CN220237783U - Raw material rectification equipment for improving quality of mixed xylenes - Google Patents
Raw material rectification equipment for improving quality of mixed xylenes Download PDFInfo
- Publication number
- CN220237783U CN220237783U CN202321523122.XU CN202321523122U CN220237783U CN 220237783 U CN220237783 U CN 220237783U CN 202321523122 U CN202321523122 U CN 202321523122U CN 220237783 U CN220237783 U CN 220237783U
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- CN
- China
- Prior art keywords
- barrel
- fixed mounting
- rectifying
- storage barrel
- mixed xylenes
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- 239000008096 xylene Substances 0.000 title claims abstract description 52
- 239000002994 raw material Substances 0.000 title claims abstract description 16
- 150000003738 xylenes Chemical class 0.000 title claims abstract description 13
- 239000007788 liquid Substances 0.000 claims abstract description 50
- 238000007790 scraping Methods 0.000 claims description 6
- 230000001681 protective effect Effects 0.000 claims description 4
- 238000003780 insertion Methods 0.000 claims description 2
- 230000037431 insertion Effects 0.000 claims description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 abstract description 41
- 238000001816 cooling Methods 0.000 abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 4
- 238000000034 method Methods 0.000 description 5
- 230000006378 damage Effects 0.000 description 4
- 239000000428 dust Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 208000027418 Wounds and injury Diseases 0.000 description 2
- 208000014674 injury Diseases 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 230000001360 synchronised effect Effects 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000000976 ink Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 229940078552 o-xylene Drugs 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000007170 pathology Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Extraction Or Liquid Replacement (AREA)
Abstract
The utility model discloses raw material rectifying equipment for improving the quality of mixed xylenes, which comprises a storage barrel, wherein a supporting leg is fixedly arranged at the bottom of the storage barrel, a liquid outlet pipe is fixedly arranged at the bottom of the storage barrel, a valve is fixedly arranged at one side of the liquid outlet pipe, a filter block is fixedly arranged in the storage barrel, a supporting column is fixedly arranged at the top of the storage barrel, a rectifying barrel is fixedly arranged at the other end of the supporting column, a cooler is fixedly arranged at the top of the storage barrel, and a drainage tube is fixedly arranged at one side of the cooler. The inside of rectifying barrel is inserted through the one end of the drainage tube that sets up, and the xylene liquid in rectifying barrel is through rectifying the back, enters into the inside of cooler by the drainage tube and makes its cooling, and not cools off through water to the cooling rate accelerates and the resource reduces, and when the device was used, the gear was rotatory through the drive of motor, thereby drives hollow tooth post and motor rotation, thereby produced the effect of kinetic energy.
Description
Technical Field
The utility model belongs to the technical field of chemistry, and particularly relates to raw material rectification equipment for improving the quality of mixed xylenes.
Background
Xylene is widely used as a solvent in the industries of paint, resin, dye, ink and the like; the method is used for synthesizing monomers or solvents in the industries of medicines, explosives, pesticides and the like; can also be used as a high-octane gasoline component and is an important raw material for organic chemical industry. It can also be used for removing asphalt from the car body. The hospital pathology department is mainly used for tissue and slice transparency and dewaxing, the industrial o-xylene is used as a raw material, firstly, the raw material is washed by industrial concentrated sulfuric acid until an acid layer is colorless, then, the raw material is washed by 10% sodium hydroxide solution and water in sequence until the raw material is qualified, the water layer is separated, then, the raw material is dried by anhydrous calcium chloride, and then, the raw material is rectified, after the distillate is clear, the middle distillate is collected to obtain a pure product, and when the raw material is in actual use, the cooling effect cannot keep up, the separation of the xylene is unclear, the rectification quality of the product is poor, and the heat energy waste is serious.
Disclosure of Invention
Aiming at the defects existing in the prior art, the utility model aims to provide raw material rectifying equipment for improving the quality of mixed xylenes, which solves the problems of poor rectifying quality and cooling.
In order to achieve the above purpose, the present utility model provides the following technical solutions: the utility model provides a raw materials rectifying apparatus for mixing xylene quality promotes, includes the storage bucket, the bottom fixed mounting of storage bucket has the supporting leg, the bottom fixed mounting of storage bucket has the drain pipe, one side fixed mounting of drain pipe has the valve, the inside fixed mounting of storage bucket has the filter block, the top fixed mounting of storage bucket has the support column, the other end fixed mounting of support column has the rectifying barrel, the top fixed mounting of storage bucket has the cooler, one side fixed mounting of cooler has the drainage tube, the top fixed mounting of rectifying barrel has the motor, the one end fixed mounting of motor has the gear, the side meshing of gear has hollow tooth post, the inside movable insertion of hollow tooth post has the feed liquor pipe, the surface fixed mounting of linkage feed liquor pipe has the liquefaction fill, the one end fixed mounting of hollow tooth post has the carousel, one side fixed mounting of carousel has the post, the inner chamber bottom movable mounting of rectifying barrel has the rectifying barrel, the surface fixed mounting of placing the liquid barrel has the scraper blade, the bottom fixed mounting of rectifying barrel has the heating device, the bottom of rectifying barrel has the drain hole.
Preferably, one end of the drainage tube is inserted into the rectifying barrel, and the other end of the drainage tube is fixedly provided with a cooler.
Through above-mentioned technical scheme, the advantage lies in that the inside of rectifying barrel is inserted to the one end of drainage tube, and the xylene liquid in rectifying barrel is after rectifying, enters into the inside of cooler by the drainage tube and makes its cooling, and does not cool through water to cooling rate accelerates and the resource reduces.
Preferably, one end of the hollow tooth column is movably inserted into the interior of the rectifying barrel to be fixedly connected with the turntable.
Through above-mentioned technical scheme, advantage lies in that when the device is used, the gear passes through the drive rotation of motor to drive hollow tooth post and motor rotation, thereby produce the effect of kinetic energy.
Preferably, one end of the linkage column is fixedly provided with a rotary table, and the other end of the linkage column is fixedly provided with a scraping plate.
Through above-mentioned technical scheme, advantage lies in the one end fixed mounting carousel of linkage post, the other end fixed mounting scraper blade to drive the carousel through hollow tooth post and rotate, synchronous drive scraper blade and put the liquid bucket and rotate, thereby scrape the xylene after the rectification of rectification barrel bottom portion.
Preferably, the surface of the liquid inlet pipe is fixedly provided with a liquefaction bucket, and the specification and the size of the liquid inlet pipe are matched with those of the liquefaction bucket.
Through above-mentioned technical scheme, advantage lies in that the liquefaction fill is fixed in the top of putting the liquid bucket through the feed liquor pipe to xylene in putting the liquid bucket is through heating evaporation to the inside liquefaction of liquefaction fill, along with the inner wall of liquefaction fill flows into the bottom of rectifying tank downwards, and the rotation of rethread scraper blade scrapes and moves the inside downstream of liquid outlet.
Preferably, a protective box is fixedly arranged at the top of the rectifying barrel.
Through above-mentioned technical scheme, advantage lies in the protective housing through rectifying barrel top installation to parts such as motor and gear are protected, have also prevented simultaneously that the device during operation from producing the injury to the people.
Preferably, a filter block is fixedly arranged in the storage barrel.
Through the technical scheme, the xylene after rectification is cooled by the cooler and then enters the storage barrel, and the filter block is fixedly arranged in the storage barrel, so that the xylene after rectification and cooling is filtered, and dust absorption of the xylene in the flowing process is prevented.
Compared with the prior art, the utility model has the beneficial effects that:
1. the inside of rectifying barrel is inserted through the one end of the drainage tube that sets up, after rectifying barrel's xylene liquid is through rectifying, enter into the inside of cooler by the drainage tube and make its cooling, and not cool off through water, thereby cooling rate accelerates and the resource reduces, when the device is used, the gear passes through the drive rotation of motor, thereby drive hollow tooth post and motor rotation, thereby produce the effect of kinetic energy, the one end fixed mounting carousel of linkage post, the other end fixed mounting scraper blade, thereby drive the carousel rotation through hollow tooth post, synchronous drive scraper blade and put the liquid bucket and rotate, thereby scrape the xylene after rectifying barrel bottom rectification.
2. The liquefied bucket is fixed above the liquid containing bucket through the liquid inlet pipe, thereby the xylene in the liquid containing bucket is heated and evaporated to be liquefied in the liquefied bucket, the xylene flows downwards to the bottom of the rectifying bucket along with the inner wall of the liquefied bucket, the xylene flows downwards to the bottom of the rectifying bucket through the scraping plate, the xylene flows downwards through the liquid outlet, the protecting box is arranged at the top of the rectifying bucket, the motor, the gear and other parts are protected, the damage to the person is prevented during the working of the device, the xylene after the rectification is cooled by the cooler and then enters the storage bucket, the filter block is fixedly arranged in the storage bucket, and the xylene after the rectification cooling is filtered, so that the xylene is prevented from adsorbing dust in the flowing process.
Drawings
FIG. 1 is a schematic front perspective view of the present utility model;
FIG. 2 is a schematic top perspective view of the present utility model;
FIG. 3 is a schematic perspective view of an axial structure of the present utility model;
fig. 4 is a schematic cross-sectional perspective view of the present utility model.
In the figure: 1. a storage tub; 2. support legs; 3. a liquid outlet pipe; 4. a valve; 5. a support column; 6. a drainage tube; 7. a heater; 8. a cooler; 9. a rectifying barrel; 10. a protective box; 11. a liquid inlet pipe; 12. a hollow tooth column; 13. a gear; 14. a motor; 15. a turntable; 16. a linkage column; 17. a liquefaction bucket; 18. a liquid placing barrel; 19. a scraper; 20. a liquid outlet; 21. and a filter block.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and fully with reference to the accompanying drawings, in which it is evident that the embodiments described are only some, but not all embodiments of the utility model. All other embodiments, which can be made by one of ordinary skill in the art without undue burden on the person of ordinary skill in the art based on the embodiments of the present utility model, are within the scope of the present utility model.
As shown in fig. 1-4, a raw material rectifying device for improving the quality of mixed xylenes comprises a storage barrel 1, a supporting leg 2 is fixedly installed at the bottom of the storage barrel 1, a liquid outlet pipe 3 is fixedly installed at the bottom of the storage barrel 1, a valve 4 is fixedly installed at one side of the liquid outlet pipe 3, a filter block 21 is fixedly installed inside the storage barrel 1, a supporting column 5 is fixedly installed at the top of the storage barrel 1, a rectifying barrel 9 is fixedly installed at the other end of the supporting column 5, a cooler 8 is fixedly installed at the top of the storage barrel 1, a drainage tube 6 is fixedly installed at one side of the cooler 8, a motor 14 is fixedly installed at the top of the rectifying barrel 9, a gear 13 is fixedly installed at one end of the motor 14, a hollow tooth column 12 is meshed on the side surface of the gear 13, a liquid inlet pipe 11 is movably inserted into the hollow tooth column 12, a rotary table 15 is fixedly installed at one end of the hollow tooth column 12, a linkage column 16 is fixedly installed at one side of the rotary table 15, a liquid placing barrel 18 is movably installed at the bottom of an inner cavity of the rectifying barrel 9, a scraper blade 19 is fixedly installed at the surface of the liquid placing barrel 18, a heating port 20 is fixedly installed at the bottom of the rectifying barrel 9, and a liquid outlet 20 is fixedly installed at the bottom of the rectifying barrel 9.
The working principle of the technical scheme is as follows:
one end of the drainage tube 6 is inserted into the rectification barrel 9, after the xylene liquid in the rectification barrel 9 is rectified, the xylene liquid enters into the cooler 8 through the drainage tube 6 to be cooled, and the xylene liquid is not cooled through water, so that the cooling speed is increased and resources are reduced.
In another embodiment, as shown in fig. 1-4, the liquefying hopper 17 is fixed above the liquid placing barrel 18 through the liquid inlet pipe 11, so that the xylene in the liquid placing barrel 18 is heated and evaporated to be liquefied in the liquefying hopper 17, and flows downwards to the bottom of the rectifying barrel 9 along with the inner wall of the liquefying hopper 17, and then flows downwards to the inner part of the liquid outlet 20 through the rotation of the scraping plate 19.
In another embodiment, as shown in fig. 1-4, the protection box 10 arranged at the top of the rectifying barrel 9 protects the motor 14, the gear 13 and other parts, and also prevents injury to people during the operation of the device.
In another embodiment, as shown in fig. 1 to 4, the rectified xylene is cooled by the cooler 8 and then enters the storage tank 1, and the filter block 21 is fixedly installed through the inside of the storage tank 1, so that the rectified and cooled xylene is filtered, and the xylene is prevented from adsorbing dust in the flowing process.
The working principle and the using flow of the utility model are as follows: one end of the drainage tube 6 is inserted into the rectification barrel 9, after the xylene liquid in the rectification barrel 9 is rectified, the xylene liquid enters into the cooler 8 through the drainage tube 6 to be cooled, and the xylene liquid is not cooled through water, so that the cooling speed is increased and resources are reduced.
The liquefaction bucket 17 is fixed above the liquid containing barrel 18 through the liquid inlet pipe 11, thereby xylene in the liquid containing barrel 18 is heated and evaporated to be liquefied in the liquefaction bucket 17, the xylene after rectification cooling is filtered through the filter block 21 in the storage barrel 1 along with the downward inflow of the inner wall of the liquefaction bucket 17 to the bottom of the rectification barrel 9, the xylene is scraped to flow down in the liquid outlet 20 through the rotation of the scraper 19, the parts such as the motor 14 and the gear 13 are protected through the protection box 10 arranged at the top of the rectification barrel 9, meanwhile, the damage to people is prevented when the device works, the rectified xylene is cooled by the cooler 8 and then enters the storage barrel 1, and the xylene after rectification cooling is prevented from adsorbing dust in the flowing process.
When the device is used, xylene to be rectified is poured into the liquid containing barrel 18 through the liquid inlet pipe 11, then the motor 14 is started to drive the gear 13 to rotate, meanwhile, the hollow toothed column 12 meshed with the gear 13 synchronously rotates, then the rotary disk 15 arranged at one end of the hollow toothed column 12 rotates to enable the scraping plate 19 and the liquid containing barrel 18 to start rotating through the connection of the linkage column 16, then the heater 7 is started to heat and evaporate the xylene in the liquid containing barrel 18, the evaporated gas rises to the inside of the liquefaction bucket 17 to liquefy, the evaporated gas flows downwards to the bottom of the rectification barrel 9 along with the inner wall of the liquefaction bucket 17, then flows into the liquid outlet 20 through the rotation of the scraping plate 19, enters the cooler 8 through the drainage tube 6 to be cooled, the rectified and cooled xylene enters the storage barrel 1 to be filtered and flows to the bottom of the storage barrel 1 through the filter block 21 for one time, and when the xylene needs to be taken, the xylene in the rotation 41 can flow out through the liquid outlet pipe 3.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. Raw material rectification equipment for improving quality of mixed xylenes, comprising a storage barrel (1), and being characterized in that: the utility model discloses a rectification device, including storage barrel (1), motor (14) and rotary disc (15), including storage barrel (1), supporting leg (2) are fixed mounting in the bottom of storage barrel (1), drain pipe (3) are fixed mounting in the bottom of storage barrel (1), one side fixed mounting of drain pipe (3) has valve (4), the inside fixed mounting of storage barrel (1) has filter block (21), the top fixed mounting of storage barrel (1) has support column (5), the other end fixed mounting of support column (5) has rectifying barrel (9), the top fixed mounting of storage barrel (1) has cooler (8), one side fixed mounting of cooler (8) has drainage tube (6), the top fixed mounting of rectifying barrel (9) has motor (14), one end fixed mounting of motor (14) has gear (13), the side meshing of gear (13) has hollow tooth post (12), the inside movable insertion of hollow tooth post (12) has feed liquor pipe (11), the fixed surface of feed liquor pipe (11) installs liquefaction fill (17), one end fixed mounting of hollow tooth post (12) has rotary disc (15), one side fixed mounting of rotary disc (16) has inner chamber (18) fixed mounting of rotary disc (18), the bottom of the rectifying barrel (9) is fixedly provided with a heater (7), and the bottom of the rectifying barrel (9) is provided with a liquid outlet (20).
2. A feed rectification apparatus for upgrading mixed xylenes as claimed in claim 1, wherein: one end of the drainage tube (6) is inserted into the rectifying barrel (9), and the other end of the drainage tube is fixedly provided with a cooler (8).
3. A feed rectification apparatus for upgrading mixed xylenes as claimed in claim 1, wherein: one end of the hollow tooth column (12) is movably inserted into the interior of the rectifying barrel (9) to be fixedly connected with the rotary table (15).
4. A feed rectification apparatus for upgrading mixed xylenes as claimed in claim 1, wherein: one end of the linkage column (16) is fixedly provided with a rotary table (15), and the other end of the linkage column is fixedly provided with a scraping plate (19).
5. A feed rectification apparatus for upgrading mixed xylenes as claimed in claim 1, wherein: the surface of the liquid inlet pipe (11) is fixedly provided with a liquefying hopper (17), and the specification and the size of the liquid inlet pipe (11) are matched with those of the liquefying hopper (17).
6. A feed rectification apparatus for upgrading mixed xylenes as claimed in claim 1, wherein: the top of the rectifying barrel (9) is fixedly provided with a protective box (10).
7. A feed rectification apparatus for upgrading mixed xylenes as claimed in claim 1, wherein: the filter block (21) is fixedly arranged in the storage barrel (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321523122.XU CN220237783U (en) | 2023-06-15 | 2023-06-15 | Raw material rectification equipment for improving quality of mixed xylenes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321523122.XU CN220237783U (en) | 2023-06-15 | 2023-06-15 | Raw material rectification equipment for improving quality of mixed xylenes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220237783U true CN220237783U (en) | 2023-12-26 |
Family
ID=89229946
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321523122.XU Active CN220237783U (en) | 2023-06-15 | 2023-06-15 | Raw material rectification equipment for improving quality of mixed xylenes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220237783U (en) |
-
2023
- 2023-06-15 CN CN202321523122.XU patent/CN220237783U/en active Active
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