CN219701893U - Neutralization device after pickling of low-chloro phthalocyanine blue - Google Patents
Neutralization device after pickling of low-chloro phthalocyanine blue Download PDFInfo
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- CN219701893U CN219701893U CN202320566286.4U CN202320566286U CN219701893U CN 219701893 U CN219701893 U CN 219701893U CN 202320566286 U CN202320566286 U CN 202320566286U CN 219701893 U CN219701893 U CN 219701893U
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- neutralization
- top surface
- groove
- pickling
- fixedly arranged
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- 238000006386 neutralization reaction Methods 0.000 title claims abstract description 55
- 238000005554 pickling Methods 0.000 title claims abstract description 18
- 239000002253 acid Substances 0.000 claims abstract description 30
- 239000012065 filter cake Substances 0.000 claims abstract description 23
- 239000007788 liquid Substances 0.000 claims abstract description 23
- 238000006243 chemical reaction Methods 0.000 claims abstract description 22
- 238000003756 stirring Methods 0.000 claims abstract description 15
- 238000005406 washing Methods 0.000 claims description 7
- 230000003472 neutralizing effect Effects 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 2
- IEQIEDJGQAUEQZ-UHFFFAOYSA-N phthalocyanine Chemical class N1C(N=C2C3=CC=CC=C3C(N=C3C4=CC=CC=C4C(=N4)N3)=N2)=C(C=CC=C2)C2=C1N=C1C2=CC=CC=C2C4=N1 IEQIEDJGQAUEQZ-UHFFFAOYSA-N 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 13
- 239000012466 permeate Substances 0.000 abstract 1
- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 description 6
- 238000002360 preparation method Methods 0.000 description 4
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000004063 acid-resistant material Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
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Abstract
The utility model discloses neutralization equipment after pickling of low-chloro phthalocyanine blue, which has the technical scheme that: the device comprises a base, wherein a neutralization barrel is arranged on the top surface of the base, a supporting rod is fixedly arranged on the top surface of the base, a connecting rod is fixedly arranged on the top surface of the supporting rod, and a turntable is arranged on the bottom surface of the connecting rod; the stirring assembly is arranged on the bottom surface of the rotary table and is used for carrying out neutralization stirring treatment on acid filter cakes after pickling, the stirring assembly is arranged, the acid filter cakes after pickling can be placed on the reaction basket, the filter screen can prevent the acid filter cakes from leaking into process water, so that the acid filter cakes are prevented from being scattered and taken out well, the acid filter cakes after pickling are placed in the reaction basket, the process water is enabled to permeate the reaction basket and contact with the acid filter cakes, the neutralization reaction rate is accelerated, specific treatment is carried out under a specific pH value, and the liquid level sensor can detect the liquid level depth in the neutralization barrel through the liquid level sensor, so that the neutralization liquid content in the neutralization barrel is controlled.
Description
Technical Field
The utility model relates to the technical field of neutralization equipment, in particular to low-chloro phthalocyanine blue acid-washing post-neutralization equipment.
Background
Phthalocyanine blue is an organic matter, a bright green blue rod-like crystal, is flammable, is insoluble in water, alcohol and hydrocarbon, is dissolved in concentrated sulfuric acid to form an olive-colored solution, and is diluted to separate out a blue suspension.
According to publication No.: chinese patent CN203577804U, neutralization apparatus, an improved apparatus for neutralization of acidic liquids by means of alkaline liquids, whereby both liquid streams are introduced together, whereby the neutralization vessel need not be constructed of acid resistant materials, and wherein the apparatus can be controlled by monitoring the pH of the resulting combined liquid stream exiting the neutralization vessel.
However, the neutralization apparatus described above still has some drawbacks, such as: an improved device for neutralization of an acidic liquid by means of an alkaline liquid, whereby both liquid streams are introduced together, has the following drawbacks: in the preparation of acid-soluble low-chlorinated phthalocyanine blue, neutralization treatment is needed to be carried out on acid filter cakes after acid washing, and specific treatment is needed to be carried out at a specific pH value in the neutralization process, so that the preparation requirement of the low-chlorinated phthalocyanine blue is difficult to be met by a simple device.
Disclosure of Invention
Aiming at the defects of the prior art, the utility model provides neutralization equipment after acid washing of low-chlorinated phthalocyanine blue, which solves the problems that in the preparation of acid-soluble low-chlorinated phthalocyanine blue, neutralization treatment is needed to be carried out on acid filter cakes after acid washing, and specific treatment is needed to be carried out at a specific pH value in the neutralization process, and the preparation of low-chlorinated phthalocyanine blue is difficult to be satisfied by a simple device.
The technical aim of the utility model is realized by the following technical scheme:
a low-chloro phthalocyanine blue post-pickling neutralization apparatus comprising: the neutralizing barrel is arranged on the top surface of the base, a supporting rod is fixedly arranged on the top surface of the base, a connecting rod is fixedly arranged on the top surface of the supporting rod, and a turntable is arranged on the bottom surface of the connecting rod; and the stirring assembly is arranged on the bottom surface of the turntable and is used for neutralizing and stirring the acid filter cakes subjected to acid washing.
Through adopting above-mentioned technical scheme, through setting up stirring assembly for neutralization reaction rate guarantees to carry out specific processing under specific PH value.
Preferably, the stirring assembly comprises: the device comprises two limiting frames, wherein the two limiting frames are respectively clamped at the top ends of the neutralization barrel, a reaction basket is fixedly installed between the two limiting frames, the reaction basket is made of a filter screen, a first thread groove is formed in the top surface of the limiting frame, a threaded rod is connected with the inner thread of the first thread groove, two limiting grooves are formed in the bottom surface of the rotary table, and two movable grooves are formed in the inner top surfaces of the limiting grooves respectively.
Through adopting above-mentioned technical scheme, through setting up the reaction basket, the acid filter cake after the pickling can be placed to the reaction basket, and the filter screen can prevent that acid filter cake from spilling into process water to prevent that acid filter cake from dispersing and not being good to take out.
Preferably, the inside of spacing groove is provided with the connecting block, the second thread groove has been seted up to the inside of connecting block, the top surface fixed mounting of connecting block has two spliced poles, two the spliced pole respectively with movable groove movable sleeve establishes, the inside of spacing groove is provided with two springs, two the spring respectively with the spliced pole movable sleeve establishes, the one end of spring with the top surface fixed mounting of connecting block, the other end of spring with the inside top surface fixed mounting of spacing groove.
Through adopting above-mentioned technical scheme, through setting up the spring, the connecting block that the spring can be convenient for upwards pushes up to make the threaded rod unscrew.
Preferably, the bottom surface fixed mounting of carousel has electric putter, electric putter's flexible end fixed mounting has the connection pad, the bottom surface fixed mounting of connection pad has the PH detector.
Through adopting above-mentioned technical scheme, through setting up electric putter, electric putter can drive the PH detector and stretch out and draw back to reach the PH value that detects the inside process water of neutralization bucket.
Preferably, the top surface of neutralization bucket has seted up the mounting groove, the inside fixed mounting of mounting groove has level sensor.
Through adopting above-mentioned technical scheme, through setting up level sensor, level sensor can detect the inside liquid level degree of depth of neutralization bucket to the neutralization bucket inside neutralization liquid content of control.
Preferably, the top surface of carousel has seted up the drive slot, the bottom surface fixed mounting of connecting rod has driving motor, driving motor's output with the fixed cover of drive slot is established.
Through adopting above-mentioned technical scheme, through setting up driving motor, driving motor can provide power for the rotation of carousel, reduces artifical working strength.
In summary, the utility model has the following advantages:
through setting up stirring subassembly, the acid filter cake after the pickling can be placed to the reaction basket, and the filter screen can prevent that acid filter cake from spilling to in the process water to avoid acid filter cake to scatter and be poor take out, put into the inside of reaction basket with the acid filter cake after the pickling, make process water see through the reaction basket, with acid filter cake contact, accelerate neutralization reaction rate, guarantee to carry out specific processing under specific PH value.
Through setting up level sensor, level sensor can detect the inside liquid level degree of depth of neutralization bucket to the inside neutralization liquid content of neutralization bucket is in the control, through setting up the spring, and the connecting block of being convenient for of spring upwards pushes up, thereby makes the threaded rod unscrew.
Drawings
FIG. 1 is a schematic perspective view of the present utility model;
FIG. 2 is a schematic view of a split construction of the present utility model;
FIG. 3 is a schematic view of a spacing structure of the present utility model;
FIG. 4 is a schematic diagram of the turntable structure of the present utility model;
fig. 5 is an enlarged schematic view of a partial structure of fig. 4 a.
Reference numerals: 1. a base; 2. a neutralization barrel; 3. a support rod; 4. a connecting rod; 5. a turntable; 6. a limiting frame; 7. a reaction basket; 8. a first thread groove; 9. a threaded rod; 10. a limit groove; 11. a movable groove; 12. a connecting block; 13. a second thread groove; 14. a connecting column; 15. a spring; 16. an electric push rod; 17. a connecting disc; 18. a PH detector; 19. a mounting groove; 20. a liquid level sensor; 21. a driving groove; 22. and driving the motor.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Referring to fig. 1, fig. 3 and fig. 5, neutralization equipment after low chlorophthalocyanine blue pickling, the on-line screen storage device comprises a base 1, neutralization barrel 2 has been placed to the top surface of base 1, the top surface fixed mounting of base 1 has bracing piece 3, the top surface fixed mounting of bracing piece 3 has connecting rod 4, the bottom surface of connecting rod 4 is provided with carousel 5, the bottom surface of carousel 5 is provided with stirring subassembly for carry out neutralization stirring to the acid cake after the pickling, through setting up stirring subassembly, accelerate neutralization reaction rate, guarantee to carry out specific processing under specific PH value, stirring subassembly includes two limit brackets 6, two limit brackets 6 joint respectively in the top of neutralization barrel 2, fixed mounting has reaction basket 7 between two limit brackets 6, the material of reaction basket 7 is the filter screen, first thread groove 8 has been seted up to the top surface of limit bracket 6, the inside threaded connection of first thread groove 8 has 9, two limit grooves 10 have been seted up respectively to the bottom surface of carousel 5, two movable grooves 11 have been seted up respectively to the inside top surface of two limit grooves 10, through setting up reaction basket 7, acid cake after reaction basket 7 can be placed, can prevent that the filter cake from spilling out in order to take out the filter screen water, can prevent that the acid cake from spilling out after the pickling process.
Referring to fig. 2 and 5, a connecting block 12 is disposed in the limiting groove 10, a second thread groove 13 is disposed in the connecting block 12, two connecting columns 14 are fixedly mounted on the top surface of the connecting block 12, the two connecting columns 14 are movably sleeved with the movable groove 11 respectively, two springs 15 are disposed in the limiting groove 10, the springs 15 are of existing structures and are not described in detail herein, the two springs 15 are movably sleeved with the connecting columns 14 respectively, one end of each spring 15 is fixedly mounted on the top surface of the connecting block 12, the other end of each spring 15 is fixedly mounted on the top surface of the limiting groove 10, the springs 15 are arranged to facilitate the upward pushing of the connecting block 12, so that the threaded rod 9 is screwed out, an electric push rod 16 is fixedly mounted on the bottom surface of the turntable 5, the electric push rod 16 is of an existing structure and is not described herein, a connecting disc 17 is fixedly mounted on the bottom surface of the connecting disc 17, the PH detector 18 is not described herein in detail for the existing structure, the PH detector 18 can be driven by the electric push rod 16, and the PH detector 18 can be stretched out and drawn back by the electric push rod 16, so that the PH detector 18 can reach the PH value of water in the barrel 2.
Referring to fig. 2, the top surface of the neutralization bucket 2 is provided with a mounting groove 19, the inside of the mounting groove 19 is fixedly provided with a liquid level sensor 20, the liquid level sensor 20 is of an existing structure and is not described in detail herein, the liquid level sensor 20 can detect the liquid level depth inside the neutralization bucket 2 by arranging the liquid level sensor 20, so that the neutralization liquid content inside the neutralization bucket 2 is controlled, the top surface of the turntable 5 is provided with a driving groove 21, the bottom surface of the connecting rod 4 is fixedly provided with a driving motor 22, the driving motor 22 is of an existing structure and is not described in detail herein, the output end of the driving motor 22 is fixedly sleeved with the driving groove 21, and the driving motor 22 can provide power for the rotation of the turntable 5 by arranging the driving motor 22, so that the manual working strength is reduced.
Working principle: referring to fig. 1-5, when in use, a worker can put a certain amount of process water into the neutralization bucket 2, put the acid-washed acid filter cake into the reaction basket 7, so that the process water passes through the reaction basket 7 and contacts with the acid filter cake, the two ends of the threaded rod 9 are respectively in threaded connection with the first threaded groove 8 and the second threaded groove 13, the driving motor 22 is started to drive the reaction basket 7 to rotate, after a period of time, the electric push rod 16 is started to drive the PH detector 18 to stretch and retract, thereby achieving the purpose of detecting the PH value of the process water in the neutralization bucket 2, the electric push rod 16 is retracted after the PH control value reaches a specific value, the reaction basket 7 is continuously driven to rotate, so that the acid filter cake is fully reacted with the process water, the spring 15 can facilitate the upward pushing of the connecting block 12, so that the threaded rod 9 is screwed out, the limit frame 6 is taken out, and the neutralized filter cake is taken out in the reaction basket 7 for facilitating the next processing.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. A low-chloro phthalocyanine blue post-pickling neutralization apparatus comprising:
the device comprises a base (1), wherein a neutralization barrel (2) is arranged on the top surface of the base (1), a supporting rod (3) is fixedly arranged on the top surface of the base (1), a connecting rod (4) is fixedly arranged on the top surface of the supporting rod (3), and a turntable (5) is arranged on the bottom surface of the connecting rod (4);
and the stirring assembly is arranged on the bottom surface of the rotary table (5) and is used for neutralizing and stirring the acid filter cakes subjected to acid washing.
2. The post-pickling neutralization apparatus of claim 1, wherein the stirring assembly comprises:
two spacing (6), two spacing (6) joint respectively are in the top of neutralization bucket (2), two fixed mounting has reaction basket (7) between spacing (6), the material of reaction basket (7) is the filter screen, first screw thread groove (8) have been seted up to the top surface of spacing (6), the inside threaded connection of first screw thread groove (8) has threaded rod (9), two spacing groove (10) have been seted up to the bottom surface of carousel (5), two movable groove (11) have been seted up respectively to the inside top surface of spacing groove (10).
3. The low-chlorinated phthalocyanine after-pickling neutralization device according to claim 2, wherein a connecting block (12) is arranged in the limiting groove (10), a second thread groove (13) is formed in the connecting block (12), two connecting columns (14) are fixedly arranged on the top surface of the connecting block (12), the two connecting columns (14) are movably sleeved with the movable groove (11) respectively, two springs (15) are arranged in the limiting groove (10), the two springs (15) are movably sleeved with the connecting columns (14) respectively, one end of each spring (15) is fixedly arranged on the top surface of the connecting block (12), and the other end of each spring (15) is fixedly arranged on the top surface of the inner part of the limiting groove (10).
4. The low-chlorophthalocyanine blue acid-washing after-neutralization device according to claim 1, wherein an electric push rod (16) is fixedly arranged on the bottom surface of the rotary table (5), a connecting disc (17) is fixedly arranged at the telescopic end of the electric push rod (16), and a PH detector (18) is fixedly arranged on the bottom surface of the connecting disc (17).
5. The low-chlorophthalocyanine blue post-pickling neutralization device according to claim 1, wherein a mounting groove (19) is formed in the top surface of the neutralization barrel (2), and a liquid level sensor (20) is fixedly mounted in the mounting groove (19).
6. The low-chloro phthalocyanine blue acid pickling after-neutralization device according to claim 1, wherein a driving groove (21) is formed in the top surface of the turntable (5), a driving motor (22) is fixedly arranged on the bottom surface of the connecting rod (4), and the output end of the driving motor (22) is fixedly sleeved with the driving groove (21).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320566286.4U CN219701893U (en) | 2023-03-22 | 2023-03-22 | Neutralization device after pickling of low-chloro phthalocyanine blue |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320566286.4U CN219701893U (en) | 2023-03-22 | 2023-03-22 | Neutralization device after pickling of low-chloro phthalocyanine blue |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219701893U true CN219701893U (en) | 2023-09-19 |
Family
ID=88014385
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202320566286.4U Active CN219701893U (en) | 2023-03-22 | 2023-03-22 | Neutralization device after pickling of low-chloro phthalocyanine blue |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219701893U (en) |
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2023
- 2023-03-22 CN CN202320566286.4U patent/CN219701893U/en active Active
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