization container 12.

Although embodiments of the present application have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the application, the scope of which is defined in the appended claims and their equivalents.

Claims (6)

1. The utility model provides a medicament evaporation crystallization jar, includes inlayer jar body (1), its characterized in that: the novel inner tank is characterized in that an outer tank body (2) is arranged outside the inner tank body (1), a first supporting column (3) is arranged at the bottom of the outer tank body (2), a stirring mechanism (4) is arranged inside the inner tank body (1), a supporting plate (5) is arranged inside the inner tank body (1), a first through hole (6) is formed in the surface of the outer tank body (2), an air outlet pipeline (7) is arranged on the surface of the outer tank body (2), the air outlet pipeline (7) penetrates through the outer tank body (2) to the outside through the first through hole (6), and an air outlet valve (8) is arranged above the air outlet pipeline (7);

the utility model discloses a solar energy condenser is characterized in that a condensing tank body (9) is arranged below an outer layer tank body (2), a diversion pipe (10) is arranged inside the condensing tank body (9), a throttle valve (11) is arranged at the bottom of the condensing tank body (9), a crystallization container (12) is arranged below the throttle valve (11), a backing plate (13) is arranged on the lower surface of the crystallization container (12), a bottom plate (14) is arranged on the right side of the outer layer tank body (2), a second supporting column (15) is arranged on the lower surface of the bottom plate (14), an electric heater (16) is arranged on the upper surface of the second supporting column (15), and a heat-conducting pipeline (17) is arranged on the left side of the electric heater (16);

the inner tank body (1) is internally provided with a placement block (26), and an evaporation dish (27) is arranged above the placement block (26).

2. A pharmaceutical evaporation crystallization tank according to claim 1, wherein: the stirring mechanism (4) comprises a fixed block (401), the fixed block (401) is arranged on the upper surface of a supporting plate (5), a motor (402) is arranged on the upper surface of the fixed block (401), a first conical gear (403) is connected to the output end of the motor (402), a second conical gear (404) is meshed on the first conical gear (403), a rotating shaft (405) is connected to the bottom of the second conical gear (404), a connecting block (406) is connected to the bottom of the rotating shaft (405), connecting holes (407) are formed in two sides of the connecting block (406), connecting rods (408) are connected to the two sides of the connecting rods (408) in a penetrating manner, and stirring rods (409) are arranged on the two sides of each connecting rod (408).

3. A pharmaceutical evaporation crystallization tank according to claim 1, wherein: second through holes (18) are formed in two sides of the top of the inner tank body (1), a circulating pipeline (19) is arranged in the inner tank body (1), the circulating pipeline (19) penetrates through the second through holes (18) to the outside of the inner tank body (1), and the diameter of the second through holes (18) is matched with the diameter of the circulating pipeline (19).

4. A pharmaceutical evaporation crystallization tank according to claim 1, wherein: the surface of the condensation tank body (9) is provided with a limiting groove (20), the outer side surface of the diversion pipe (10) is provided with a limiting rod (21), and the limiting groove (20) is L-shaped.

5. A pharmaceutical evaporation crystallization tank according to claim 1, wherein: the back of the condensation tank body (9) is provided with a cold air box (22), an adjusting rotating handle (23) is arranged above the cold air box (22), the cold air box (22) is electrically connected with a cold air spray head (28), the cold air spray head (28) is arranged on the inner wall of the condensation tank body (9), and the surface of the adjusting rotating handle (23) is provided with temperature adjustment scales.

6. A pharmaceutical evaporation crystallization tank according to claim 1, wherein: the output end of the electric heater (16) is provided with a control valve (24), one end of the control valve (24) is communicated with a heat-conducting pipeline (17), and the top of the control valve (24) is provided with a handle.