CN219377517U - Crude product centrifugal equipment - Google Patents
Crude product centrifugal equipment Download PDFInfo
- Publication number
- CN219377517U CN219377517U CN202320723649.0U CN202320723649U CN219377517U CN 219377517 U CN219377517 U CN 219377517U CN 202320723649 U CN202320723649 U CN 202320723649U CN 219377517 U CN219377517 U CN 219377517U
- Authority
- CN
- China
- Prior art keywords
- motor
- separating cylinder
- crude
- separating
- hole
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000012043 crude product Substances 0.000 title abstract description 5
- 230000000694 effects Effects 0.000 claims abstract description 8
- 238000005119 centrifugation Methods 0.000 claims 6
- 238000000926 separation method Methods 0.000 abstract description 33
- 239000000463 material Substances 0.000 abstract description 10
- 238000003889 chemical engineering Methods 0.000 abstract description 2
- 239000012847 fine chemical Substances 0.000 abstract description 2
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 7
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 238000006146 oximation reaction Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- YDVGBUGJAICLHV-UHFFFAOYSA-N 2-(hydroxyamino)-1-phenylethanone Chemical class ONCC(=O)C1=CC=CC=C1 YDVGBUGJAICLHV-UHFFFAOYSA-N 0.000 description 1
- 150000008062 acetophenones Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Centrifugal Separators (AREA)
Abstract
The utility model relates to the technical field of fine chemical engineering, and discloses crude product centrifugal equipment, which comprises a separation box, wherein a motor seat is fixedly arranged at the bottom of the separation box, a first motor is fixedly arranged in the motor seat, and an output shaft of the first motor is fixedly connected with a rotating shaft. According to the utility model, after the rotary separation is completed, the first motor is kept to drive the first separating cylinder to rotate, the second motor is matched with the start of the second motor, the long shaft is driven to rotate, the cam on the long shaft is rotated, the cam is driven to rotate at the bottom of the first separating cylinder, and meanwhile, the elastic action of the top spring is utilized, so that the first separating cylinder continuously performs up-and-down vibration motion after the separation, the integral vibration is realized, and crude materials blocked or attached to the inner wall of the first separating cylinder are loosened and gathered in the first separating cylinder, so that the disassembly and the discharge are performed, the actual discharge effect is good, and the discharge completion amount is improved.
Description
Technical Field
The utility model relates to the technical field of fine chemical engineering, in particular to crude product centrifugal equipment.
Background
The alpha-hydroxyaminoacetophenone derivative is used as an important intermediate raw material (such as a photoinitiator preparation raw material), and the prior art mostly adopts oximation (also called isosulfing) reaction to prepare the alpha-oximation acetophenone derivative, but has the following technical defects: a) Ethyl acetate is usually used as a solvent, hydrochloric acid is used for catalysis, nitrite is solid and is insoluble in an organic solvent, and centrifugal separation is usually needed to complete separation and acquisition of crude nitrite when mixed nitrite is acquired.
In the prior art, coarse nitrite is mixed in an insoluble organic solvent in the use process, and is put into a separation device for centrifugal separation after being fully mixed to obtain coarse nitrite, however, after actual centrifugal separation, part of coarse nitrite with particles suitable for filter holes is blocked or adhered to the filter holes of a separation cylinder, so that the coarse nitrite adhered or blocked on the separation cylinder is difficult to separate and discharge in the separation cylinder, the actual discharge efficiency is low, and the use effect is poor.
Disclosure of Invention
In order to overcome the defects of the prior art, the utility model provides crude product centrifugal equipment, which has the advantages of improving the separation discharging effect and effectively separating and obtaining the coarse and fine raw materials.
In order to achieve the above purpose, the present utility model provides the following technical solutions: the utility model provides a crude centrifugal equipment, includes the separator box, the bottom fixed mounting of separator box has the motor cabinet, the inside fixed mounting of motor cabinet has a motor, the output shaft fixedly connected with pivot of a motor, the upper end of pivot passes the separator box and extends to the inside of separator box, the top movable mounting of pivot has a separating drum, a hole has been seted up to the surface of separating drum, the top cap has been cup jointed to the top surface screw thread of separator box, the loop bar has been cup jointed in the top surface activity of top cap, the bottom surface fixedly connected with limiting plate of loop bar, fixed intercommunication has the spring between the top surface of limiting plate and the top cap, the below of a separating drum is equipped with the cam, the internal surface fixed sleeve of cam has the major axis, the surface fixed mounting of separator box has the motor frame, the inside fixed mounting of motor frame has No. two motors, the output shaft and major axis fixed connection of No. two motors.
As a preferable technical scheme of the utility model, the outer surface of the first separating cylinder is fixedly sleeved with a mounting ring, and the top surface of the mounting ring is in threaded sleeve connection with the second separating cylinder.
As a preferable technical scheme of the utility model, a second hole is formed in the outer surface of the second separating cylinder, and the second separating cylinder is positioned on the outer side of the first separating cylinder.
As a preferable technical scheme of the utility model, the top surface of the mounting ring is provided with a thread groove, and the inner surface of the thread groove is in threaded sleeve joint with the second separating cylinder.
As a preferable technical scheme of the utility model, the bottom surface of the first separating cylinder is fixedly provided with a bottom plate, and the bottom surface of the bottom plate is provided with a clamping hole.
As a preferable technical scheme of the utility model, the top surface of the rotating shaft is fixedly connected with a clamping block, and the outer surface of the clamping block is movably sleeved with the clamping hole.
As a preferable technical scheme of the utility model, the diameter of the first hole is larger than that of the second hole, and the diameter of the limiting plate is larger than that of the top of the first separating cylinder.
Compared with the prior art, the utility model has the following beneficial effects:
after the rotary separation is completed, the first separating cylinder is driven to rotate by the first motor, the second motor is matched to start, the long shaft is driven to rotate by the second motor, the cam on the long shaft is rotated, the cam is driven to rotate at the bottom of the first separating cylinder, the elastic action of the top spring is utilized, the first separating cylinder continuously moves up and down in vibration after separation, the integral vibration is realized, and crude materials blocked or attached to the inner wall of the first separating cylinder are loosened and gathered in the first separating cylinder, so that the discharge is detached, the actual discharge effect is good, and the discharge completion amount is improved.
The mounting ring is fixedly sleeved on the outer surface of the first separating cylinder, the thread groove is formed in the top surface of the mounting ring, the thread groove is utilized to complete the thread sleeving of the second separating cylinder, the first Kong Wancheng thick and thin materials on the first separating cylinder are utilized to separate and screen in the actual separating process, and the second holes are utilized to filter out the mixed insoluble solvents, so that the thick and thin materials are easy to mix and separate and centrifugally separate, and the actual separating and collecting effect is comprehensively improved.
Drawings
FIG. 1 is a schematic diagram of the structure of the present utility model;
FIG. 2 is a schematic cross-sectional view of the present utility model;
FIG. 3 is an exploded view of the present utility model between the top cover and the retainer plate;
FIG. 4 is an exploded view of the cartridge and bottom plate of the present utility model;
FIG. 5 is a schematic illustration of the socket joint between the cam and the long shaft of the present utility model;
FIG. 6 is a schematic view of a mounting ring of the present utility model.
In the figure: 1. a separation box; 2. a motor base; 3. a motor I; 4. a rotating shaft; 5. a first separating cylinder; 6. a first hole; 7. a second separating cylinder; 8. a second hole; 9. a top cover; 10. a loop bar; 11. a limiting plate; 12. a spring; 13. a cam; 14. a motor frame; 15. a motor II; 16. a long axis; 17. a mounting ring; 18. a thread groove; 19. a bottom plate; 20. a clamping hole; 21. and (5) clamping blocks.
Detailed Description
The technical solutions in the embodiments of the present utility model will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model.
As shown in fig. 1 to 6, the utility model provides crude centrifugal equipment, which comprises a separation box 1, wherein a motor seat 2 is fixedly arranged at the bottom of the separation box 1, a first motor 3 is fixedly arranged in the motor seat 2, an output shaft of the first motor 3 is fixedly connected with a rotating shaft 4, the upper end of the rotating shaft 4 penetrates through the separation box 1 and extends into the separation box 1, a first separation cylinder 5 is movably arranged at the top of the rotating shaft 4, a first hole 6 is formed in the outer surface of the first separation cylinder 5, a top cover 9 is sleeved on the top surface of the separation box 1 in a threaded manner, a sleeve rod 10 is movably sleeved on the top surface of the top cover 9, a limiting plate 11 is fixedly connected with the bottom surface of the sleeve rod 10, a spring 12 is fixedly communicated between the top surface of the limiting plate 11 and the top cover 9, a cam 13 is arranged below the first separation cylinder 5, a long shaft 16 is fixedly sleeved on the inner surface of the cam 13, a motor frame 14 is fixedly arranged on the outer surface of the separation box 1, a second motor 15 is fixedly arranged in the inner part of the motor frame 14, and the output shaft of the second motor 15 is fixedly connected with the long shaft 16.
The outer surface of the first separating cylinder 5 is fixedly sleeved with a mounting ring 17, and the top surface of the mounting ring 17 is in threaded sleeve connection with the second separating cylinder 7. The installation of the second separating cylinder 7 is realized by utilizing the mounting ring 17, and the separation and collection of fine materials are realized by the second separating cylinder 7. The surface of the second separating cylinder 7 is provided with a second hole 8, and the second separating cylinder 7 is positioned at the outer side of the first separating cylinder 5. And the mixed solvent flows out by utilizing a second hole 8 on a second separating cylinder 7, and fine materials separated once are separated and filtered, so that double separation and collection are realized.
The top surface of the mounting ring 17 is provided with a thread groove 18, and the inner surface of the thread groove 18 is in threaded sleeve joint with the second separating cylinder 7. Through seting up thread groove 18 and making No. two separating drum 7 screw cup joint, be convenient for install and separation, easy operation, the separation is convenient.
The bottom surface of the first separating cylinder 5 is fixedly provided with a bottom plate 19, and the bottom surface of the bottom plate 19 is provided with a clamping hole 20. The clamping sleeve is completed by sleeving the clamping block 21 on the rotary shaft 4 through the bottom plate 19, the first separating cylinder 5 can be driven to rotate when the rotary shaft 4 is guaranteed to rotate, and meanwhile, the material is conveniently taken out by being conveniently dismounted upwards.
The top surface of the rotating shaft 4 is fixedly connected with a clamping block 21, and the outer surface of the clamping block 21 is movably sleeved with the clamping hole 20. The clamping is completed by sleeving the clamping holes 20 with the clamping blocks 21 with the protrusions on the two sides.
The diameter of the first hole 6 is larger than that of the second hole 8, and the diameter of the limiting plate 11 is larger than that of the top of the first separating cylinder 5. The diameters of the first hole 6 and the second hole 8 are controlled, the separation and collection specification of crude materials is controlled, and the size of the limiting plate 11 is controlled to complete good sealing control of the top surface of the first separating cylinder 5.
The first separating cylinder 5 is arranged at the top of the rotating shaft 4, a clamping block 21 at the top of the rotating shaft 4 is sleeved in a clamping hole 20 on the top surface of a bottom plate 19, the second separating cylinder 7 is in threaded sleeve connection with a threaded groove 18, the mixed solution is put into the first separating cylinder 5 and covered with a top cover 9, a limiting plate 11 downwards covers the top of the first separating cylinder 5, meanwhile, a spring 12 is compressed, a first motor 3 is started for rotary separation, crude materials are trapped in the first separating cylinder 5, fine materials are trapped in the second separating cylinder 7, a solvent flows out of the separating box 1, the second motor 15 is kept to be continuously rotated and started after separation is completed, the second motor 15 drives a cam 13 on a long shaft 16 to rotate and impacts the first separating cylinder 5, the first separating cylinder 5 moves up and down, the spring 12 is vibrated, all motors are closed after collision vibration is completed, the top cover 9 is rotated, the first separating cylinder 5 and the second separating cylinder 7 are taken out of the separating box 1, and separation discharging is completed.
Claims (7)
1. Crude centrifugal equipment, including separator box (1), its characterized in that: the utility model discloses a motor cabinet (2) is installed to the bottom fixed mounting of separator box (1), the inside fixed mounting of motor cabinet (2) has motor (3) No. one, the output shaft fixedly connected with pivot (4) of motor (3) No. one, the upper end of pivot (4) passes separator box (1) and extends to the inside of separator box (1), the top movable mounting of pivot (4) has a separating drum (5), a hole (6) has been seted up to the surface of separating drum (5), top screw thread of separator box (1) has cup jointed top lid (9), the top surface activity of top lid (9) has cup jointed loop bar (10), the bottom surface fixedly connected with limiting plate (11) of loop bar (10), fixed intercommunication has spring (12) between the top surface of limiting plate (11) and top lid (9), the below of separating drum (5) is equipped with cam (13), the internal surface fixed major axis (16) that cup joints of cam (13), the surface fixed mounting of motor (14) of separator box (1) has motor (14), no. two output shaft (15) are connected with inside fixed mounting of motor (15).
2. A crude centrifugation device as claimed in claim 1, wherein: the outer surface of the first separating cylinder (5) is fixedly sleeved with a mounting ring (17), and the top surface of the mounting ring (17) is in threaded sleeve connection with the second separating cylinder (7).
3. A crude centrifugation device as claimed in claim 2, characterized in that: and a second hole (8) is formed in the outer surface of the second separating cylinder (7), and the second separating cylinder (7) is positioned on the outer side of the first separating cylinder (5).
4. A crude centrifugation device as claimed in claim 2, characterized in that: the top surface of the mounting ring (17) is provided with a thread groove (18), and the inner surface of the thread groove (18) is in threaded sleeve connection with the second separating cylinder (7).
5. A crude centrifugation device as claimed in claim 1, wherein: the bottom surface of a first separating cylinder (5) is fixedly provided with a bottom plate (19), and the bottom surface of the bottom plate (19) is provided with a clamping hole (20).
6. A crude centrifugation device as claimed in claim 1, wherein: the top surface fixedly connected with fixture block (21) of pivot (4), the surface and the card hole (20) activity of fixture block (21) cup joint.
7. A crude centrifugation device as claimed in claim 1, wherein: the diameter of the first hole (6) is larger than that of the second hole (8), and the diameter of the limiting plate (11) is larger than that of the top of the first separating cylinder (5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320723649.0U CN219377517U (en) | 2023-04-04 | 2023-04-04 | Crude product centrifugal equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320723649.0U CN219377517U (en) | 2023-04-04 | 2023-04-04 | Crude product centrifugal equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219377517U true CN219377517U (en) | 2023-07-21 |
Family
ID=87166617
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202320723649.0U Active CN219377517U (en) | 2023-04-04 | 2023-04-04 | Crude product centrifugal equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219377517U (en) |
-
2023
- 2023-04-04 CN CN202320723649.0U patent/CN219377517U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 225400 east side of Binjiang Road, Taixing Economic Development Zone, Taizhou City, Jiangsu Province Patentee after: Taixing Qiangli Xianxian Electronic New Materials Co.,Ltd. Address before: 225400 east side of Binjiang Road, Taixing Economic Development Zone, Taizhou City, Jiangsu Province Patentee before: Taixing Xianxian Chemical Co.,Ltd. |