CN219334220U

CN219334220U - Pipeline reaction device for synthesizing chloramine

Info

Publication number: CN219334220U
Application number: CN202221848133.0U
Authority: CN
Inventors: 路勇; 陈艳艳; 李波; 于如军
Original assignee: Shandong Jiayu Chemical Technology Co ltd
Current assignee: Shandong Jiayu Chemical Technology Co ltd
Priority date: 2022-07-18
Filing date: 2022-07-18
Publication date: 2023-07-14
Anticipated expiration: 2032-07-18

Abstract

The utility model relates to the technical field of reaction equipment, in particular to a pipeline reaction device for synthesizing chloramine, which comprises an adjusting component, wherein the adjusting component is provided with a reaction component, the reaction component comprises a reaction barrel, a barrel cover is fixedly arranged above the reaction barrel, a straight water pipe is inserted above the barrel cover, the adjusting component comprises a temperature control barrel, the temperature control barrel is arranged below a feeding barrel, one side of the temperature control barrel is provided with a rotary handle, and one side of the temperature control barrel is provided with a water pump.

Description

Pipeline reaction device for synthesizing chloramine

Technical Field

The utility model relates to the technical field of reaction equipment, in particular to a pipeline reaction device for synthesizing chloramine.

Background

The chloro-amine is a chemical substance named as O-3-chloro-2-propenyl hydroxyl, the chemical substance is required to be added for reaction in the production process of the chloro-amine, then the chloro-amine is stood for layering, the reaction speed is too slow in the normal temperature state, and a large amount of heat is released for explosion to cause loss in the reaction of the chloro-amine;

the utility model discloses a reation kettle for neutralization of chloramine, the device passes through the box, the pivot, a support, the fixture block, puddler and thin strip's setting, operating personnel can add the chloramine raw materials on the shrouding of adding the mouth inside, the shrouding receives weight and can overturn through the loose axle, make chloramine raw materials add in the box, the top at the box is installed to the motor, can drive the pivot and rotate, the pivot drives the support and rotates, the puddler can carry out the block through the fixture block and be connected with the support, the puddler follows the support and rotates, at rotatory in-process, stir the material that the box is inside to add through the puddler, make it mix, liquid also accessible through-hole circulate during the stirring simultaneously, the thin strip of puddler both sides can promote the flow between the material liquid, be favorable to promoting the even mixing between the material that adds, simultaneously can know the pH value of chloramine mixed liquid through the PH value detector.

However, in general reaction equipment, the separation mode of the organic layer and the water layer is usually to suck the water layer by using a rubber head suction pipe, or to pour the water layer to separate, and suction by using a suction pipe is more troublesome, the suction efficiency needs to be repeated back and forth, the pouring mode can enable the water layer and the organic layer to incline at the same time, and the organic layer can be poured out when the water layer is poured out, so that partial waste is caused, and the separation effect is poor. In view of this, we propose a pipeline reaction apparatus for the synthesis of chloramine.

Disclosure of Invention

In order to overcome the defects, the utility model provides a pipeline reaction device for synthesizing chloramine.

The technical scheme of the utility model is as follows:

the utility model provides a pipeline reaction unit for synthesizing chloramine, includes adjusting part, be equipped with reaction unit on the adjusting part, reaction unit includes the reaction bucket, reaction bucket top fixed mounting has the bung, bung top fixed mounting has a plurality of inlet pipes, rotatable mounting in inlet pipe middle part has the fixture block, inlet pipe top fixed mounting has the feedwell, peg graft in bung top has the straight water pipe, adjusting part includes the accuse temperature bucket, the feedwell below is located to the accuse temperature bucket, and the accuse temperature bucket can overlap to establish outside the reaction bucket, accuse temperature bucket bilateral symmetry fixed mounting has riser one, riser one bottom fixed mounting has the cylinder.

As the preferable technical scheme of the utility model, the two sides of the reaction barrel are symmetrically and fixedly provided with the side plates, the two sides of the barrel cover are fixedly provided with the transverse plates, and the upper part of the straight water pipe is in threaded connection with the fixing ring.

As the preferable technical scheme of the utility model, two sides of the temperature control barrel are symmetrically provided with the second vertical plates, the outer sides of the lower parts of the second vertical plates are fixedly provided with the base, and the upper parts of the base are fixedly provided with the air cylinders.

As the preferable technical scheme of the utility model, a fixed block is fixedly arranged on the output shaft of the air cylinder, a straight rod is rotatably arranged in the middle of the fixed block, the straight rod passes through the fixed block, extends between two vertical plates II and is fixedly connected with a side plate, and a rotary handle is fixedly arranged on one side of one straight rod.

As the preferable technical scheme of the utility model, a water pump is fixedly arranged above one of the bases, a water hose is fixedly connected above the water pump, and the water hose passes through a second vertical plate on the same side and is fixedly connected with a straight water pipe.

As the preferable technical scheme of the utility model, the two inner side walls of the vertical plate are provided with lifting grooves, transverse grooves are arranged above the lifting grooves, the transverse plates are inserted into the transverse grooves, and the straight rods move up and down in the lifting grooves.

Compared with the prior art, the utility model has the beneficial effects that:

according to the utility model, the temperature control barrel is sleeved outside the reaction barrel, the reaction of the chloramine is rapid by adjusting the temperature of the reaction barrel, so that the chloramine can react in a stable and rapid environment, the straight water pipe is fixedly arranged above the barrel cover and can be directly inserted into the boundary point between the water layer and the organic layer, the length of the straight water pipe only contacts the water layer but does not contact the organic layer, the organic layer is not sucked when the water layer is sucked by the water pump, the separation effect of the water layer and the organic layer is improved, and then the chloramine organic layer is poured out by rotating the reaction barrel through the rotating handle, so that the method is very simple, convenient and rapid, and the efficiency is improved.

Drawings

FIG. 1 is a schematic diagram of the overall structure of the present utility model;

FIG. 2 is a second schematic diagram of the overall structure of the present utility model;

FIG. 3 is a schematic structural diagram of a reaction module according to the present utility model;

FIG. 4 is a schematic view of the structure of the adjusting assembly according to the present utility model.

The significance of each punctuation mark in the figure is as follows:

1. and (3) a reaction assembly: 11. a reaction barrel; 12. a feed barrel; 13. a feed pipe; 14. a side plate; 15. a barrel cover; 16. a fixing ring; 17. a straight water pipe; 18. a cross plate; 19. a clamping block;

2. and an adjusting assembly: 21. a second vertical plate; 22. rotating the handle; 23. a fixed block; 24. a cylinder; 25. a base; 26. a flexible water pipe; 27. a first vertical plate; 28. a temperature control barrel; 29. a straight rod; 210. a water pump; 211. a lifting groove; 212. and a transverse groove.

Detailed Description

The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.

In the description of the present utility model, it should be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", etc. indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings are merely for convenience in describing the present utility model and simplifying the description, and do not indicate or imply that the apparatus or elements referred to must have a specific orientation, be configured and operated in a specific orientation, and thus should not be construed as limiting the present utility model.

Referring to fig. 1-4, the present utility model provides a technical solution:

the utility model provides a pipeline reaction unit for synthesizing chloramine, including adjusting part 2, be equipped with reaction unit 1 on the adjusting part 2, reaction unit 1 includes reaction barrel 11, reaction barrel 11 top fixed mounting has bung 15, bung 15 top fixed mounting has a plurality of inlet pipes 13, rotatable mounting in inlet pipe 13 middle part has fixture block 19, inlet pipe 13 top fixed mounting has feedwell 12, peg graft has straight water pipe 17 above bung 15, adjusting part 2 includes accuse temperature bucket 28, accuse temperature bucket 28 locates feedwell 12 below, and accuse temperature bucket 28 can overlap to establish outside reaction barrel 11, accuse temperature bucket 28 bilateral symmetry fixed mounting has riser one 27, riser one 27 bottom fixed mounting has cylinder 24, accuse temperature bucket 28 is equipped with the cold water pipe, through going into hot water and cold water regulation temperature, when just beginning the reaction, add hot water heating reaction barrel and make inside reaction faster, can produce a large amount of heats after the reflection, add the cold water cooling in the accuse bucket 28.

The side plates 14 are symmetrically and fixedly arranged on two sides of the reaction barrel 11, the transverse plates 18 are fixedly arranged on two sides of the barrel cover 15, the fixing rings 16 are connected with the upper parts of the straight water pipes 17 in a threaded manner, the fixing rings 16 are used for adjusting the length of the straight water pipes 17 extending into the reaction barrel 11 in a rotating manner, so that the straight water pipes 17 can only extend into a water layer and are not contacted with an organic layer, the water layer is prevented from being sucked through the water pump 210, the organic layer is prevented from being sucked, and the poor separation effect between the organic layer and the water intake layer is avoided.

The temperature control barrel 28 bilateral symmetry is equipped with riser two 21, and riser two 21 below outside is all fixed mounting has base 25, and base 25 top fixed mounting has cylinder 24, and fixed mounting has fixed block 23 on the cylinder 24 output shaft, and fixed block 23 middle part rotatable installation has straight-bar 29, and straight-bar 29 passes fixed block 23 and extends to between two riser two 21 and with curb plate 14 fixed connection, and one of them straight-bar 29 one side fixed mounting has rotatory handle 22, and rotatory handle 22 can drive reaction barrel 11 rotation and make the chloramine of production pour reaction barrel 11.

One of them base 25 top fixed mounting has water pump 210, and water pump 210 top fixed connection has hose 26, and hose 26 passes riser two 21 of homonymy and with straight water pipe 17 fixed connection, riser two 21 inside wall is equipped with lift groove 211, and the lift groove 211 top is equipped with horizontal groove 212, and horizontal plate 18 is pegged graft in horizontal groove 212, and straight-bar 29 reciprocates in lift groove 211, through the effect of cylinder 24, makes reaction barrel 11 reciprocate and opens and shuts with bung 15.

When the equipment is used by operators, reactants are added into the feeding barrel 12 in proportion, the rotary clamping blocks 19 are used for adjusting the quantity of the reactants, the reactants enter the reaction barrel 11, the air cylinder 24 below the temperature control barrel 28 is started to support the temperature control barrel 28 to be sleeved outside the reaction barrel 11, hot water is added into the temperature control barrel 28 to accelerate the reaction speed in the reaction barrel 11, after a certain period of time, a large amount of heat is released in the reaction barrel 11, hot water in the temperature control barrel 28 is discharged, cold water is added into the reaction barrel 11 to cool the reaction barrel, after the reaction is completed, the air cylinder 24 below the temperature control barrel 28 is started to enable the temperature control barrel 28 to be separated from the reaction barrel 11, standing and layering are carried out, the water pump 210 is started to draw out a water layer in the reaction barrel 11, then the air cylinder 24 above the base 25 is started to enable a certain distance to be reserved between the reaction barrel 11 and the barrel cover 15, the rotary handle 22 is rotated to drive the reaction barrel 11 to rotate, and a chloroamine organic layer produced in the reaction barrel 11 is poured into a container.

The foregoing has shown and described the basic principles, principal features and advantages of the utility model. It will be understood by those skilled in the art that the present utility model is not limited to the above-described embodiments, and that the above-described embodiments and descriptions are only preferred embodiments of the present utility model, and are not intended to limit the utility model, and that various changes and modifications may be made therein without departing from the spirit and scope of the utility model as claimed. The scope of the utility model is defined by the appended claims and equivalents thereof.

Claims

1. A pipe reaction device for the synthesis of chloramine, comprising a conditioning assembly (2), characterized in that: be equipped with reaction subassembly (1) on adjusting part (2), reaction subassembly (1) includes reaction bucket (11), reaction bucket (11) top fixed mounting has bung (15), bung (15) top fixed mounting has a plurality of inlet pipes (13), fixture block (19) are rotatably installed at inlet pipe (13) middle part, inlet pipe (13) top fixed mounting has feeding bucket (12), bung (15) top grafting has straight water pipe (17), adjusting part (2) include accuse temperature bucket (28), accuse temperature bucket (28) are located feeding bucket (12) below, and accuse temperature bucket (28) can overlap to establish in reaction bucket (11) outside, accuse temperature bucket (28) both sides symmetry fixed mounting has riser one (27), riser one (27) bottom fixed mounting has cylinder (24).

2. The pipe reaction apparatus for synthesizing chloramine as set forth in claim 1, wherein: the side plates (14) are symmetrically and fixedly arranged on two sides of the reaction barrel (11), the transverse plates (18) are fixedly arranged on two sides of the barrel cover (15), and the fixing rings (16) are connected with the upper side of the straight water pipe (17) in a threaded manner.

3. A pipeline reaction apparatus for synthesizing a chloroamine according to claim 2, wherein: the temperature control barrel (28) bilateral symmetry is equipped with riser two (21), riser two (21) below outside all fixed mounting has base (25), base (25) top fixed mounting has cylinder (24).

4. A pipeline reaction apparatus for synthesizing a chloroamine according to claim 3, wherein: the cylinder (24) output shaft is fixedly provided with a fixed block (23), the middle part of the fixed block (23) is rotatably provided with a straight rod (29), the straight rod (29) penetrates through the fixed block (23) to extend between two vertical plates (21) and is fixedly connected with the side plate (14), and one side of the straight rod (29) is fixedly provided with a rotary handle (22).

5. The pipe reaction apparatus for synthesizing chloramine as set forth in claim 4, wherein: one of them base (25) top fixed mounting has water pump (210), water pump (210) top fixedly connected with hose (26), hose (26) pass riser two (21) of homonymy and with straight water pipe (17) fixed connection.

6. The pipe reaction apparatus for synthesizing chloramine as set forth in claim 5, wherein: the inner side wall of the second vertical plate (21) is provided with a lifting groove (211), a transverse groove (212) is formed above the lifting groove (211), the transverse plate (18) is inserted into the transverse groove (212), and the straight rod (29) moves up and down in the lifting groove (211).