CN116216827A - Device for recycling organic solvent from organic waste liquid in manufacturing industry - Google Patents
Device for recycling organic solvent from organic waste liquid in manufacturing industry Download PDFInfo
- Publication number
- CN116216827A CN116216827A CN202310509023.4A CN202310509023A CN116216827A CN 116216827 A CN116216827 A CN 116216827A CN 202310509023 A CN202310509023 A CN 202310509023A CN 116216827 A CN116216827 A CN 116216827A
- Authority
- CN
- China
- Prior art keywords
- waste liquid
- kettle body
- gear
- reaction kettle
- fixedly connected
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 121
- 239000003960 organic solvent Substances 0.000 title claims abstract description 22
- 239000010815 organic waste Substances 0.000 title claims abstract description 21
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 19
- 238000004064 recycling Methods 0.000 title abstract description 9
- 238000006243 chemical reaction Methods 0.000 claims abstract description 75
- 230000005540 biological transmission Effects 0.000 claims abstract description 57
- 238000004140 cleaning Methods 0.000 claims description 34
- 230000000087 stabilizing effect Effects 0.000 claims description 6
- 244000309464 bull Species 0.000 claims description 4
- 238000009434 installation Methods 0.000 claims description 2
- 230000005012 migration Effects 0.000 claims description 2
- 238000013508 migration Methods 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 abstract description 54
- 239000000126 substance Substances 0.000 abstract description 50
- 238000009835 boiling Methods 0.000 abstract description 23
- 239000002699 waste material Substances 0.000 description 89
- 239000000463 material Substances 0.000 description 15
- 238000000034 method Methods 0.000 description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 238000004821 distillation Methods 0.000 description 6
- 238000000926 separation method Methods 0.000 description 5
- 230000008016 vaporization Effects 0.000 description 5
- 230000007613 environmental effect Effects 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
- 230000032683 aging Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 238000009834 vaporization Methods 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 239000002351 wastewater Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000009841 combustion method Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 238000012851 eutrophication Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/02—Treatment of water, waste water, or sewage by heating
- C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
- C02F1/043—Details
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/0804—Cleaning containers having tubular shape, e.g. casks, barrels, drums
- B08B9/0808—Cleaning containers having tubular shape, e.g. casks, barrels, drums by methods involving the use of tools, e.g. by brushes, scrapers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/0856—Cleaning of water-treatment installations
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention belongs to the technical field of organic solvents, and particularly relates to a device for recycling organic solvents from organic waste liquid in manufacturing industry, which comprises a reaction kettle body, wherein a cover body is arranged at the top end of the reaction kettle body, a motor is fixedly arranged at the top end of the cover body, a stable ferrule is fixedly connected with the bottom end of a mounting frame, the stable ferrule is fixedly connected with the inner wall of the reaction kettle body, a central shaft of a first gear is connected with the mounting frame through a bearing, a transmission frame is arranged in the stable ferrule, four ends of the transmission frame are fixedly connected with transmission blocks, and heating plates are fixedly connected with the bottom ends of the transmission blocks, so that substances in different areas with the same property can not reach different boiling points, and various substances are contained in steam, so that condensed liquid is impure, and the subsequent treatment is required.
Description
Technical Field
The invention relates to the technical field of organic solvent recovery, in particular to a device for recovering an organic solvent from organic waste liquid in manufacturing industry.
Background
The organic waste liquid is a liquid containing various harmful substances, which can cause eutrophication of water, and the combustion method is generally used for treating the organic waste liquid at the present stage, but the method can generate a large amount of carbon dioxide, and the treatment mode is unreasonable;
such as Chinese patent: a distillation recovery device and a method for hydrogen chloride in acid etching waste liquid, and the publication number is: CN203411428U, which is a device for recycling organic solvents in low concentration hydrochloric acid solution, by distillation and multi-stage recycling tower, can be further transferred to other absorption towers to increase recycling efficiency, and has low recycling cost, no new harmful substances are added and generated, but the device has the following problems:
1: when the reaction kettle is used for distilling the waste liquid, the existing reaction kettle only plays a role in holding and sealing, when the reaction kettle is heated, the bottom or other local areas are heated generally, the boiling points of the waste liquid of different substances in the waste liquid are different, the local heating mode can lead to uneven heating of the waste liquid at the middle part of the liquid or at the part far away from a heat source, the temperature of the internal liquid is in the process of continuously increasing, the temperature of the whole waste liquid is different, the temperature can reach the boiling points of two or more substances in the waste liquid, the steam still contains a plurality of substances, the substances cannot be separated independently, and the subsequent treatment is also needed;
2: after the waste liquid is heated, partial substances in the waste liquid can be solidified, so that the bottom and the inner wall of the reaction kettle are adhered, the follow-up cleaning is difficult, if the solidified substances are harmful substances, safety threat can be caused to workers during manual cleaning, and if the waste liquid is directly washed, the solidified substances are scattered on the periphery by water flow, and certain pollution can be caused after the solidified substances cannot be effectively cleaned.
Disclosure of Invention
The invention aims to provide a device for recycling an organic solvent from an organic waste liquid in manufacturing industry, so as to solve the problems that when the waste liquid is distilled by using a reaction kettle in the background technology, the existing reaction kettle only plays a role in holding and sealing, when the reaction kettle is heated, the bottom or other local areas are generally heated, the boiling points of waste liquid of different substances in the waste liquid are different, the local heating mode can lead to uneven heating of the waste liquid at the middle part of the liquid or at a part far away from a heat source, the temperature of the internal liquid is in the process of continuously increasing, the temperature of the whole waste liquid is different, the temperature can reach the boiling point of two or more substances in the waste liquid, the steam still contains a plurality of substances, the substances cannot be separated singly, the subsequent treatment is needed, part of the substances in the waste liquid can be solidified after the waste liquid is heated, the bottom and the inner wall of the reaction kettle are adhered, the subsequent difficult to clean, if the solidified substances are harmful substances, safety threat can be caused to workers during the manual cleaning, and if the waste liquid is directly washed, water flows and the peripheral substances are not cleaned effectively.
In order to achieve the above purpose, the present invention provides the following technical solutions: the utility model provides a retrieve device of organic solvent in follow manufacturing organic waste liquid, includes the reation kettle body, the lid is installed on the top of reation kettle body, the top fixed mounting of lid has the motor, the output of motor passes the inside that the lid extends to the reation kettle body, the inside of reation kettle body is provided with the mounting bracket, the bottom fixedly connected with of mounting bracket stabilizes the lasso, the inner wall fixed connection of stable lasso and reation kettle body, the centre of stable lasso bottom is provided with gear one, the top that the mounting bracket extends to the mounting bracket is passed to the center pin on gear one, be connected through the bearing between center pin and the mounting bracket of gear one, fixed connection between the center pin of gear one and the output of motor, the inside of stable lasso is provided with the drive frame, four ends of drive frame are all fixedly connected with drive block, the bottom of drive block is connected with the hot plate, the below of drive frame is provided with four sets of drive plates two, the top of drive plate is connected with the drive plate one through the bearing frame, the bottom of output valve body is connected with the side of reation kettle, the bottom of reation kettle is connected with the side of the side surface mounting bracket, the reactor is connected with the input flange, the reactor is connected with the side fixed connection.
Preferably, the inner wall of the stable ferrule is provided with a slide way, one side, close to each other, of the transmission block is fixedly connected with a first abutting block, two ends of the first abutting block are provided with pulleys through bearings, the pulleys are located in the slide way, and the upper side and the lower side of the pulleys are in contact with the inner wall of the slide way.
Preferably, one side that the conflict piece is first and is close to each other is the wave, evenly be provided with four group's gears two around the gear one, the top of gear two is all connected with the bottom of mounting bracket through the bearing, the bottom fixedly connected with conflict piece two of gear two, the end of conflict piece two is inconsistent with conflict piece one wave one side.
Preferably, the second gear and the first gear are meshed with each other, the first gear rotates for one circle, and the second gear rotates for four circles.
Preferably, push rods are arranged on two sides of the lower portion of the transmission disc, two groups of push rods are parallel to each other, two groups of push rods are respectively hinged to the first transmission disc and the second transmission disc on the same side, and the connecting positions of the push rods, the first transmission disc and the second transmission disc are located in the middle of two sides of the bottom ends of the first transmission disc and the second transmission disc.
Preferably, the bottom ends of the four groups of cleaning frames are contacted with the inner wall of the bottom end of the reaction kettle body, the bottom ends of the cleaning frames are provided with saw-tooth grooves, the length and width dimensions of the single group of cleaning frames are smaller than five centimeters of the radius of the inner wall of the bottom end of the reaction kettle body, namely, the four groups of cleaning frames can cover most areas of the inner wall of the bottom end of the reaction kettle body.
Preferably, the surface of bull stick is connected with the bearing mounting bracket through the bearing, and the bearing mounting bracket passes through the inner wall of bolt installation in reation kettle body side.
Preferably, the inside fixedly connected with sleeve pipe of output valve pipe, the sleeve pipe is hollow cylindric, the delivery outlet has been seted up to the inside one end that the sleeve pipe is located the reation kettle, the screw hole has been seted up to the outside one end that the sleeve pipe is located the reation kettle, the screw rod has been inserted to the inside of screw hole, be connected through the screw thread between screw rod and the screw hole, the end fixedly connected with control rod of screw rod, the control rod passes the output valve pipe and extends to the outside of output valve pipe.
Preferably, the inside of sleeve pipe is provided with the shutoff board, the diameter of shutoff board is greater than the delivery outlet, and the diameter of shutoff board is less than the diameter of sleeve pipe inner circle, the shutoff board receives sleeve pipe shape restriction can only be at the inside horizontal migration of sleeve pipe, the side parcel that the shutoff board is close to the delivery outlet has the seal cover, the shutoff of shutoff board with the delivery outlet.
Preferably, the screw is located the inside one end fixedly connected with push pedal of sleeve pipe, the centre department of shutoff board and push pedal is provided with the spring, the one end and the shutoff board fixed surface of spring are connected, the other end and the fixed surface of push pedal of spring are connected.
Compared with the prior art, the invention has the beneficial effects that:
through setting up the hot plate, the user is through four sets of hot plates for the hot plate heats the middle part of waste liquid, and take the waste liquid up through wobbling hot plate and flow, thereby make different waste liquids constantly with the hot plate contact heating, and four sets of hot plates are located four positions of waste liquid, further increase the area of heating, firstly make the waste liquid volume of heating simultaneously more, secondly, can increase the mobility of waste liquid through four sets of hot plates, increase the contact ageing of waste liquid and hot plate, synthesize above-mentioned, make the waste liquid can reach the effect of heating evenly in the reation kettle body, can not produce the local lower that heats, the condition that the local is higher, change the operation of heat transfer between the traditional waste liquid into waste liquid and directly contact with the heat source, thereby reach the boiling point fast, and can not produce the different time of material that the same nature different region reaches the boiling point, thereby lead to contain multiple material in the steam, thereby make the condensate liquid impure, lead to follow-up still need to handle, compare traditional reation kettle distillation mode, this device makes waste liquid reach the same temperature at same time, thereby make the condensate liquid that obtains the same material of distilling, it is convenient to carry out the follow-up again, the follow-up treatment again;
through setting up the clearance frame for the user is follow-up only to pour into clear water into the reation kettle body inside then start stable lasso, can control clearance frame swing and scrape the brush cleaning to reation kettle body bottom inner wall, thereby need not the user to open the lid and wash the manual work, avoid because during manual cleaning, inside harmful cured material produces the potential safety hazard to the staff, also avoid because during clear water washes, harmful cured material scatters in the device in the periphery, thereby with the surrounding environment pollution, do not obtain effective clearance when also avoiding surrounding environment scattering harmful material, follow-up causes secondary potential safety hazard to the staff, semi-automatic self-cleaning mode also makes things convenient for the staff follow-up to carry out quick clearance to the reation kettle body, do not need to consume a large amount of manual work and clear up the operation, increase the recovery extraction efficiency to organic solution in the waste liquid;
through setting up output valve pipe, the user is through the boiling point of the different materials in the waste liquid that is ready in advance, the internal pressure of reation kettle when calculating each material boiling point temperature again, then adjust the deformation degree of spring for the spring coefficient and the corresponding of pressure can of spring, the device passes through multiunit output valve pipe, the inside spring of adjusting of cooperation output valve pipe, the single material in the waste liquid reaches boiling point vaporization simultaneously in the cooperation hot plate, can make the internal single material of reation kettle evaporate the back and directly discharge through output valve pipe, obtain pure material, do not need follow-up separation, and make the user need not carry out unnecessary operation in the handling through output valve pipe, only need adjust the spring in advance can, and to different waste liquids, all can separate through adjusting the spring, make the device can adapt to the waste liquid of most materials.
Drawings
FIG. 1 is a schematic cross-sectional view of a three-dimensional structure of the present invention;
FIG. 2 is a schematic perspective view of the mounting bracket, gear one, heating plate and cleaning bracket of the present invention;
FIG. 3 is a schematic top view of a stabilization collar of the present invention;
FIG. 4 is a schematic perspective view of a gear I, a driving block and a stabilizing collar according to the present invention;
FIG. 5 is an exploded view of the transmission housing, gear one and gear two of the present invention;
FIG. 6 is a schematic bottom perspective view of a driving block, a second abutting block, a first driving disk and a second driving disk according to the present invention;
FIG. 7 is a schematic bottom perspective view of a first and a second driving disks according to the present invention;
FIG. 8 is a schematic cross-sectional view showing an opened state of an output valve tube according to the present invention;
FIG. 9 is a schematic cross-sectional view of the output valve tube in a closed state according to the present invention;
fig. 10 is a schematic elevational view of the present invention.
In the figure: 1. a reaction kettle body; 2. a cover body; 3. a motor; 4. a mounting frame; 5. stabilizing the ferrule; 6. a first gear; 7. a transmission frame; 8. a transmission block; 9. a first abutting block; 10. a second gear; 11. a second abutting block; 12. a heating plate; 13. a first transmission disc; 14. a second transmission disc; 15. a push rod; 16. a rotating rod; 17. a cleaning frame; 18. a flange input pipe; 19. an output valve tube; 20. a sleeve; 21. an output port; 22. a threaded hole; 23. a screw; 24. a control lever; 25. a plugging plate; 26. a spring; 27. a support frame; 28. and (5) discharging waste pipes.
Description of the embodiments
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
The invention is further described below with reference to examples.
Examples
The device for recycling organic solvent from organic waste liquid in manufacturing industry of the embodiment comprises a reaction kettle body 1, wherein a cover body 2 is arranged at the top end of the reaction kettle body 1, a motor 3 is fixedly arranged at the top end of the cover body 2, an output end of the motor 3 penetrates through the cover body 2 to extend into the reaction kettle body 1, a mounting frame 4 is arranged in the reaction kettle body 1, a stable ferrule 5 is fixedly connected with the bottom end of the mounting frame 4, the stable ferrule 5 is fixedly connected with the inner wall of the reaction kettle body 1, a gear I6 is arranged in the middle of the bottom end of the stable ferrule 5, a central shaft at the top end of the gear I6 penetrates through the mounting frame 4 to extend to the top end of the mounting frame 4, the central shaft of the gear I6 is connected with the mounting frame 4 through a bearing, the central shaft of the gear I6 is fixedly connected with the output end of the motor 3, and a heating plate 12 is fixedly connected with the bottom end of a transmission block 8.
Further, the inside of stabilizing lasso 5 is provided with drive frame 7, four ends of drive frame 7 all fixedly connected with drive block 8, the slide has been seted up to the inner wall of stabilizing lasso 5, the pulley is all installed through the bearing at the both ends of conflict block one 9, the pulley is located the inside of slide, the upper and lower both sides of pulley all contacts with the inner wall of slide, the one side that drive block 8 is close to each other all fixedly connected with conflict block one 9, the one side that conflict block one 9 is close to each other is the wave form, evenly be provided with four sets of gears two 10 around gear one 6, the top of gear two 10 all is connected with the bottom of mounting bracket 4 through the bearing, the bottom fixedly connected with conflict block two 11 of gear two 10, the end of conflict block two 11 is inconsistent with conflict block one 9 wave one side, intermeshing between gear two 10 and gear one 6, gear one 6 rotates one round, gear two 10 rotates four rounds.
In the embodiment, when the device starts to be used, firstly, a user connects a pipeline for outputting waste liquid with a flange input pipe 18, the waste liquid is input into the reaction kettle body 1 through the flange input pipe 18, after the input is finished, the user seals the flange input pipe 18, then a motor 3 and a heating plate 12 are started, the output end of the motor 3 starts to rotate, the heating plate 12 starts to heat the waste liquid, when the output end of the motor 3 drives a gear I6 to rotate, the gear I6 is meshed with a gear II 10 to drive a gear II 10 to rotate, the gear II 10 is fixedly connected with a collision block II 11, the collision block II 11 and the gear II 10 rotate in the same direction and at the same speed, the collision block II 11 and one side of the collision block I9 wave form, the collision block I9 swings left and right, the transmission block 8 drives the heating plate 12 at the bottom end to swing left and right, the heating plate 12 is positioned in the middle of the inside of the reaction kettle body 1, the middle part of the waste liquid is heated through the heating plate 12, the heating plate 12 is in a cross plate shape, in the swinging process of the heating plate 12, the waste liquid is driven to flow in the inside of the reaction kettle body 1, namely, the waste liquid continuously flows to enable the waste liquid contacted with the heating plate 12 to be continuously changed, so that the waste liquid is heated more uniformly, through the arrangement of the heating plate 12, a user passes through four groups of heating plates 12, the heating plate 12 heats the middle part of the waste liquid, and brings the waste liquid up to flow through the swinging heating plate 12, so that different waste liquids are continuously contacted with the heating plate 12 to be heated, the four groups of heating plates 12 are positioned at four positions of the waste liquid, the heating area is further increased, the quantity of the waste liquid which is heated simultaneously is more, and the fluidity of the waste liquid can be increased through the four groups of heating plates 12, the contact ageing of waste liquid and heating plate 12 is increased, synthesize the aforesaid, make the waste liquid can reach the even effect of being heated in reation kettle body 1, can not produce the part and be heated lowly, the part is heated higher condition, change the operation of heat transfer between the traditional waste liquid into waste liquid direct and heat source contact heat absorption, thereby reach the boiling point fast, and can not produce the material in the different regions of the same nature and reach the time difference of boiling point, thereby it contains multiple material to lead to in the steam, thereby it is impure to make the condensate liquid, lead to follow-up still need to handle, compare traditional reation kettle distillation's mode, this device makes the waste liquid reach the same temperature at the same time, thereby make the distillation condensate liquid same material that obtains, it is convenient fast, do not need follow-up to handle again.
Examples
In other aspects, this embodiment further provides a device for recovering an organic solvent from an organic waste liquid in manufacturing industry, as shown in fig. 1-10, a first transmission disc 13 is disposed below the transmission block 8, four second transmission discs 14 are disposed below the transmission frame 7, the top ends of the second transmission discs 14 are connected with the bottom ends of the transmission frame 7 through bearings, the first transmission disc 13 is fixed on the top end of the surface of the heating plate 12, the bottom ends of the second transmission discs 14 are fixedly connected with a rotating rod 16, and the bottom ends of the rotating rod 16 are fixedly connected with a cleaning frame 17.
Further, push rods 15 are arranged on two sides below the first transmission disc 13, the two groups of push rods 15 are parallel to each other, two ends of the two groups of push rods 15 are respectively hinged to the first transmission disc 13 and the second transmission disc 14 on the same side, the connecting positions of the push rods 15 and the first transmission disc 13 and the second transmission disc 14 are located in the middle of two sides of the bottom ends of the first transmission disc 13 and the second transmission disc 14, the bottom ends of the four groups of cleaning frames 17 are in contact with the inner wall of the bottom end of the reaction kettle body 1, saw-tooth-shaped grooves are formed in the bottom ends of the cleaning frames 17, the length and width of the single group of cleaning frames 17 are smaller than five centimeters of the radius of the inner wall of the bottom end of the reaction kettle body 1, namely, the four groups of cleaning frames 17 can cover most of the area of the inner wall of the bottom end of the reaction kettle body 1, the surface of the rotary rod 16 is connected with a bearing mounting frame through a bearing, and the bearing mounting frame is mounted on the inner wall of the side surface of the reaction kettle body 1 through bolts.
When the device is cleaned by a user, when the heating plate 12 is vibrated by the aid of the transmission block 8 and the abutting block two 11, the transmission block 8 is driven to swing when the transmission block 8 swings, so that two groups of push rods 15 are driven to swing, at the moment, the push rods 15 push the transmission disc two 14 and the transmission disc one 13 to swing in the same direction and at the same angle, thereby the rotating rod 16 at the bottom end of the transmission disc two 14 is driven by the transmission disc two 14 to swing, the four groups of cleaning frames 17 are driven by the rotating rod 16 to swing, the serrated grooves at the bottom end of the cleaning frames 17 are formed, the inner wall at the bottom end of the reaction kettle body 1 is scraped and brushed, after the solidified substance bonded at the bottom end of the reaction kettle body 1 is separated from the reaction kettle body 1, the solidified substance is filled into the interior of the reaction kettle body 1, the waste discharge pipe 28 is opened again, and the waste water is discharged for centralized treatment, and the cleaning frames 17 are arranged, so that the inner wall at the bottom of the reaction kettle body 1 is driven to be cleaned by the control the swinging of the cleaning frames 17, the user is not required to open the cover body 2, the manual cleaning is performed, the hidden danger is avoided from the cleaning device to be polluted by the environment, the user is avoided from the environmental protection of the environment, and the environmental protection is high-friendly device is convenient, and the environmental protection is caused by the environmental protection.
Examples
In other aspects, this embodiment also provides a device for recovering an organic solvent from an organic waste liquid in manufacturing industry, as shown in fig. 1-10, a flange input pipe 18 is installed on a side surface of a reaction kettle body 1, the flange input pipe 18 is communicated with the inside of the reaction kettle body 1, an output valve pipe 19 is installed on a side surface of the reaction kettle body 1, the output valve pipe 19 is communicated with the inside of the reaction kettle body 1, a supporting frame 27 is fixedly connected to the surface of the reaction kettle body 1, and a waste discharging pipe 28 is fixedly connected to the bottom end of the reaction kettle body 1.
Further, the inside fixedly connected with sleeve pipe 20 of output valve pipe 19, sleeve pipe 20 is hollow cylindric, the one end that sleeve pipe 20 is located the inside of reation kettle body 1 has seted up delivery outlet 21, threaded hole 22 has been seted up to the one end that sleeve pipe 20 is located the outside of reation kettle body 1, threaded hole 22's inside has inserted screw rod 23, be connected through the screw thread between screw rod 23 and the threaded hole 22, the end fixedly connected with control rod 24 of screw rod 23, control rod 24 passes the outside that output valve pipe 19 extends to output valve pipe 19, the inside of sleeve pipe 20 is provided with shutoff board 25, the cross section of shutoff board 25 is circular, the diameter of shutoff board 25 is greater than delivery outlet 21, the diameter of shutoff board 25 is less than the diameter of sleeve pipe 20 inner circle, the shutoff board 25 is limited by sleeve pipe 20 shape only, the side parcel that shutoff board 25 is close to delivery outlet 21 has the seal cover, the shutoff board 25 cooperation seal cover will delivery outlet 21, the one end fixedly connected with the push pedal of screw rod 23 inside sleeve pipe 20, the middle part of shutoff board 25 and push pedal is provided with spring 26, the one end and the shutoff board 25 surface fixedly connected with shutoff board 25 of spring 26.
In the embodiment, when the waste liquid is heated in the reaction kettle body 1, the boiling points of different substances are different, when the different substances in the waste liquid are boiled and vaporized, the obtained steam is a single substance, the reaction kettle body 1 is a sealed container, the internal pressure is in direct proportion to the internal temperature, the elastic coefficient of the spring 26 is fixed, the user calculates the pressure in the reaction kettle body 1 at different temperatures and then rotates the control rod 24, so that the control rod 24 drives the screw 23 to move towards the inside of the sleeve 20, the spring 26 is extruded by the push plate, the spring 26 is deformed, the elastic coefficient of the spring 26 is in direct proportion to the deformation degree of the spring 26, the user adjusts the deformation degree of the spring 26, so that the elastic coefficient of the spring 26 corresponds to the pressure at a certain temperature in the reaction kettle body 1, and when the reaction kettle body 1 reaches a certain temperature, the method comprises boiling and vaporizing a substance in the waste liquid, simultaneously, the pressure in the reaction kettle body 1 corresponds to the spring coefficient of a group of springs 26 in the output valve tube 19, at the moment, the plugging plate 25 is pushed to move by the pressure in the reaction kettle body 1, so that the plugging plate 25 no longer plugs the output port 21, the substance after boiling and vaporizing passes through the output port 21 and is discharged by the output valve tube 19, a user connects a condensing tube with the output valve tube 19, the vaporized substance is output by the condensing tube and condensed into liquid, by setting the output valve tube 19, the user calculates the pressure in the reaction kettle body 1 when the boiling point temperature of each substance is prepared in advance, then adjusts the deformation degree of the springs 26, so that the spring coefficient of the springs 26 corresponds to the pressure, the single substance in the waste liquid reaches the boiling point vaporization simultaneously by matching with the heating plate 12, the single substance in the reaction kettle body 1 can be directly discharged through the output valve pipe 19 after being vaporized, so that pure substances are obtained, the subsequent separation is not needed, a user does not need to perform redundant operation in the treatment process through the output valve pipe 19, the spring 26 is only needed to be adjusted in advance, and the separation can be performed by adjusting the spring 26 for different waste liquids, so that the device can adapt to the waste liquid of most substances.
The complete working principle and working process of the technical scheme are as follows:
when the device starts to be used, firstly, a user connects a pipeline for outputting waste liquid with a flange input pipe 18, the waste liquid is input into the reaction kettle body 1 through the flange input pipe 18, after the input is finished, the user seals the flange input pipe 18, then a motor 3 and a heating plate 12 are started, the output end of the motor 3 starts to rotate, the heating plate 12 starts to heat the waste liquid, after the output end of the motor 3 drives a gear I6 to rotate, the gear I6 is meshed with a gear II 10, thereby driving four groups of gears II 10 to rotate, the gear II 10 is fixedly connected with a collision block II 11, then the collision block II 11 and the gear II 10 rotate at the same speed in the same direction, the collision block II 11 collides with one side of a collision block 9 in a wave mode, so that the collision block I9 swings left and right, a transmission block 8 swings left and right, the transmission block 8 drives the heating plate 12 at the bottom end to swing left and right, the heating plate 12 is positioned in the middle of the inside of the reaction kettle body 1, the middle part of the waste liquid is heated through the heating plate 12, the heating plate 12 is in a cross plate shape, in the swinging process of the heating plate 12, the waste liquid is driven to flow in the inside of the reaction kettle body 1, namely, the waste liquid continuously flows to enable the waste liquid contacted with the heating plate 12 to be continuously changed, so that the waste liquid is heated more uniformly, through the arrangement of the heating plate 12, a user passes through four groups of heating plates 12, the heating plate 12 heats the middle part of the waste liquid, and brings the waste liquid up to flow through the swinging heating plate 12, so that different waste liquids are continuously contacted with the heating plate 12 to be heated, the four groups of heating plates 12 are positioned at four positions of the waste liquid, the heating area is further increased, the quantity of the waste liquid which is heated simultaneously is more, and the fluidity of the waste liquid can be increased through the four groups of heating plates 12, the contact aging of the waste liquid and the heating plate 12 is increased, the effect of uniform heating of the waste liquid in the reaction kettle body 1 is comprehensively achieved, the situation that the local heating is lower and the local heating is higher is avoided, the operation of heat transfer between traditional waste liquid is changed into the condition that the waste liquid directly contacts with a heat source to absorb heat, so that the boiling point is quickly reached, the time difference of the boiling points of substances in the same property different areas is avoided, the steam is caused to contain various substances, the condensed liquid is impure, the subsequent treatment is caused, and compared with the distillation mode of the traditional reaction kettle, the device enables the waste liquid to reach the same temperature at the same time, so that the obtained distilled condensed liquid is quick and convenient, and the subsequent treatment is not needed;
when a user cleans the device, when the heating plate 12 is rocked by the transmission block 8 and the abutting block two 11 in a left-right matching way, the transmission block 8 is driven to sway, so that the two groups of push rods 15 are driven to sway, at the moment, the push rods 15 push the transmission disc two 14 and the transmission disc one 13 to sway in the same direction and in the same angle, thereby the transmission disc two 14 drives the rotating rod 16 at the bottom end of the transmission disc two 14 to sway, the rotating rod 16 drives the four groups of cleaning frames 17 to sway, the serrated grooves at the bottom end of the cleaning frames 17 are used for scraping the inner wall at the bottom end of the reaction kettle body 1, the solidified substances adhered at the bottom end of the reaction kettle body 1 are separated from the reaction kettle body 1, then the clear water and the solidified substances are filled into the reaction kettle body 1, the leaked waste water is discharged for centralized treatment, and then the cleaning frames 17 are arranged, so that the user only needs to fill the clear water into the reaction kettle body 1, and then the stable ring 5 is started, the swinging of the cleaning frames 17 is controlled to scrape the inner wall at the bottom end of the reaction kettle body 1, thus the user is not required to open the cover body 2 for manual cleaning, the inner wall is required to be cleaned, the hidden danger is avoided, the hidden danger is also caused by the fact that the user is cleaned by the automatic cleaning device is polluted in the environment, and the environment is also is convenient to clean the environment, and the surrounding the environment is not polluted, and the subsequent cleaning device is polluted in the environment is cleaned by the environment, and the environment is also is convenient to be cleaned and polluted;
when the waste liquid is heated in the reaction kettle body 1, boiling points of different substances are different, when different substances in the waste liquid boil and vaporize, single substance is in the obtained steam, the reaction kettle body 1 is a sealed container, the internal pressure is in direct proportion to the internal temperature, the elastic coefficient of the spring 26 is fixed, a user calculates the internal pressure of the reaction kettle body 1 at different temperatures and then rotates the control rod 24 to drive the screw rod 23 to move towards the inside of the sleeve 20, so that the spring 26 is extruded by the push plate, the spring 26 deforms, the elastic coefficient of the spring 26 is in direct proportion to the deformation degree of the spring 26, the user adjusts the deformation degree of the spring 26 to ensure that the elastic coefficient of the spring 26 corresponds to the pressure at a certain temperature in the reaction kettle body 1, when the internal pressure of the reaction kettle body 1 reaches a certain temperature, a certain substance in the waste liquid boils and vaporizes, meanwhile, the pressure inside the reaction kettle body 1 corresponds to the spring coefficient of the springs 26 inside a group of output valve pipes 19, at the moment, the plugging plate 25 is pushed to move by the pressure inside the reaction kettle body 1, so that the plugging plate 25 no longer plugs the output port 21, at the moment, the boiled and vaporized substances pass through the output port 21 and are discharged through the output valve pipes 19, a user connects the condensing pipes with the output valve pipes 19, the vaporized substances are output through the condensing pipes and condensed into liquid, by arranging the output valve pipes 19, the user calculates the pressure inside the reaction kettle body 1 when the boiling point temperature of each substance is calculated by preparing the boiling point of different substances in waste liquid in advance, then the deformation degree of the springs 26 is adjusted, so that the spring coefficient of the springs 26 corresponds to the pressure, the device is matched with the springs 26 adjusted inside the output valve pipes 19 through a plurality of groups of output valve pipes 19, the single substance in the waste liquid reaches the boiling point vaporization simultaneously by matching with the heating plate 12, the single substance in the reaction kettle body 1 can be directly discharged through the output valve pipe 19 after being vaporized, so that pure substances are obtained, the subsequent separation is not needed, a user does not need to perform redundant operation in the treatment process through the output valve pipe 19, the spring 26 is only needed to be adjusted in advance, and the separation can be performed by adjusting the spring 26 for different waste liquids, so that the device can adapt to the waste liquid of most substances.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are, therefore, to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (10)
1. The utility model provides a retrieve device of organic solvent in follow manufacturing organic waste liquid, includes reation kettle body (1), its characterized in that: the utility model discloses a reaction kettle, including a reaction kettle body (1), a motor (3) is installed on the top of reaction kettle body (1), top fixed mounting of lid (2) has motor (3), the output of motor (3) passes the inside that lid (2) extended to reaction kettle body (1), the inside of reaction kettle body (1) is provided with mounting bracket (4), the bottom fixedly connected with of mounting bracket (4) stabilizes lasso (5), the middle department of stabilizing lasso (5) bottom is provided with gear one (6), the center pin on gear one (6) top passes mounting bracket (4) and extends to the top of mounting bracket (4), be connected through the bearing between the center pin of gear one (6) and mounting bracket (4), fixed connection between the center pin of gear one (6) and the output of motor (3), the inside of stabilizing lasso (5) is provided with drive frame (7), four end fixedly connected with drive blocks (8) of drive frame (7), drive blocks (8) are all connected with each other, drive plate one (14) are all connected with drive plate (7) below, drive plate one (12) are all provided with drive plate (13), the top of driving disk two (14) is connected with the bottom of drive frame (7) through the bearing, driving disk one (13) is fixed in the top on hot plate (12) surface, the bottom fixedly connected with bull stick (16) of driving disk two (14), the bottom of bull stick (16) all fixedly connected with clearance frame (17), flange input tube (18) are installed to the side-mounting of reactor body (1), flange input tube (18) are linked together with the inside of reactor body (1), output valve pipe (19) are installed to the side-mounting of reactor body (1), output valve pipe (19) are linked together with the inside of reactor body (1), reactor body (1) surface fixedly connected with support frame (27), the bottom fixedly connected with of reactor body (1) lets out useless pipe (28).
2. An apparatus for recovering organic solvent from organic waste liquid of manufacturing industry as defined in claim 1, wherein: the inner wall of stable lasso (5) has seted up the slide, one side that transmission piece (8) are all close to each other is all fixedly connected with conflict piece (9), the pulley is all installed through the bearing to the both ends of conflict piece (9), and the pulley is located the inside of slide, and the upper and lower both sides of pulley all contact with the inner wall of slide.
3. An apparatus for recovering organic solvent from organic waste liquid of manufacturing industry as claimed in claim 2, wherein: the utility model discloses a device for preventing interference, including a gear, a mounting rack (4), a first abutting block (9), a second abutting block (11) and a second abutting block (9), wherein one side of the first abutting block (9) is in a wavy shape, four groups of gears (10) are uniformly arranged around the first gear (6), the top of the second gear (10) is connected with the bottom of the mounting rack (4) through bearings, and the bottom of the second gear (10) is fixedly connected with the second abutting block (11), and the end of the second abutting block (11) abuts against one wavy side of the first abutting block (9).
4. A device for recovering organic solvent from organic waste liquid of manufacturing industry as claimed in claim 3, wherein: the gear II (10) is meshed with the gear I (6), the gear I (6) rotates for one circle, and the gear II (10) rotates for four circles.
5. An apparatus for recovering organic solvent from organic waste liquid of manufacturing industry as defined in claim 1, wherein: push rods (15) are arranged on two sides below the first transmission disc (13), two groups of push rods (15) are parallel to each other, two groups of push rods (15) are hinged to the first transmission disc (13) and the second transmission disc (14) on the same side respectively at two ends, and the connection parts between the push rods (15) and the first transmission disc (13) and the second transmission disc (14) are located in the middle of two sides of the bottom ends of the first transmission disc (13) and the second transmission disc (14).
6. An apparatus for recovering organic solvent from organic waste liquid of manufacturing industry as defined in claim 1, wherein: the bottom of four groups of cleaning frames (17) all contact with the inner wall of the bottom end of the reaction kettle body (1), saw-tooth-shaped grooves are formed in the bottom end of the cleaning frames (17), the length and width dimensions of a single group of cleaning frames (17) are smaller than five centimeters of the radius of the inner wall of the bottom end of the reaction kettle body (1), namely, the four groups of cleaning frames (17) can cover most areas of the inner wall of the bottom end of the reaction kettle body (1).
7. An apparatus for recovering organic solvent from organic waste liquid of manufacturing industry as defined in claim 1, wherein: the surface of bull stick (16) is connected with the bearing mounting bracket through the bearing, and the bearing mounting bracket passes through the inner wall of bolt installation in reation kettle body (1) side.
8. An apparatus for recovering organic solvent from organic waste liquid of manufacturing industry as defined in claim 1, wherein: the inside fixedly connected with sleeve pipe (20) of output valve pipe (19), sleeve pipe (20) are hollow cylindric, output port (21) have been seted up to the inside one end of sleeve pipe (20) being located reation kettle body (1), screw hole (22) have been seted up to the outside one end of sleeve pipe (20) being located reation kettle body (1), screw rod (23) have been inserted to the inside of screw hole (22), be connected through the screw thread between screw rod (23) and screw hole (22), the end fixedly connected with control rod (24) of screw rod (23), control rod (24) pass output valve pipe (19) and extend to the outside of output valve pipe (19).
9. An apparatus for recovering organic solvent from organic waste liquid of manufacturing industry as defined in claim 8, wherein: the inside of sleeve pipe (20) is provided with shutoff board (25), the cross section of shutoff board (25) is circular, the diameter of shutoff board (25) is greater than delivery outlet (21), and the diameter of shutoff board (25) is less than the diameter of sleeve pipe (20) inner circle, shutoff board (25) are restricted by sleeve pipe (20) shape and can only be in the inside horizontal migration of sleeve pipe (20), the side parcel that shutoff board (25) is close to delivery outlet (21) has the seal cover, shutoff board (25) are with delivery outlet (21) shutoff.
10. An apparatus for recovering organic solvent from organic waste liquid of manufacturing industry as defined in claim 9, wherein: the screw rod (23) is located the inside one end fixedly connected with push pedal of sleeve pipe (20), the centre department of shutoff board (25) and push pedal is provided with spring (26), the one end and the shutoff board (25) fixed surface of spring (26) are connected, the other end and the fixed surface of push pedal of spring (26) are connected.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310509023.4A CN116216827A (en) | 2023-05-08 | 2023-05-08 | Device for recycling organic solvent from organic waste liquid in manufacturing industry |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310509023.4A CN116216827A (en) | 2023-05-08 | 2023-05-08 | Device for recycling organic solvent from organic waste liquid in manufacturing industry |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN116216827A true CN116216827A (en) | 2023-06-06 |
Family
ID=86579120
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202310509023.4A Pending CN116216827A (en) | 2023-05-08 | 2023-05-08 | Device for recycling organic solvent from organic waste liquid in manufacturing industry |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN116216827A (en) |
-
2023
- 2023-05-08 CN CN202310509023.4A patent/CN116216827A/en active Pending
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP1988981A2 (en) | Multiple application purification and recycling device | |
| KR102122051B1 (en) | A circle thin film vaporization equipment | |
| CN116216827A (en) | Device for recycling organic solvent from organic waste liquid in manufacturing industry | |
| CN215691756U (en) | Horizontal meta-acyl chloride rectifying tower | |
| EP1144064A1 (en) | Heat exchanger, in particular for preheating liquid manure | |
| CN109020065A (en) | A kind of wastewater treatment method | |
| CN112781394A (en) | Steam condensation recovery device | |
| CN208915934U (en) | A kind of higher boiling chemical reagent purification filling apparatus | |
| CN219050350U (en) | MVR triple effect evaporator | |
| CN108905246A (en) | A kind of New Evaporator | |
| CN204107066U (en) | Thin film evaporator | |
| CN209468146U (en) | Distilling apparatus for waste treatment apparatus | |
| CN115304119B (en) | Industrial salt production and preparation system | |
| CN219907093U (en) | Aluminum chloride solution evaporation crystallization mechanism for industrial wastewater treatment | |
| CN219815325U (en) | Rectifying equipment is used in phenethylamine production and processing | |
| CN216549999U (en) | Concentrated water treatment facilities of MVR evaporimeter | |
| CN217220235U (en) | Solvent oil rectifying tower | |
| CN219440721U (en) | Low-moisture tetrahydrofuran purifying equipment | |
| CN220695870U (en) | Distiller for preparing rose water | |
| CN215259715U (en) | Pure steam generator with heat recovery function | |
| CN214990739U (en) | Softened water treatment device for large boiler | |
| CN219637187U (en) | Plant purification distillation plant | |
| CN220376412U (en) | Desulfurization wastewater treatment device | |
| CN220609122U (en) | Thin film evaporator | |
| CN218076426U (en) | Low temperature evaporation crystallization stills agitating unit |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20230606 |
|
| RJ01 | Rejection of invention patent application after publication |