CN219399028U

CN219399028U - Auxiliary device for alkyl sulfonate extraction preparation

Info

Publication number: CN219399028U
Application number: CN202320899959.8U
Authority: CN
Inventors: 罗葵东; 张红丽; 崔宝良; 肖瑞霞
Original assignee: Liaocheng Yili Chemical Co ltd
Current assignee: Liaocheng Yili Chemical Co ltd
Priority date: 2023-04-20
Filing date: 2023-04-20
Publication date: 2023-07-25
Anticipated expiration: 2033-04-20

Abstract

The utility model relates to the technical field of extraction auxiliary devices, and discloses an auxiliary device for extracting and preparing alkyl phenyl sulfonate, which comprises an extraction box, wherein a separating funnel is arranged in the extraction box, the inside of the extraction box is connected with the separating funnel through a clamping mechanism, and an accelerating mechanism is arranged outside the extraction box; the accelerating mechanism comprises a heating ring, a power supply, a gas booster and a vibration exciter, wherein the heating ring is fixedly connected to the inside of the extraction box, the power supply is fixedly connected to the rear side of the outside of the extraction box, the power supply is electrically connected with the heating ring, the gas booster is fixedly connected to one side of the extraction box, the vibration exciter is fixedly connected to the other side of the extraction box, and the clamping mechanism comprises a plurality of pipe sleeves. According to the utility model, the extraction and separation rate between solutions is accelerated through the accelerating mechanism, the production efficiency is improved, the filter screen is arranged to complete the filtration of separated liquid, and the separated liquid is collected into the collecting container, so that the use convenience is improved.

Description

Auxiliary device for alkyl sulfonate extraction preparation

Technical Field

The utility model relates to the technical field of extraction auxiliary devices, in particular to an auxiliary device for preparing alkyl sulfonate by extraction.

Background

Phenyl alkylsulfonate is a chemical substance, light yellowish, transparent liquid, an environmentally friendly plasticizer, and is usually prepared by using an extraction process, wherein the extraction is a unit operation of separating a mixture by utilizing different solubilities of components in a system in solvents, namely a method of transferring solute substances from one solvent to another by utilizing the difference of solubility or partition coefficients of the substances in two solvents which are mutually insoluble (or slightly soluble).

The chinese patent document 202021229525.X discloses a solid phase extraction auxiliary device, including support and sample holding cup, the sample holding cup sets up on the support, and the sample holding cup includes cup body and cup pipe, and the cup pipe sets up the bottom at the cup body, and the support includes base, many spinal branchs daggers and mount pad, and many spinal branchs daggers set up on the base, and the mount pad is fixed to be set up on the top of many spinal branchs daggers. This patent does not increase the extraction separation rate between solutions when performing the auxiliary extraction, resulting in lower production efficiency.

Disclosure of Invention

The utility model aims to solve the defects in the prior art, and provides an auxiliary device for extracting and preparing alkyl sulfonate phenyl ester.

In order to achieve the above purpose, the present utility model adopts the following technical scheme: an auxiliary device for extracting and preparing alkyl sulfonate comprises an extraction box, wherein a separating funnel is arranged in the extraction box, the extraction box is connected with the separating funnel through a clamping mechanism, and an accelerating mechanism is arranged outside the extraction box;

the accelerating mechanism comprises a heating ring, a power supply, a gas booster and a vibration exciter, wherein the heating ring is fixedly connected to the inside of the extraction box, the power supply is fixedly connected to the rear side of the outside of the extraction box, the power supply is electrically connected with the heating ring, the gas booster is fixedly connected to one side of the extraction box, and the vibration exciter is fixedly connected to the other side of the extraction box.

As a further description of the above technical solution:

the clamping mechanism comprises a plurality of pipe sleeves, one ends of the pipe sleeves are fixedly connected to the inside of the extraction box, compression springs are fixedly connected to the inside of the pipe sleeves, sliding columns are fixedly connected to the other sides of the compression springs, and arc-shaped clamping rings are fixedly connected to the other ends of the sliding columns.

As a further description of the above technical solution:

the sliding column is connected inside the pipe sleeve in a sliding way.

As a further description of the above technical solution:

the collecting box is installed to the bottom of extraction case, the inside of collecting box is provided with the filter screen, the inside below sliding connection that is located the filter screen of front side of collecting box has the collecting container.

As a further description of the above technical solution:

the filter screen is an active carbon filter screen.

As a further description of the above technical solution:

the top threaded connection of extraction case has sealed lid, the lateral wall of sealed lid is provided with rubber seal.

As a further description of the above technical solution:

the bottom of extraction case is provided with the weeping mouth, the bottom of separating funnel runs through the weeping mouth.

The utility model has the following beneficial effects:

according to the utility model, firstly, the extraction and separation rate between solutions is accelerated through the accelerating mechanism, the production efficiency is improved, and the separated liquid is filtered through the filter screen and collected into the collecting container, so that the use convenience is improved.

Drawings

FIG. 1 is a perspective view of an auxiliary device for phenyl alkylsulfonate extraction according to the present utility model;

FIG. 2 is a schematic view of a separating funnel of an auxiliary device for preparing alkyl sulfonate by extraction;

FIG. 3 is a schematic illustration of a jacket of an auxiliary device for phenyl alkylsulfonate extraction according to the present utility model;

FIG. 4 is a schematic diagram of a spring of an auxiliary device for phenyl alkylsulfonate extraction according to the present utility model;

fig. 5 is a schematic diagram of a filter screen of an auxiliary device for alkyl sulfonate extraction preparation according to the present utility model.

Legend description:

1. an extraction box; 2. a separating funnel; 3. a pipe sleeve; 4. a compression spring; 5. a spool; 6. an arc-shaped clamping ring; 7. a leak; 8. a heating ring; 9. a power supply; 10. a gas booster; 11. a vibration exciter; 12. a collection box; 13. a filter screen; 14. a collection container; 15. sealing cover.

Detailed Description

The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.

Referring to fig. 1-5, one embodiment provided by the present utility model is: an auxiliary device for extracting and preparing alkyl sulfonate comprises an extraction box 1, wherein a separating funnel 2 is arranged in the extraction box 1, the inside of the extraction box 1 is connected with the separating funnel 2 through a clamping mechanism, and an accelerating mechanism is arranged outside the extraction box 1; the accelerating mechanism comprises a heating ring 8, a power supply 9, a gas booster 10 and a vibration exciter 11, wherein the heating ring 8 is fixedly connected in the extraction box 1, the power supply 9 is fixedly connected at the rear side outside the extraction box 1, the power supply 9 is electrically connected with the heating ring 8, the gas booster 10 is fixedly connected at one side of the extraction box 1, the vibration exciter 11 is fixedly connected at the other side of the extraction box 1, the clamping mechanism comprises a plurality of pipe sleeves 3, one end of each pipe sleeve 3 is fixedly connected in the extraction box 1, the compression spring 4 is fixedly connected in the pipe sleeve 3, the slide column 5 is fixedly connected at the other side of each compression spring 4, the arc-shaped clamping ring 6 is fixedly connected at the other end of each slide column 5, the separating funnel 2 filled with mixed liquid is placed in the extraction box 1, and due to the compression spring 4 arranged in the pipe sleeve 3, the sliding column 5 is driven to move towards the direction close to the separating funnel 2, the arc clamping rings 6 are driven to move in a following manner, the separating funnel 2 is clamped and fixed through the combined action of the arc clamping rings 6 arranged around, the bottom of the separating funnel 2 is aligned to the inside of the collecting box 12 through the leak opening 7, then, the top of the extraction box 1 is sealed and covered by the rotary sealing cover 15, and then the rotary sealing cover is simultaneously started, the power supply 9, the gas booster 10 and the vibration exciter 11 are simultaneously started, the power supply 9 is started, the temperature of the extraction box 1 is lifted through the heating ring 8, the gas booster 10 is started to pressurize the inside, meanwhile, the vibration exciter 11 is started, high-frequency oscillation is generated on the solution in the separating funnel 2, the extraction separation rate between the solutions is accelerated through the operations, and the production efficiency is improved.

The slide post 5 sliding connection installs the collecting box 12 in the inside of pipe box 3, the inside of collecting box 12 is provided with filter screen 13, the inside below sliding connection who is located filter screen 13 of collecting box 12 is provided with collecting vessel 14, after the extraction is accomplished, pick up extracting box 1, open the valve of separating funnel 2 bottom, place extracting box 1 again on collecting box 12, the liquid of separation falls into collecting vessel 14 inside through the filtration of filter screen 13 at last, finally take out collecting vessel 14 and can accomplish the collection, the convenience of using has been improved, filter screen 13 is the active carbon filter screen, better filterability, the top threaded connection of extracting box 1 has sealed lid 15, sealed lid 15's lateral wall is provided with rubber seal, the improvement leakproofness, extracting box 1's bottom is provided with leak 7, separating funnel 2's bottom runs through leak 7, separating liquid is from separating funnel 2 bottom, through leak 7 entering collecting box 12 inside, accomplish the filtration collection in the collecting vessel 14 at last.

Working principle: firstly, place separating funnel 2 that fills mixed liquor inside extraction case 1, because the inside compression spring 4 that is provided with of pipe box 3, under compression spring 4's elasticity restoring force, drive slide 5 and remove towards the direction that is close to separating funnel 2, and then drive arc clamping ring 6 and follow the removal, through a plurality of arc clamping rings 6 combined action that set up all around, carry out centre gripping fixing to separating funnel 2, the bottom of separating funnel 2 is aimed at the inside of collecting box 12 through weep hole 7 this moment, then, rotary seal lid 15 seals and covers extraction case 1 top, simultaneously start, power 9, gas booster 10 and vibration exciter 11, the start of power 9 carries out the temperature promotion to extraction case 1 inside through heating ring 8, gas booster 10 starts to inside pressurization, the start of vibration exciter 11 simultaneously, produce high-frequency oscillation to the solution inside separating funnel 2, through above operation, the extraction separation rate between the solution has been accelerated, after the extraction is accomplished, take extraction case 1 up, the valve in separating funnel 2 bottom is opened, place extraction case 1 again on collecting case 12, the liquid that separates and finally falls into the inside of collecting container 14 through the filter screen 13, the filter screen that can be convenient and easy to collect, the container is finished.

Finally, it should be noted that: the foregoing description is only illustrative of the preferred embodiments of the present utility model, and although the present utility model has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described, or equivalents may be substituted for elements thereof, and any modifications, equivalents, improvements or changes may be made without departing from the spirit and principles of the present utility model.

Claims

1. The utility model provides an auxiliary device of alkyl sulfonate phenyl ester extraction preparation, includes extraction case (1), its characterized in that: the extraction box is characterized in that a separating funnel (2) is arranged in the extraction box (1), the inside of the extraction box (1) is connected with the separating funnel (2) through a clamping mechanism, and an accelerating mechanism is arranged outside the extraction box (1);

the accelerating mechanism comprises a heating ring (8), a power supply (9), a gas booster (10) and a vibration exciter (11), wherein the heating ring (8) is fixedly connected to the inside of the extraction box (1), the power supply (9) is fixedly connected to the rear side of the outside of the extraction box (1), the power supply (9) is electrically connected with the heating ring (8), the gas booster (10) is fixedly connected to one side of the extraction box (1), and the vibration exciter (11) is fixedly connected to the other side of the extraction box (1).

2. An auxiliary device for the extraction and preparation of phenyl alkylsulfonate as claimed in claim 1, wherein: the clamping mechanism comprises a plurality of pipe sleeves (3), one end of each pipe sleeve (3) is fixedly connected with the inside of the extraction box (1), a compression spring (4) is fixedly connected with the inside of each pipe sleeve (3), a sliding column (5) is fixedly connected with the other side of each compression spring (4), and an arc-shaped clamping ring (6) is fixedly connected with the other end of each sliding column (5).

3. An auxiliary device for the extraction and preparation of phenyl alkylsulfonate as claimed in claim 2, wherein: the sliding column (5) is connected inside the pipe sleeve (3) in a sliding way.

4. An auxiliary device for the extraction and preparation of phenyl alkylsulfonate as claimed in claim 1, wherein: the bottom of extraction case (1) is installed collecting box (12), the inside of collecting box (12) is provided with filter screen (13), the inside below sliding connection that is located filter screen (13) of front side of collecting box (12) has collecting vessel (14).

5. The auxiliary device for the extraction and preparation of phenyl alkylsulfonate according to claim 4, wherein: the filter screen (13) is an active carbon filter screen.

6. An auxiliary device for the extraction and preparation of phenyl alkylsulfonate as claimed in claim 1, wherein: the top thread connection of extraction case (1) has sealed lid (15), the lateral wall of sealed lid (15) is provided with rubber seal.

7. An auxiliary device for the extraction and preparation of phenyl alkylsulfonate as claimed in claim 1, wherein: the bottom of extraction case (1) is provided with weeping mouth (7), the bottom of separating funnel (2) runs through weeping mouth (7).