CN219816258U - Efficient extraction equipment for preparing desacetyl erigeron breviscapus - Google Patents

Efficient extraction equipment for preparing desacetyl erigeron breviscapus Download PDF

Info

Publication number
CN219816258U
CN219816258U CN202321250704.5U CN202321250704U CN219816258U CN 219816258 U CN219816258 U CN 219816258U CN 202321250704 U CN202321250704 U CN 202321250704U CN 219816258 U CN219816258 U CN 219816258U
Authority
CN
China
Prior art keywords
water supply
pipe
tank body
assembly
desacetyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202321250704.5U
Other languages
Chinese (zh)
Inventor
王珊珊
钱执熙
邵曼玉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Lianxing Pharmaceutical Technology Co ltd
Original Assignee
Shanghai Lianxing Pharmaceutical Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Lianxing Pharmaceutical Technology Co ltd filed Critical Shanghai Lianxing Pharmaceutical Technology Co ltd
Priority to CN202321250704.5U priority Critical patent/CN219816258U/en
Application granted granted Critical
Publication of CN219816258U publication Critical patent/CN219816258U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Extraction Or Liquid Replacement (AREA)

Abstract

The utility model discloses high-efficiency extraction equipment for preparing desquamation maohoridine, which comprises a tank body, a water supply assembly, a stirring assembly and a collecting assembly, wherein a feed inlet is formed in the upper portion of the tank body, a discharge pipe is arranged at the lower portion of the tank body, the discharge pipe is connected with a discharge valve, a heating assembly is connected to the outside of the tank body, the stirring assembly comprises a power source and a rotating rod, the power source is used for driving the rotating rod to rotate, the rotating rod is rotationally connected to the tank body, the rotating rod is connected with a plurality of stirring rods, the water supply assembly comprises a water tank and a water supply pipe, and the water tank is communicated with the water supply pipe. According to the utility model, the water supply assembly is arranged, so that the dropping speed can be controlled, the reaction rate is controlled, and the partial reaction is prevented from being too large by matching with stirring, so that the whole reaction is more uniform, and the collection assembly is arranged at the lower side of the tank body to collect the extracted desacetyl erigeron glycoside.

Description

Efficient extraction equipment for preparing desacetyl erigeron breviscapus
Technical Field
The utility model belongs to the field of extraction equipment, and particularly relates to efficient extraction equipment for preparing desacetyl erigeron breviscapus.
Background
Deacetyl glucoside (molecular formula C) 47 H 74 O 19 ) Is a medicament for treating acute and chronic contractile cardiac insufficiency, atrial fibrillation and paroxysmal supraventricular tachycardia, and is prepared by taking a pilin c as a precursor and deacetylating the pilin c in an alcohol solution; however, the existing deacetylated hairy vein glycoside has certain defects in the production process and needs to be improved.
When the existing extraction equipment is used, the problems of uneven reaction, slow reaction rate and incomplete product collection often occur.
Disclosure of Invention
The utility model aims to provide efficient extraction equipment for preparing desacetyl erigeron breviscapus, which solves the problem of low extraction efficiency of the existing equipment.
In order to solve the problems in the prior art, the utility model adopts the following technical scheme:
a high-efficiency extraction device for preparing desacetyl erigeron breviscapus comprises a tank body, a water supply assembly, a stirring assembly and a collecting assembly.
The upper portion of the tank body is provided with a feed inlet, the lower part of the tank body is provided with a discharge pipe, the discharge pipe is connected with a discharge valve, and the outside of the tank body is connected with a heating component.
The stirring assembly comprises a power source and a rotating rod, wherein the power source is used for driving the rotating rod to rotate, the rotating rod is rotationally connected to the tank body, and the rotating rod is connected with a plurality of stirring rods.
The water supply assembly comprises a water tank and a water supply pipe, wherein the water tank is communicated with the water supply pipe, and the water supply pipe stretches into the tank body.
The collecting assembly is arranged below the discharging pipe and comprises a collecting groove, and the collecting groove is connected with a filter screen.
Through setting up water supply assembly, can control the dropping speed, control reaction rate to the cooperation stirring can avoid the local reaction too big, makes the whole reaction more even, and sets up at jar body downside and collect the subassembly, collects the deacetyl maohoriside that draws.
Further, jar body coupling has the support frame, through setting up the support frame, rises jar body, is convenient for place the collection subassembly in jar body downside, heating element is including winding in the heating pipe in jar body outside, the heating pipe can adopt electric heating, also can adopt water bath heating, if adopt water bath heating, needs connect inlet tube and outlet pipe at the both ends of heating pipe, through setting up the heating pipe, can heat jar body, through control temperature improvement reaction rate.
Further, the power supply includes the motor, the casing of motor is connected in jar body top, and the motor passes through drive assembly and dwang connection, drive assembly includes drive belt and two belt pulleys, and two belt pulleys are connected respectively in the axle head of dwang and motor, the belt is connected in two belt pulleys, utilizes the motor to drive stirring subassembly and rotates, stirs the reactant in the jar for the reaction is more even, the puddler is equipped with three groups, and three groups puddler distributes along the axis direction of dwang, and the puddler of a set of below is connected with the brush, the brush is connected in the downside of puddler, and three groups the puddler equidistant setting, and a set of below that said here refers to a set of from the belt pulley the farthest, namely be located a set of bottom during the in-service use, because can produce solid precipitation after the reaction, is convenient for collect fixed precipitation through setting up the brush.
Further, the novel reaction tank is characterized by further comprising a spraying assembly arranged in the tank body, the spraying assembly comprises a water distribution pipe, the water distribution pipe is connected to the top of the tank body through a plurality of fixing frames, the water distribution pipe is connected with a plurality of spray heads, the spraying assembly is arranged, after the reaction is finished, the inner wall of the tank body and the stirring assembly are flushed through spraying of the spraying assembly, products after the reaction can be collected as much as possible, and the products after the reaction are prevented from being left in the tank body.
Further, the delivery pipe includes water supply header pipe, first delivery pipe and second delivery pipe, water supply header pipe and water tank intercommunication, water supply header pipe passes through first delivery pipe and water distribution pipe intercommunication, and water supply header pipe stretches into the jar internal portion through the second delivery pipe, first delivery pipe is connected with first valve, the second delivery pipe is connected with the second valve, through setting up first delivery pipe and second delivery pipe to set up the valve on first delivery pipe and second delivery pipe, in the reaction, open the second valve, the gradual dropwise add of carbonate aqueous solution in the water tank contains the alcohol solution of maohexaside, make the two react, after the reaction, collect the deposit of production, close the second valve at this moment, open first valve, carbonate aqueous solution passes through spray assembly blowout, washes jar body inner wall and stirring subassembly, the top of water tank is equipped with the water inlet for replenishing carbonate aqueous solution in the water tank, the filter screen slope sets up, because the discharging pipe does not set up in the central point of jar body bottom, consequently sets up the filter screen slope, the one end that is close to the discharging pipe is higher, the one end that keeps away from the discharging pipe is lower, rely on gravity one end can be lower to the slip to the required collecting tank, the water pump is just accomplished to the collecting tank.
The beneficial effects of the utility model are as follows:
1. the utility model improves the reaction rate as much as possible and improves the extraction efficiency on the premise of ensuring the reaction quality through various means comprehensive control.
2. The utility model can provide proper reaction temperature and ensure uniform reaction by stirring and heating.
3. The collecting component is arranged at the lower part of the tank body, so that the product can be directly collected, and the solution can be intensively treated.
Drawings
FIG. 1 is a schematic diagram of the structure of the present utility model;
FIG. 2 is a front view of the present utility model;
FIG. 3 is a cross-sectional view taken along the direction A-A in FIG. 2;
FIG. 4 is a schematic view of the stirring assembly of FIG. 3;
FIG. 5 is a schematic view of the spray assembly of example 4;
fig. 6 is a schematic view showing the structure of a water supply assembly in embodiment 5.
In the figure: 1-a tank body; 11-a discharge pipe; 12-a heating assembly; 13-a discharge valve; 2-a water supply assembly; 21-a water tank; 22-a water supply main pipe; 23-a first water supply pipe; 24-a second water supply pipe; 25-a first valve; 26-a second valve; 3-a collection assembly; 31-a collection tank; 32-a filter screen; 4-an electric motor; 5-a spray assembly; 51-a water distribution pipe; 52-a spray head; 53-fixing frame; 6-supporting frames; 7-a stirring assembly; 71-a rotating rod; 72-stirring rod; 73-hairbrush; 74-pulleys.
Detailed Description
The utility model is further described with reference to the drawings and reference numerals.
In order that the above-recited objects, features and advantages of the present utility model will be more clearly understood, a more particular description of the utility model will be rendered by reference to specific embodiments thereof which are illustrated in the appended drawings. It should be noted that, without conflict, the embodiments of the present utility model and features in the embodiments may be combined with each other.
The terms "first," "second," "third," and the like are used merely to distinguish between descriptions and are not to be construed as indicating or implying relative importance.
In the description of the present utility model, it should also be noted that, unless explicitly specified and limited otherwise, the terms "disposed," "mounted," "connected," and "connected" are to be construed broadly, and may be, for example, fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; can be directly connected or indirectly connected through an intermediate medium, and can be communication between two elements. The specific meaning of the above terms in the present utility model will be understood in specific cases by those of ordinary skill in the art.
The following describes specific embodiments of the present utility model in detail with reference to the drawings. It should be understood that the detailed description and specific examples, while indicating and illustrating the utility model, are not intended to limit the utility model.
Example 1:
as shown in fig. 1 to 4, a high-efficiency extraction apparatus for preparing desacetyl erigeron glycoside comprises a tank 1, a water supply assembly 2, a stirring assembly 7 and a collection assembly 3.
The upper portion of the tank body 1 is provided with a feed inlet (not marked in the figure), the lower portion of the tank body 1 is provided with a discharge pipe 11, the discharge pipe 11 is connected with a discharge valve 13, and the outside of the tank body 1 is connected with a heating component 12.
The stirring assembly 7 comprises a power source and a rotating rod 71, wherein the power source is used for driving the rotating rod 71 to rotate, the rotating rod 71 is rotationally connected to the tank body 1, and the rotating rod 71 is connected with a plurality of stirring rods 72.
The water supply assembly 2 comprises a water tank 21 and a water supply pipe (the water supply pipe is a generic name of a water supply main 22, a first water supply pipe 23 and a second water supply pipe 24), wherein the water tank 21 is communicated with the water supply pipe, and the water supply pipe extends into the tank body 1.
The collecting assembly 3 is arranged below the discharging pipe 11, the collecting assembly 3 comprises a collecting groove 31, and the collecting groove 31 is connected with a filter screen 32.
Through setting up water supply assembly 2, can control the dropping speed, control reaction rate to the cooperation stirring can avoid the local reaction too big, makes the whole reaction more even, and sets up collection subassembly 3 at jar body 1 downside, collects the deacetyl hairy glycoside that draws.
Example 2:
on the basis of the embodiment 1, the tank body 1 is connected with a supporting frame 6.
Through setting up support frame 6, raise jar body 1, be convenient for place collection subassembly 3 at jar body 1 downside.
The heating assembly 12 comprises a heating pipe wound on the outer side of the tank body 1.
The heating pipe can adopt electric heating or water bath heating, and if water bath heating is adopted, the water inlet pipe and the water outlet pipe are required to be connected at the two ends of the heating pipe.
By providing a heating pipe, the tank 1 can be heated, and the reaction rate can be increased by controlling the temperature.
When the temperature control device is used, the temperature of the heating pipe is adjusted according to the temperature requirement, so that the temperature inside the tank body 1 can tend to be stable, the reaction inside the tank body 1 is facilitated, a temperature sensor can be arranged inside the tank body 1, the temperature inside the tank body is monitored through the temperature sensor, and the temperature control is more accurate.
Example 3:
on the basis of embodiment 2, the power source comprises a motor 4, a shell of the motor 4 is connected to the top of the tank body 1, and the motor 4 is connected with a rotating rod 71 through a transmission assembly.
The transmission assembly comprises a transmission belt and two pulleys 74, the two pulleys 74 being connected to the shaft ends of the rotating rod 71 and the motor 4, respectively, the belt being connected to the two pulleys 74.
The stirring assembly 7 is driven to rotate by the motor 4 to stir reactants in the tank body 1, so that the reaction is more uniform.
The stirring rods 72 are provided with three groups, the three groups of stirring rods 72 are distributed along the axial direction of the rotating rod 71, the stirring rod 72 of the lowest group is connected with a brush 73, and the brush 73 is connected to the lower side of the stirring rod 72.
The three sets of stirring bars 72 are equally spaced, and the lowermost set as referred to herein is the set furthest from the pulley 74, i.e. the set which is at the bottom in actual use.
Since solid precipitate is generated after the reaction, the fixed precipitate is conveniently collected by providing the brush 73.
Example 4:
on the basis of embodiment 3, as shown in fig. 5, the spray assembly 5 is further included in the tank 1, the spray assembly 5 includes a water distribution pipe 51, the water distribution pipe 51 is connected to the top of the tank 1 through a plurality of fixing frames 53, and the water distribution pipe 51 is connected with a plurality of spray heads 52.
Through setting up spray assembly 5, spray through spray assembly 5 after the reaction is accomplished and wash jar body 1 inner wall and stirring subassembly 7, can be with the product after the reaction as far as possible's collection, avoid the product after the reaction to leave in jar body 1 inside.
Example 5:
on the basis of embodiment 4, as shown in fig. 6, the water supply pipe comprises a water supply main 22, a first water supply pipe 23 and a second water supply pipe 24, wherein the water supply main 22 is communicated with the water tank 21, the water supply main 22 is communicated with the water distribution pipe 51 through the first water supply pipe 23, the water supply main 22 extends into the tank body 1 through the second water supply pipe 24, the first water supply pipe 23 is connected with a first valve 25, and the second water supply pipe 24 is connected with a second valve 26.
Through setting up first delivery pipe 23 and second delivery pipe 24 to set up the valve on first delivery pipe 23 and second delivery pipe 24, when reacting, open second valve 26, the carbonate aqueous solution in the water tank 21 gradually drips into the alcohol solution that contains the maohuaside, makes the two react, after the reaction finishes, collects the deposit that produces, closes second valve 26 this moment, opens first valve 25, and the carbonate aqueous solution is through spraying subassembly 5 blowout, washes jar body 1 inner wall and stirring subassembly 7.
The top of the water tank 21 is provided with a water inlet for supplementing the water tank 21 with the carbonate aqueous solution.
The filter screen 32 is disposed obliquely.
Because discharging pipe 11 does not set up the central point in the bottom of jar body 1, consequently set up filter screen 32 slope, the one end that is close to discharging pipe 11 is higher, and the one end that keeps away from discharging pipe 11 is lower, and the sediment relies on gravity to slide to the lower one end of filter screen 32, just needs a collecting vat 31 just can accomplish the collection of solid sediment.
A water pump (not shown) is connected to the bottom of the collecting tank 31.
Because the capacity of the collecting tank 31 is limited, by providing a water pump at the bottom of the collecting tank 31, the filtered alcohol solution can be transported to another container by the water pump, and the filtered liquid can be collected and recovered.
The specific working principle is as follows:
when the novel kettle is used, alcohol solution dissolved with the pilin is firstly introduced into the kettle body 1, carbonate water solution is simultaneously introduced into the water tank 21, then the heating component 12 and the stirring component 7 are started to heat and stir the alcohol solution in the kettle body 1, when the temperature reaches a temperature range suitable for reaction, the second valve 26 is opened to control the dropping speed of the carbonate water solution, meanwhile, the carbonate water solution reacts with the alcohol solution to generate sediment (deacetyl pilin), when sediment is not generated, the second valve 26 is closed, the discharge valve 13 is opened to collect, the stirring component 7 continues to rotate in the collecting process, the first valve 25 is opened, the carbonate water solution is sprayed out through the spraying component 5 to clean the inner wall of the kettle body 1 and the stirring component 7, the cleaned liquid is discharged from the discharge pipe 11 together, the sediment is filtered out by the filter screen 32 after the sediment falls into the filter screen 32, and the sediment is dried after the sediment is collected, so that the deacetyl pilin can be obtained.
The utility model is not limited to the above-described alternative embodiments, and any person who may derive other various forms of products in the light of the present utility model, however, any changes in shape or structure thereof, all falling within the technical solutions defined in the scope of the claims of the present utility model, fall within the scope of protection of the present utility model.

Claims (9)

1. An efficient extraction device for preparing desacetyl erigeron breviscapus, which is characterized in that: comprises a tank body (1), a water supply assembly (2), a stirring assembly (7) and a collecting assembly (3);
the upper part of the tank body (1) is provided with a feed inlet, the lower part of the tank body (1) is provided with a discharge pipe (11), the discharge pipe (11) is connected with a discharge valve (13), and the outside of the tank body (1) is connected with a heating component (12);
the stirring assembly (7) comprises a power source and a rotating rod (71), wherein the power source is used for driving the rotating rod (71) to rotate, the rotating rod (71) is rotationally connected to the tank body (1), and the rotating rod (71) is connected with a plurality of stirring rods (72);
the water supply assembly (2) comprises a water tank (21) and a water supply pipe, wherein the water tank (21) is communicated with the water supply pipe, and the water supply pipe stretches into the tank body (1);
the collecting assembly (3) is arranged below the discharging pipe (11), the collecting assembly (3) comprises a collecting groove (31), and the collecting groove (31) is connected with a filter screen (32).
2. The efficient extraction apparatus for preparing desacetyl erigeron glycoside according to claim 1, characterized in that: the heating component (12) comprises a heating pipe wound on the outer side of the tank body (1).
3. The efficient extraction apparatus for preparing desacetyl erigeron glycoside according to claim 1, characterized in that: the power source comprises a motor (4), a shell of the motor (4) is connected to the top of the tank body (1), and the motor (4) is connected with a rotating rod (71) through a transmission assembly.
4. A high-efficiency extraction apparatus for preparing desacetyl erigeron glycoside according to claim 3, characterized in that: the transmission assembly comprises a transmission belt and two belt pulleys (74), wherein the two belt pulleys (74) are respectively connected to the shaft ends of the rotating rod (71) and the motor (4), and the belt is connected to the two belt pulleys (74).
5. The efficient extraction apparatus for preparing desacetyl erigeron glycoside according to claim 1, characterized in that: the stirring rods (72) are provided with three groups, the three groups of stirring rods (72) are distributed along the axis direction of the rotating rods (71), the stirring rods (72) of the lowermost group are connected with brushes (73), and the brushes (73) are connected to the lower sides of the stirring rods (72).
6. The efficient extraction apparatus for preparing desacetyl erigeron glycoside according to claim 1, characterized in that: the novel water distribution device is characterized by further comprising a spraying assembly (5) arranged in the tank body (1), wherein the spraying assembly (5) comprises a water distribution pipe (51), the water distribution pipe (51) is connected to the top of the tank body (1) through a plurality of fixing frames (53), and the water distribution pipe (51) is connected with a plurality of spray heads (52).
7. The efficient extraction apparatus for preparing desacetyl erigeron glycoside according to claim 6, characterized in that: the water supply pipe comprises a water supply main pipe (22), a first water supply pipe (23) and a second water supply pipe (24), wherein the water supply main pipe (22) is communicated with the water tank (21), the water supply main pipe (22) is communicated with the water distribution pipe (51) through the first water supply pipe (23), the water supply main pipe (22) stretches into the tank body (1) through the second water supply pipe (24), the first water supply pipe (23) is connected with a first valve (25), and the second water supply pipe (24) is connected with a second valve (26).
8. The efficient extraction apparatus for preparing desacetyl erigeron glycoside according to claim 1, characterized in that: the filter screen (32) is obliquely arranged.
9. The efficient extraction apparatus for preparing desacetyl erigeron glycoside according to claim 1, characterized in that: the tank body (1) is connected with a supporting frame (6).
CN202321250704.5U 2023-05-22 2023-05-22 Efficient extraction equipment for preparing desacetyl erigeron breviscapus Active CN219816258U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202321250704.5U CN219816258U (en) 2023-05-22 2023-05-22 Efficient extraction equipment for preparing desacetyl erigeron breviscapus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202321250704.5U CN219816258U (en) 2023-05-22 2023-05-22 Efficient extraction equipment for preparing desacetyl erigeron breviscapus

Publications (1)

Publication Number Publication Date
CN219816258U true CN219816258U (en) 2023-10-13

Family

ID=88251181

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202321250704.5U Active CN219816258U (en) 2023-05-22 2023-05-22 Efficient extraction equipment for preparing desacetyl erigeron breviscapus

Country Status (1)

Country Link
CN (1) CN219816258U (en)

Similar Documents

Publication Publication Date Title
CN110548714A (en) automatic change chinese-medicinal material belt cleaning device
CN219816258U (en) Efficient extraction equipment for preparing desacetyl erigeron breviscapus
CN216224361U (en) Reaction device for preparing methyl propionylacetate
CN209825067U (en) Steaming device suitable for tea processing
CN112869143B (en) Novel production facility of walnut phytolipid
CN214665767U (en) Special desiccator of astaxanthin production with filtering capability
CN215137394U (en) Silicon dioxide filtering and separating device for producing anhydrous hydrogen fluoride
CN215428937U (en) Synthesis equipment of 2,3, 4-trimethoxybenzaldehyde
CN113355829B (en) Dip dyeing device for core spun yarn production
CN211322967U (en) Multi-functional majia shaddock belt cleaning device
CN115502019A (en) Anti-radiation fabric coating device for down jackets
CN213348841U (en) Based on nitre production is with luo and reation kettle
CN209890780U (en) Titanium dioxide nanofiber preparation facilities
CN210331692U (en) Spray drier is used in production of multi-functional industrial protein powder
CN113430349A (en) Heat treatment production line for notebook computer shell
CN112449789A (en) Cotton seed delinting device
CN218115843U (en) Crepe fabric sizing equipment
CN220859367U (en) Betel nut cleaning equipment
CN219047258U (en) Novel food processing washs device
CN219730595U (en) Vacuum distillation kettle in heat treatment cleaning waste liquid recycling system
CN111034412A (en) Corn seed is with capsule device
CN217828887U (en) Blueberry juice low temperature concentration device
CN219463255U (en) Concentrated jar of liquid medicine
CN221141296U (en) Wastewater recycling treatment device
CN218147312U (en) Dyeing device for environment-friendly regenerated polyester bulked yarns

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant