CN220176107U - Genistein extraction and preparation device - Google Patents
Genistein extraction and preparation device Download PDFInfo
- Publication number
- CN220176107U CN220176107U CN202321246323.XU CN202321246323U CN220176107U CN 220176107 U CN220176107 U CN 220176107U CN 202321246323 U CN202321246323 U CN 202321246323U CN 220176107 U CN220176107 U CN 220176107U
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- Prior art keywords
- extraction
- tank
- reaction
- preparation device
- genistein
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- 238000000605 extraction Methods 0.000 title claims abstract description 87
- 229940045109 genistein Drugs 0.000 title claims abstract description 16
- TZBJGXHYKVUXJN-UHFFFAOYSA-N genistein Natural products C1=CC(O)=CC=C1C1=COC2=CC(O)=CC(O)=C2C1=O TZBJGXHYKVUXJN-UHFFFAOYSA-N 0.000 title claims abstract description 16
- 235000006539 genistein Nutrition 0.000 title claims abstract description 16
- ZCOLJUOHXJRHDI-CMWLGVBASA-N genistein 7-O-beta-D-glucoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC(O)=C2C(=O)C(C=3C=CC(O)=CC=3)=COC2=C1 ZCOLJUOHXJRHDI-CMWLGVBASA-N 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 239000007788 liquid Substances 0.000 claims abstract description 38
- 238000007789 sealing Methods 0.000 claims description 11
- 238000003780 insertion Methods 0.000 claims description 5
- 230000037431 insertion Effects 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 description 9
- 239000002994 raw material Substances 0.000 description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 238000002791 soaking Methods 0.000 description 5
- 239000002893 slag Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 238000001035 drying Methods 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- 238000012423 maintenance Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009924 canning Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
Abstract
The utility model discloses an extraction and preparation device of genistein, which comprises a reaction extraction tank and a liquid storage tank arranged opposite to the reaction extraction tank, wherein the bottom of the inner wall of the reaction extraction tank is rotationally connected with a cross throwing frame, four central shafts are fixedly arranged on the cross throwing frame, a filter cylinder component for intercepting extraction is sleeved on the central shafts, and a variable speed motor is fixedly arranged in the middle of the bottom end of the reaction extraction tank.
Description
Technical Field
The utility model relates to the technical field of genistein extraction, in particular to an extraction and preparation device of genistein.
Background
Genistein, mainly exists in leguminous plants and is widely used. The genistein is mainly extracted by adopting an ethanol soaking extraction mode, during extraction, crushed leguminous plant raw materials and ethanol are added into an extraction tank together, and finally, soaking, mixing and extraction are carried out. Such a common extraction and preparation device has the following disadvantages:
1. when the extracting solution is discharged after the extraction is finished, a large amount of extracting solution is contained in the raw material slag, the discharging of the extracting solution is insufficient, residues exist, and the waste is easy to occur;
2. the extraction mode of stirring and soaking has poor extraction effect and low efficiency;
3. after extraction, the difficulty of cleaning and maintaining the extraction tank is high, and time and labor are wasted.
Disclosure of Invention
The utility model aims to provide a genistein extraction and preparation device, which solves the problems of insufficient discharge of extracting solution, poor extraction effect, low efficiency and inconvenient cleaning of the existing extraction and preparation device in the prior art.
In order to achieve the above purpose, the present utility model provides the following technical solutions: the device comprises a reaction extraction tank and a liquid storage tank which is opposite to the reaction extraction tank, wherein the bottom of the inner wall of the reaction extraction tank is rotationally connected with a cross throwing frame, four central shafts are fixedly arranged on the cross throwing frame, a filter cartridge assembly for intercepting extraction is sleeved on the central shafts, a variable speed motor is fixedly arranged in the middle of the bottom end of the reaction extraction tank, the output end of the variable speed motor is fixedly connected with the bottom end of the cross throwing frame, one side of the bottom end of the reaction extraction tank is fixedly communicated with a liquid discharge pipe, the bottom end of the liquid discharge pipe is fixedly communicated with the top end of the liquid storage tank, an electromagnetic valve is fixedly arranged in the middle of the liquid discharge pipe, a lifting pump is fixedly arranged at the top end of the liquid storage tank, a lifting pipe is fixedly communicated with a water outlet of the lifting pump, and a sealing tank cover is hinged to the top end of the reaction extraction tank; the cross throwing frame is additionally arranged, residual extracting solution in the slag can be fully thrown out by virtue of centrifugal force after soaking and extraction, the full discharge of the extracting solution can be realized, the problem of waste of the extracting solution is reduced, the raw materials can be fully contacted and mixed with the extracting solution by adopting a mode of multiple intermittent extraction combining slow stirring extraction, liquid discharge, high-speed spin-drying and reflux extraction, the extraction effect is good, the efficiency is high, the filter cartridge component can be quickly pulled out and detached after the extraction is finished, and convenience is provided for cleaning and maintenance of the extracting tank.
Preferably, the filter cartridge assembly comprises a porous filter cartridge and a positioning insert cartridge arranged in the middle of the porous filter cartridge, wherein the top end of the central shaft penetrates through the positioning insert cartridge to be connected with a locknut in a threaded manner, and the disassembly and the assembly are rapid.
Preferably, one side at the top end of the porous filter cylinder is hinged with a cylinder sealing cover, a hanging buckle frame is fixedly arranged on the cylinder sealing cover, a hanging buckle assembly is fixedly arranged at the other side at the top end of the porous filter cylinder, and the hanging buckle assembly is opposite to the hanging buckle frame, so that the filter cylinder assembly can be quickly pulled out and disassembled after extraction is finished, and convenience is provided for cleaning and maintaining an extraction tank, and cleaning is time-saving and labor-saving.
Preferably, the water inlet of elevator pump extends to the inside of liquid reserve tank, the top of riser and the inside fixed intercommunication of reaction extraction jar can make raw and other materials fully contact with the extract and mix, and it is more abundant to draw, draws effectual, efficient.
Preferably, the four corners at the top end of the reaction extraction tank are fixedly provided with support foot frames, and the support is stable and reliable.
Preferably, the front of the liquid storage tank is fixedly provided with a timing switch, and the lifting pump, the electromagnetic valve and the variable speed motor are electrically connected with an external power supply through the timing switch, so that the operation is simple.
Preferably, the bottom of liquid reserve tank one side is fixed to be linked together has the extract calandria, install the valve on the extract calandria, it is convenient to discharge the extract.
Compared with the prior art, the utility model has the beneficial effects that:
1. the cross throwing frame is additionally arranged in the extraction and preparation device, so that residual extracting solution in the slag can be fully thrown out by virtue of centrifugal force after soaking and extraction, the full discharge of the extracting solution can be realized, and the problem of waste of the extracting solution is reduced;
2. the method adopts a mode of multiple intermittent extraction combining slow stirring extraction, liquid discharge, high-speed spin-drying and reflux extraction, so that the raw materials are fully contacted and mixed with the extracting solution, the extraction is more sufficient, the extraction effect is good, and the efficiency is high;
3. the filter cartridge assembly is integrally pulled and detached to isolate raw material slag, and can be rapidly pulled and detached after extraction is finished, so that convenience is brought to cleaning maintenance of the extraction tank, and cleaning is time-saving and labor-saving.
Drawings
FIG. 1 is a front cross-sectional view of an extraction and preparation apparatus of the present utility model:
FIG. 2 is a schematic structural view of the cross swing frame of the present utility model;
FIG. 3 is a front cross-sectional view of the filter cartridge assembly of the present utility model;
fig. 4 is an enlarged view of a portion a of the present utility model.
In the figure: 1. a reaction extraction tank; 2. a liquid storage tank; 3. a filter cartridge assembly; 31. a porous filter cartridge; 32. positioning the insertion barrel; 33. a cartridge cover; 34. a hanging buckle frame; 35. a hanging buckle component; 4. a central shaft; 5. a cross throwing frame; 6. a variable speed motor; 7. sealing the can lid; 8. a locknut; 9. a riser; 10. a lift pump; 11. a liquid discharge pipe; 12. an electromagnetic valve; 13. a timing switch; 14. an extracting solution discharge pipe; 15. and supporting the foot rest.
Detailed Description
The technical solutions in the embodiments of the present utility model will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model.
Referring to fig. 1-4, the utility model provides an extraction and preparation device for genistein, which comprises a reaction extraction tank 1 and a liquid storage tank 2 which is opposite to the reaction extraction tank 1, wherein the bottom of the inner wall of the reaction extraction tank 1 is rotationally connected with a cross throwing frame 5, four central shafts 4 are fixedly arranged on the cross throwing frame 5, a filter cylinder component 3 for intercepting extraction is sleeved on the central shafts 4, a variable speed motor 6 is fixedly arranged in the middle of the bottom end of the reaction extraction tank 1, the output end of the variable speed motor 6 is fixedly connected with the bottom end of the cross throwing frame 5, one side of the bottom end of the reaction extraction tank 1 is fixedly communicated with a liquid discharge pipe 11, the bottom end of the liquid discharge pipe 11 is fixedly communicated with the top end of the liquid storage tank 2, the middle part of the liquid discharge pipe 11 is fixedly provided with an electromagnetic valve 12, the top end of the liquid storage tank 2 is fixedly provided with a lifting pump 10, the water outlet of the lifting pump 10 is fixedly communicated with a lifting pipe 9, the top end of the reaction extraction tank 1 is hinged with a sealing tank cover 7, the water inlet of the lifting pump 10 extends to the inside the liquid storage tank 2, and the top end of the lifting pipe 9 is fixedly communicated with the inside the reaction extraction tank 1;
when the device is used, the device can be started, the variable speed motor 6 can rotate at a low speed, the filter cylinder assembly 3 is driven to rotate in the reaction extraction tank 1 for a period of time through the cross throwing frame 5, raw materials are fully contacted and mixed with extracting solution, then the electromagnetic valve 12 is opened, extracting solution can enter the liquid storage tank 2 through the liquid discharge pipe 11, the variable speed motor 6 rotates at a high speed, residual extracting solution in the porous filter cylinder 31 can be thrown out under the action of centrifugal force and enters the liquid storage tank 2, after a period of time, the electromagnetic valve 12 is closed, the variable speed motor 6 rotates at a low speed again, the extracting solution is added into the reaction extraction tank 1 through the lifting pump 10 again by the lifting pipe 9, and the mode of multiple intermittent extraction combined with slow stirring extraction, liquid discharge, high-speed spin-drying and reflux extraction is adopted, so that the raw materials are fully contacted and mixed with the extracting solution, the extracting effect is good, and the efficiency is high.
Referring to fig. 1, 2 and 4, further, the filter cartridge assembly 3 includes a porous filter cartridge 31 and a positioning insertion tube 32 disposed in the middle of the porous filter cartridge 31, the top end of the central shaft 4 is connected with a locknut 8 through the positioning insertion tube 32 in a threaded manner, one side of the top end of the porous filter cartridge 31 is hinged with a cartridge cover 33, a hanging buckle frame 34 is fixedly disposed on the cartridge cover 33, a hanging buckle assembly 35 is fixedly disposed on the other side of the top end of the porous filter cartridge 31, and the hanging buckle assembly 35 is opposite to the hanging buckle frame 34;
when the filter cartridge assembly is used, the sealing can cover 7 is lifted, the hanging buckle assembly 35 is buckled, the cartridge sealing cover 33 is lifted, the locknut 8 is unscrewed and removed, the filter cartridge assembly 3 can be integrally pulled out upwards, the extracted filter residues can be cleaned, the filter cartridge assembly 3 can be quickly pulled out and detached after the extraction is finished, and convenience is provided for cleaning and maintaining the extraction can, and cleaning is time-saving and labor-saving.
Referring to fig. 1, further, four corners of the top end of the reaction extraction tank 1 are fixedly provided with supporting foot frames 15, the front surface of the liquid storage tank 2 is fixedly provided with a timing switch 13, the lifting pump 10, the electromagnetic valve 12 and the variable speed motor 6 are electrically connected with an external power supply through the timing switch 13, the bottom of one side of the liquid storage tank 2 is fixedly communicated with an extracting liquid drain pipe 14, and the extracting liquid drain pipe 14 is provided with a valve;
when in use, the timing switch 13 controls the on-off of the lift pump 10, the electromagnetic valve 12 and the variable speed motor 6 at regular time, so that the work is smooth and stable, and the safety and the reliability are realized.
When the embodiment of the utility model is used, the following steps are adopted: the sealed tank cover 7 is lifted, the hanging buckle assembly 35 is sequentially buckled, the barrel sealing cover 33 is lifted, crushed raw materials are added into the porous filter barrel 31, the barrel sealing cover 33 is closed, the hanging buckle assembly 35 is hung on the hanging buckle frame 34, a proper amount of ethanol solution is added into the reaction extraction tank 1 as an extracting agent, after the sealed tank cover 7 is closed, the equipment can be started, the variable speed motor 6 can firstly rotate at a low speed, the filter barrel assembly 3 is driven by the cross throwing frame 5 to rotate in the reaction extraction tank 1 for a period of time, raw materials are fully contacted and mixed with extracting solution, the electromagnetic valve 12 is opened, at the moment, extracting solution enters the liquid storage tank 2 through the liquid discharge pipe 11, then the variable speed motor 6 rotates at a high speed, under the action of centrifugal force, extracting solution remained in the porous filter barrel 31 can be thrown out into the liquid storage tank 2, after a period of time, the electromagnetic valve 12 is closed, the variable speed motor 6 rotates at a low speed again, the lifting pump 10 is used for adding the extracting solution into the reaction extraction tank 1 again through the lifting pipe 9, the equipment is closed after repeated extraction, and extracting solution is discharged for a plurality of times.
Although the present utility model has been described with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described, or equivalents may be substituted for elements thereof, and any modifications, equivalents, improvements and changes may be made without departing from the spirit and principles of the present utility model.
Claims (7)
1. The device for extracting and preparing genistein comprises a reaction extraction tank (1) and a liquid storage tank (2) which is opposite to the reaction extraction tank (1), and is characterized in that: the bottom of the inner wall of the reaction extraction tank (1) is rotationally connected with a cross throwing frame (5), four central shafts (4) are fixedly arranged on the cross throwing frame (5), a filter cylinder component (3) for intercepting extraction is sleeved on the central shafts (4), a variable speed motor (6) is fixedly arranged in the middle of the bottom end of the reaction extraction tank (1), the output end of the variable speed motor (6) is fixedly connected with the bottom end of the cross throwing frame (5), one side of reaction extraction jar (1) bottom is fixed to be linked together and is had fluid-discharge tube (11), the bottom of fluid-discharge tube (11) is fixed to be linked together with the top of liquid reserve tank (2), the middle part fixed mounting of fluid-discharge tube (11) has solenoid valve (12), the top fixed mounting of liquid reserve tank (2) has elevator pump (10), the delivery port fixed intercommunication of elevator pump (10) has riser (9), the top of reaction extraction jar (1) articulates there is sealed tank cap (7).
2. The extraction and preparation device of genistein according to claim 1, characterized in that: the filter cartridge assembly (3) comprises a porous filter cartridge (31) and a positioning insertion cartridge (32) arranged in the middle of the porous filter cartridge (31), and the top end of the central shaft (4) penetrates through the positioning insertion cartridge (32) to be connected with a locknut (8) in a threaded mode.
3. The extraction and preparation device of genistein according to claim 2, characterized in that: one side at the top end of the porous filter cylinder (31) is hinged with a cylinder sealing cover (33), a hanging buckle frame (34) is fixedly arranged on the cylinder sealing cover (33), a hanging buckle assembly (35) is fixedly arranged at the other side at the top end of the porous filter cylinder (31), and the hanging buckle assembly (35) is opposite to the hanging buckle frame (34).
4. The extraction and preparation device of genistein according to claim 1, characterized in that: the water inlet of the lifting pump (10) extends to the inside of the liquid storage tank (2), and the top end of the lifting pipe (9) is fixedly communicated with the inside of the reaction extraction tank (1).
5. The extraction and preparation device of genistein according to claim 1, characterized in that: four corners at the top end of the reaction extraction tank (1) are fixedly provided with supporting foot frames (15).
6. The extraction and preparation device of genistein according to claim 1, characterized in that: the front of the liquid storage tank (2) is fixedly provided with a timing switch (13), and the lifting pump (10), the electromagnetic valve (12) and the variable speed motor (6) are electrically connected with an external power supply through the timing switch (13).
7. The extraction and preparation device of genistein according to claim 1, characterized in that: the bottom of one side of the liquid storage tank (2) is fixedly communicated with an extracting solution discharge pipe (14), and a valve is arranged on the extracting solution discharge pipe (14).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321246323.XU CN220176107U (en) | 2023-05-17 | 2023-05-17 | Genistein extraction and preparation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321246323.XU CN220176107U (en) | 2023-05-17 | 2023-05-17 | Genistein extraction and preparation device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220176107U true CN220176107U (en) | 2023-12-15 |
Family
ID=89101606
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321246323.XU Active CN220176107U (en) | 2023-05-17 | 2023-05-17 | Genistein extraction and preparation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220176107U (en) |
-
2023
- 2023-05-17 CN CN202321246323.XU patent/CN220176107U/en active Active
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