CN220176594U - Device for extracting, separating and purifying ursolic acid - Google Patents
Device for extracting, separating and purifying ursolic acid Download PDFInfo
- Publication number
- CN220176594U CN220176594U CN202320967154.2U CN202320967154U CN220176594U CN 220176594 U CN220176594 U CN 220176594U CN 202320967154 U CN202320967154 U CN 202320967154U CN 220176594 U CN220176594 U CN 220176594U
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- CN
- China
- Prior art keywords
- heating
- filter screen
- fixed
- chamber
- ursolic acid
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- WCGUUGGRBIKTOS-GPOJBZKASA-N (3beta)-3-hydroxyurs-12-en-28-oic acid Chemical compound C1C[C@H](O)C(C)(C)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C(O)=O)CC[C@@H](C)[C@H](C)[C@H]5C4=CC[C@@H]3[C@]21C WCGUUGGRBIKTOS-GPOJBZKASA-N 0.000 title claims abstract description 25
- 229940096998 ursolic acid Drugs 0.000 title claims abstract description 25
- PLSAJKYPRJGMHO-UHFFFAOYSA-N ursolic acid Natural products CC1CCC2(CCC3(C)C(C=CC4C5(C)CCC(O)C(C)(C)C5CCC34C)C2C1C)C(=O)O PLSAJKYPRJGMHO-UHFFFAOYSA-N 0.000 title claims abstract description 25
- 238000010438 heat treatment Methods 0.000 claims abstract description 51
- 238000005485 electric heating Methods 0.000 claims abstract description 15
- 239000012535 impurity Substances 0.000 claims abstract description 15
- 238000004140 cleaning Methods 0.000 claims abstract description 11
- 230000000087 stabilizing effect Effects 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims description 24
- 239000007788 liquid Substances 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 13
- 238000011049 filling Methods 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 230000010405 clearance mechanism Effects 0.000 claims description 3
- 238000000926 separation method Methods 0.000 abstract description 7
- 238000000746 purification Methods 0.000 abstract description 6
- 238000000605 extraction Methods 0.000 abstract description 5
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 238000000034 method Methods 0.000 description 11
- 239000011259 mixed solution Substances 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 5
- 238000001914 filtration Methods 0.000 description 5
- 238000009835 boiling Methods 0.000 description 3
- 238000003916 acid precipitation Methods 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 230000000069 prophylactic effect Effects 0.000 description 1
- -1 triterpene carboxylic acid compound Chemical class 0.000 description 1
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- Extraction Or Liquid Replacement (AREA)
Abstract
The utility model discloses an ursolic acid extraction and separation purification device, which comprises a stabilizing box, wherein a plurality of electric heating blocks are fixedly arranged in an inner cavity of a heating cavity, a filter screen cleaning mechanism is fixedly connected to the bottom of the inner cavity of a filter cavity, the filter screen cleaning mechanism comprises a U-shaped seat, one side of the U-shaped seat is fixedly connected with a fixed ring, the surfaces of two output ends of a double-shaft motor are respectively sleeved with a fixed sleeve, one side of each fixed sleeve is respectively fixedly connected with two ends of a rotating rod, and one side of each rotating rod is fixedly connected with an impurity filter screen.
Description
Technical Field
The utility model relates to the technical field of separation and purification devices, in particular to an extraction, separation and purification device for ursolic acid.
Background
Ursolic acid is an organic compound, is natural triterpene carboxylic acid compound, has prophylactic and anticancer activities, and can be used as emulsifying agent for medicines and foods.
The existing industrially effective purification method is an extraction method, and the method is simple and easy to implement but takes a long time, and the purity of the obtained ursolic acid is not high enough, so in order to more efficiently realize the extraction of the ursolic acid, experiments are often carried out by combining an ethyl acetate impurity removal method with an alkali dissolution acid precipitation method as a target method, and the ursolic acid is purified according to the states of the ursolic acid in solutions with different pH values, thereby realizing the efficient extraction activity of the ursolic acid.
The existing separation and purification device is mainly used for directly heating the treatment liquid through the electric heating plate in the using process, so that the treatment liquid is heated unevenly, and filtering measures are often arranged inside equipment in the extracting process, so that impurities on a filter screen are inconvenient to clean after multiple times of filtering.
Disclosure of Invention
The utility model aims to provide an extracting, separating and purifying device for ursolic acid, which aims to solve the problems that the prior separating and purifying device provided in the background art mainly heats treatment liquid directly through an electric heating plate in the using process, so that the treatment liquid is heated unevenly, filtering measures are often arranged in equipment in the extracting process, and impurities on a filter screen are inconvenient to clean after multiple times of filtering.
In order to achieve the above purpose, the present utility model provides the following technical solutions: the utility model provides an ursolic acid draw and separation purification device, includes the stable case, the fixed intercommunication in top of stable case has a heating cylinder, the fixed intercommunication in top of heating cylinder has a mixing cylinder, agitator motor is installed at the top of mixing cylinder, the heating chamber has been seted up to the inside of heating cylinder, the inner chamber fixed mounting in heating chamber has a plurality of electric heating blocks, the filter chamber has been seted up to the inside of stable case, the bottom fixedly connected with filter screen clearance mechanism of filter chamber inner chamber, filter screen clearance mechanism includes the U-shaped seat, one side fixedly connected with solid fixed ring of U-shaped seat, the top fixedly connected with biax motor of U-shaped seat, two output of biax motor respectively with the both sides swivelling joint of U-shaped seat inner chamber, the fixed cover has all been cup jointed on the surface of two output of biax motor, two one side of fixed cover respectively with the both ends fixed connection of dwang, one side fixedly connected with impurity filter screen of dwang, just impurity and solid fixed ring's inner chamber joint.
Preferably, a feeding pipe is fixedly communicated with one side of the top of the mixing drum, a top feeding pipe is fixedly communicated with one side of the mixing drum, the feeding pipe is used for feeding materials, and the top feeding pipe is used for feeding ethyl acetate and clear water.
Preferably, one side of the heating cylinder is fixedly communicated with a bottom feeding pipe, the inner cavity of the heating cavity is filled with heating liquid, and the bottom feeding pipe is used for adding alkaline water.
Preferably, a diversion cavity is formed in the bottom of the filter screen cleaning mechanism, a liquid outlet pipe is fixedly communicated with one side of the diversion cavity, a hinged door is hinged to one side of the filter cavity, and the separation cavity is used for enabling liquid to flow out of the liquid outlet pipe after treatment.
Preferably, the output end of the stirring motor penetrates into the inner cavity of the mixing drum to be fixedly connected with a rotating shaft, the surface of the rotating shaft is fixedly connected with a stirring rod, and the stirring rod is driven to rotate through rotation of the rotating shaft.
Preferably, the bottom of mixing drum and the bottom of heating drum all are fixed to be linked together and are had the solenoid valve, the front fixed mounting of stabilizing case has switch panel, agitator motor, electric heating piece, biax motor and solenoid valve are all through switch panel and external power supply electric connection, carry out on-off control.
Compared with the prior art, the utility model has the beneficial effects that:
1. heating the heating liquid in the inner cavity of the heating cavity through the operation of the electric heating block, heating the mixed solution by the heated heating liquid, and heating the mixed solution more uniformly by utilizing a water bath heating mode;
2. the liquid is filtered through the impurity filter screen, when the filterable device in impurity filter screen top accumulated certain volume, the rotation through fixed cover of rotation drive of biax motor and dwang, the rotation of dwang drives the rotation of impurity filter screen to empty impurity to the inner chamber of filter chamber, then follow the hinged door again and shift out, thereby make things convenient for the clearance of impurity filter screen.
Drawings
FIG. 1 is a schematic diagram of the structure of the present utility model;
FIG. 2 is a cross-sectional view of the present utility model;
FIG. 3 is a top view of the screen cleaning mechanism of the present utility model;
fig. 4 is an enlarged view of the portion a of the present utility model.
In the figure: 1. a stabilizing box; 2. a heating cylinder; 3. a mixing drum; 4. a stirring motor; 5. a heating chamber; 6. an electric heating block; 7. a filter chamber; 8. a filter screen cleaning mechanism; 9. a shunt cavity; 10. a U-shaped seat; 11. a fixing ring; 12. a biaxial motor; 13. a fixed sleeve; 14. a rotating lever; 15. impurity filtering net; 16. a feed pipe; 17. a top feed tube; 18. a bottom feeding pipe; 19. a hinged door; 20. a liquid outlet pipe; 21. a rotating shaft; 22. a stirring rod; 23. a solenoid valve.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Referring to fig. 1-4, the utility model provides an apparatus for extracting, separating and purifying ursolic acid, which comprises a stabilizing box 1, wherein the top of the stabilizing box 1 is fixedly communicated with a heating cylinder 2, the top of the heating cylinder 2 is fixedly communicated with a mixing cylinder 3, the top of the mixing cylinder 3 is provided with a stirring motor 4, a heating cavity 5 is arranged in the heating cylinder 2, a plurality of electric heating blocks 6 are fixedly arranged in the cavity of the heating cavity 5, a filter cavity 7 is arranged in the stabilizing box 1, the bottom of the cavity of the filter cavity 7 is fixedly connected with a filter screen cleaning mechanism 8, the filter screen cleaning mechanism 8 comprises a U-shaped seat 10, one side of the U-shaped seat 10 is fixedly connected with a fixed ring 11, the top of the U-shaped seat 10 is fixedly provided with a double-shaft motor 12, two output ends of the double-shaft motor 12 are respectively and rotatably connected with two sides of the cavity of the U-shaped seat 10, one side of the two fixed sleeves 13 is respectively and fixedly connected with two ends of a rotating rod 14, one side of the rotating rod 14 is fixedly connected with a filter screen 15, and the impurity 15 is clamped with the cavity of the fixed ring 11; through fully mixing the contact at the inner chamber of mixing drum 3 with raw materials and ethyl acetate, carry out the edulcoration operation, after the edulcoration, pour alkaline water through bottom filling tube 18 to open electric heating piece 6, the work of electric heating piece 6 heats the heating liquid of heating chamber 5 inner chamber, the heating liquid after the heating heats the mixed solution again, it is more even to make the mixed solution be heated through the mode of water bath heating, make ursolic acid raw materials and alkaline water carry out alkali dissolution acid precipitation method activity, after the heating boiling activity of a period of time, the inside ursolic acid of ursolic acid raw materials just can realize fully extracting.
Referring to fig. 1-4, further, a feeding pipe 16 is fixedly connected to one side of the top of the mixing drum 3, a top feeding pipe 17 is fixedly connected to one side of the mixing drum 3, the feeding pipe 16 is used for feeding raw materials, and the top feeding pipe 17 is used for feeding ethyl acetate and clean water.
Referring to fig. 1-4, further, a bottom feeding tube 18 is fixedly connected to one side of the heating cylinder 2, the inner cavity of the heating cavity 5 is filled with a heating liquid, the bottom feeding tube 18 is used for adding alkaline water, and the heating liquid is high boiling point oil.
Referring to fig. 1-4, further, a diversion cavity 9 is formed at the bottom of the filter screen cleaning mechanism 8, a liquid outlet pipe 20 is fixedly connected to one side of the diversion cavity 9, a hinged door 19 is hinged to one side of the filter cavity 7, and the diversion cavity 9 is used for discharging treated liquid from the liquid outlet pipe 20.
Referring to fig. 1-4, further, an output end of the stirring motor 4 penetrates into an inner cavity of the mixing drum 3 to be fixedly connected with a rotating shaft 21, a stirring rod 22 is fixedly connected to a surface of the rotating shaft 21, and rotation of the rotating shaft 21 drives rotation of the rotating shaft 21 through rotation of the stirring motor 4, so that rotation of the stirring rod 22 is driven.
Referring to fig. 1-4, further, the bottom end of the mixing drum 3 and the bottom end of the heating drum 2 are fixedly connected with an electromagnetic valve 23, the front surface of the stabilizing box 1 is fixedly provided with a switch panel, and the stirring motor 4, the electric heating block 6, the double-shaft motor 12 and the electromagnetic valve 23 are electrically connected with an external power supply through the switch panel.
During the concrete use, firstly, will get ethyl acetate and the inside of mixing drum 3 is poured into to the clear water through top filling tube 17, then pour into the inner chamber of mixing drum 3 with ursolic acid raw materials through inlet pipe 16, open agitator motor 4 this moment, agitator motor 4's rotation drives the rotation of pivot 21 and puddler 22, thereby make raw materials and ethyl acetate intensive mixing contact, carry out the edulcoration operation, after the edulcoration, leave the inner chamber of heating drum 2 with mixed solution through solenoid valve 23, pour into the alkaline water through bottom filling tube 18 this moment, and open electric heating block 6, the work of electric heating block 6 heats the heating medium of heating chamber 5 inner chamber, the heating medium after the heating heats mixed solution again, make mixed solution be heated more evenly through the mode of water bath heating, make ursolic acid raw materials and alkaline water carry out the heavy method activity of acid, after a period's heating boiling activity, the inside ursolic acid just can realize fully extracting, then let in the inner chamber of filter chamber 7 with liquid, filter the filter screen 15, filter the inner chamber that filters liquid through impurity 15, flow into the reposition of separation chamber 9, discharge from drain tube 20 through filter screen 15, and the filter screen 14 is rotated to the filter screen 14 when certain filter screen 15 is rotated to the filter screen, thereby rotate the filter screen 13 is rotated to the filter screen 14, rotate the filter screen 13 is rotated to the filter screen 13, the filter screen is rotated to the filter screen 13 when the rotation, the filter screen is rotated, and the filter screen is rotated, the rotary handle is rotated and the rotary handle is rotated 13 is rotated, and the filter screen is rotated, is rotated and the 13 is rotated, is convenient.
Although the present utility model has been described with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described, or equivalents may be substituted for elements thereof, and any modifications, equivalents, improvements and changes may be made without departing from the spirit and principles of the present utility model.
Claims (6)
1. The device for extracting, separating and purifying ursolic acid comprises a stabilizing box (1), and is characterized in that: the utility model provides a filter screen cleaning mechanism (8) is fixed to the top of stable case (1), the top fixed intercommunication of heating tube (2) has mixing drum (3), agitator motor (4) are installed at the top of mixing drum (3), heating chamber (5) have been seted up to the inside of heating drum (2), the inner chamber fixed mounting of heating chamber (5) has a plurality of electric heating blocks (6), filter chamber (7) have been seted up to the inside of stable case (1), the bottom fixedly connected with filter screen cleaning mechanism (8) of filter chamber (7) inner chamber, filter screen cleaning mechanism (8) include U-shaped seat (10), one side fixedly connected with solid fixed ring (11) of U-shaped seat (10), the top fixed mounting of U-shaped seat (10) has biax motor (12), two output ends of biax motor (12) are connected with the both sides rotation of U-shaped seat (10) inner chamber respectively, the fixed cover (13) have all been cup jointed on the surface of two one side of fixed cover (13) respectively with the inner chamber (14) of rotation, both ends fixed connection of filter screen (15) and solid fixed ring (15) have impurity (15).
2. The device for extracting, separating and purifying ursolic acid according to claim 1, wherein: one side of mixing drum (3) top is fixed to be linked together has inlet pipe (16), one side of mixing drum (3) is fixed to be linked together has top filling tube (17).
3. The device for extracting, separating and purifying ursolic acid according to claim 1, wherein: one side of the heating cylinder (2) is fixedly communicated with a bottom feeding pipe (18), and the inner cavity of the heating cavity (5) is filled with heating liquid.
4. The device for extracting, separating and purifying ursolic acid according to claim 1, wherein: the bottom of filter screen clearance mechanism (8) has seted up reposition of redundant personnel chamber (9), the fixed intercommunication in one side in reposition of redundant personnel chamber (9) has drain pipe (20), one side in filter chamber (7) articulates there is hinged door (19).
5. The device for extracting, separating and purifying ursolic acid according to claim 1, wherein: the output end of the stirring motor (4) penetrates into the inner cavity of the mixing drum (3) and is fixedly connected with a rotating shaft (21), and the surface of the rotating shaft (21) is fixedly connected with a stirring rod (22).
6. The device for extracting, separating and purifying ursolic acid according to claim 1, wherein: the bottom of mixing drum (3) and the bottom of heating cylinder (2) all are fixed to be linked together have solenoid valve (23), the front fixed mounting of stabilizing case (1) has switch panel, agitator motor (4), electric heating block (6), biax motor (12) and solenoid valve (23) all pass through switch panel and external power supply electric connection.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320967154.2U CN220176594U (en) | 2023-04-23 | 2023-04-23 | Device for extracting, separating and purifying ursolic acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320967154.2U CN220176594U (en) | 2023-04-23 | 2023-04-23 | Device for extracting, separating and purifying ursolic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220176594U true CN220176594U (en) | 2023-12-15 |
Family
ID=89105804
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202320967154.2U Active CN220176594U (en) | 2023-04-23 | 2023-04-23 | Device for extracting, separating and purifying ursolic acid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220176594U (en) |
-
2023
- 2023-04-23 CN CN202320967154.2U patent/CN220176594U/en active Active
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