CN219251672U - Tricalcium phosphate liposome preparation rotary evaporation device - Google Patents
Tricalcium phosphate liposome preparation rotary evaporation device Download PDFInfo
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- CN219251672U CN219251672U CN202223134975.2U CN202223134975U CN219251672U CN 219251672 U CN219251672 U CN 219251672U CN 202223134975 U CN202223134975 U CN 202223134975U CN 219251672 U CN219251672 U CN 219251672U
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
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Abstract
The utility model provides a rotary evaporation device for preparing tricalcium phosphate liposome, which comprises a box body, wherein a heating chamber is arranged in the box body, an evaporation bottle is arranged in the heating chamber, a first liquid guide interface is arranged on one side of the bottom of the heating chamber, the first liquid guide interface is connected with a heat conducting liquid storage tank, a second liquid guide interface is arranged on the other side of the heating chamber, and the second liquid guide interface is connected with a cooling liquid storage tank. According to the utility model, the heat conduction liquid stored in the heating chamber is pumped into the heat conduction liquid storage tank for storage, and the cooling liquid stored in the cooling liquid storage tank is led into the heating chamber, so that the materials in the evaporation bottle are rapidly cooled, after the cooling is finished, the cooling liquid is pumped into the cooling liquid storage tank again by the second liquid pump for storage, and the heat conduction liquid stored in the heat conduction liquid storage tank is led into the heating chamber again, so that the next heating evaporation operation is facilitated.
Description
Technical Field
The utility model relates to the technical field of rotary evaporation devices, in particular to a rotary evaporation device for preparing tricalcium phosphate liposome.
Background
In the preparation process of the superfine tricalcium phosphate liposome, an evaporation device is needed, lipid and fat-soluble substances to be encapsulated such as phospholipid, cholesterol and the like are dissolved in an organic solvent, and then the solution is placed in a round bottom flask and is dried by rotary evaporation under reduced pressure. For example, application number CN202220959646.2 discloses a rotatory evaporation plant of superfine tricalcium phosphate liposome preparation, relates to tricalcium phosphate production technical field, including the preparation casing, the front rotation of preparation casing is connected with the dodge gate, the right side fixed mounting of preparation casing has the controller body, be provided with continuous feed mechanism in the inner chamber of preparation casing, the top of preparation casing is provided with abundant condensing mechanism, continuous feed mechanism includes the water bath heating cabinet body. But the device is in the material discharge back, need by the material cooling by oneself or in addition through cooling device cooling to the material, make material finished product time longer.
Disclosure of Invention
In order to solve the problems, the utility model provides a tricalcium phosphate liposome preparation rotary evaporation device, so as to solve the problems more exactly.
The utility model is realized by the following technical scheme:
the utility model provides a tricalcium phosphate liposome preparation rotary evaporation device, which comprises a box body, wherein a heating chamber is arranged in the box body, an evaporation bottle is arranged in the heating chamber, the top of the evaporation bottle is connected with a liquid inlet pipe, the upper end of the liquid inlet pipe is connected with a feed adapter fixed on the top of the box body, the bottom of the heating chamber is provided with a discharge adapter, the bottom of the evaporation bottle is connected with a liquid discharge pipe and the discharge adapter is connected with a discharge electric control valve, the outer side of the middle part of the heating chamber is provided with an electric heating plate, one side of the bottom of the heating chamber is provided with a first liquid guide interface, the outer port of the first liquid guide interface is connected with a first electric control liquid valve, the other end of the first electric control liquid valve is connected with a first liquid pump, the inner side of the box body and the same side of the first liquid pump is provided with a heat conducting liquid storage tank, the bottom of the heat conducting liquid storage tank is provided with an interface connected with the first liquid pump, one side of the heating chamber far from the first liquid guide interface is provided with a second liquid guide interface, the outer port of the second liquid guide interface is connected with a second electric control liquid valve, the other end of the second electric control valve is connected with a second liquid pump, and the other side of the cooling tank is connected with the cooling tank bottom is provided with the second liquid storage tank.
Further, a driven gear is arranged in the middle of a liquid inlet pipe connected with the top of the evaporation bottle, a motor is arranged on one side of the top of the inner cavity of the box body, a driving gear is arranged on an output shaft of the motor, and the driven gear and the driving gear are in transmission through a toothed belt.
Further, the outside parcel of heat conduction liquid holding vessel is provided with heat preservation cotton, and heat preservation cotton hugs closely the outer wall setting of heat conduction liquid holding vessel.
Further, a heat exchange tube is arranged in the cooling liquid storage tank, an air cooling supply device is arranged on one side, close to the cooling liquid storage tank, of the outer portion of the tank body, an air supply end of the air cooling supply device is connected with an air inlet end of the heat exchange tube, and an air exhaust tube opening of the heat exchange tube extends to the outer portion of the tank body.
Further, the heat exchange tube is arranged in the cooling liquid storage tank in a spirally coiled mode.
Further, the outer wall of the cooling liquid storage tank is provided with radiating fins, the rear side wall of the box body is provided with a radiating fan at a position corresponding to the cooling liquid storage tank, and the front side of the box body is provided with a radiating grid at a position corresponding to the radiating fan.
The utility model has the beneficial effects that:
1. according to the utility model, the first electric control liquid valve is controlled to be opened, the heat conduction liquid stored in the heating chamber is pumped into the heat conduction liquid storage tank for storage under the operation of the first liquid pump, the second electric control liquid valve is controlled to be opened, and the cooling liquid stored in the cooling liquid storage tank is led into the heating chamber under the operation of the second liquid pump, so that the materials in the evaporation bottle are rapidly cooled, after the cooling is finished, the cooling liquid is pumped into the cooling liquid storage tank again by the second liquid pump for storage, and the heat conduction liquid stored in the heat conduction liquid storage tank is led into the heating chamber again, so that the next heating evaporation operation is facilitated;
2. according to the cooling device, cooling gas is led into the heat exchange tube under the operation of the air cooling supply equipment, so that cooling liquid subjected to heat exchange inside the cooling liquid storage tank is cooled, the cooling liquid is convenient to cool for the next time, the outer wall of the cooling liquid storage tank is provided with the radiating fins, the rear side wall of the box body is provided with the radiating fan at a position corresponding to the cooling liquid storage tank, and the front side of the box body is provided with the radiating grid at a position corresponding to the radiating fan, so that cooling of the cooling liquid stored inside the cooling liquid storage tank is assisted.
Drawings
FIG. 1 is a perspective view in half cross section of the present utility model;
FIG. 2 is a front view of the structure of the present utility model;
FIG. 3 is a schematic view of the first three-dimensional structure of the present utility model;
fig. 4 is a schematic overall view of a second perspective structure of the present utility model.
In the figure: 1. a case; 2. a heating chamber; 201. a first liquid-guiding interface; 2011. a first electrically controlled liquid valve; 2012. a first liquid pump; 202. a second liquid-guiding interface; 2021. a second electrically controlled liquid valve; 2022. a second liquid pump; 203. an electric heating plate; 3. an evaporation bottle; 301. a discharging adapter; 302. a discharging electric control valve; 303. a feed adapter; 304. a driven gear; 305. a motor; 306. a drive gear; 307. toothed belts; 4. a heat transfer fluid storage tank; 401. thermal insulation cotton; 5. a cooling liquid storage tank; 501. a heat exchange tube; 5011. an exhaust pipe orifice; 502. an air-cooled supply device; 503. a heat radiation fin; 504. a heat radiation fan; 505. and a heat radiation grille.
Detailed Description
In order to more clearly and completely describe the technical scheme of the utility model, the utility model is further described below with reference to the accompanying drawings.
Referring to fig. 1-4, the utility model provides a rotary evaporation device for preparing tricalcium phosphate liposome, which comprises a box body 1, a heating chamber 2 is arranged in the box body 1, an evaporation bottle 3 is arranged in the heating chamber 2, the top of the evaporation bottle 3 is connected with a liquid inlet pipe, the upper end of the liquid inlet pipe is connected with a feed adapter 303 fixed at the top of the box body 1, materials can be added into the evaporation bottle 3 along the feed adapter 303, a discharge adapter 301 is arranged at the bottom of the heating chamber 2, a liquid discharge pipe is connected with the bottom of the evaporation bottle 3 and is connected with the discharge adapter 301, a discharge electric control valve 302 is arranged at the bottom of the discharge adapter 301, the discharge electric control valve 302 is used for controlling the discharge of the materials, an electric heating plate 203 is arranged at the outer side of the middle part of the heating chamber 2, heat conduction liquid is stored in the heating chamber 2, a driven gear 304 is arranged in the middle of the liquid inlet pipe connected with the top of the evaporation bottle 3, a motor 305 is arranged at one side of the top of the inner cavity of the box body 1, a driving gear 306 is arranged on the output shaft of the motor 305, a driving gear 304 and the driven gear 306 is driven by a toothed belt 307, the driven gear 304 and the driving gear 306 is driven by a toothed belt 307, the driving gear 307 is driven by the driving gear 307, the driving gear 306 under the working of the motor 305, the driving gear 307 and the driven gear 307 is driven by the toothed belt, the driving gear 3 and the driving belt, the rotation is guaranteed, the rotation and the rotation of the evaporation bottle 3 is guaranteed, and the rotary evaporation efficiency is guaranteed, and the storage efficiency is guaranteed.
The bottom one side of heating chamber 2 is equipped with first drain interface 201, the outer port of first drain interface 201 is connected with first automatically controlled liquid valve 2011, the other end of first automatically controlled liquid valve 2011 is connected with first liquid pump 2012, inside and with first liquid pump 2012 homonymy are equipped with heat conduction liquid holding vessel 4, and heat conduction liquid holding vessel 4 bottom is equipped with the interface and is connected with first liquid pump 2012, after finishing evaporation to evaporation bottle 3 inside material, control first automatically controlled liquid valve 2011 and open, and under the work of first liquid pump 2012, the heat conduction liquid with heating chamber 2 internal storage is extracted to heat conduction liquid holding vessel 4 internal storage, the outside parcel of heat conduction liquid holding vessel 4 is provided with heat preservation cotton 401, heat preservation cotton 401 hugs closely the outer wall setting of heat conduction liquid holding vessel 4, heat conduction liquid to heat conduction liquid holding vessel 4 internal storage keeps warm.
The heating chamber 2 is equipped with second drain interface 202 far away from one side of first drain interface 201, the outer port of second drain interface 202 is connected with second automatically controlled liquid valve 2021, the other end of second automatically controlled liquid valve 2021 is connected with second liquid pump 2022, inside and be equipped with coolant liquid holding vessel 5 with second liquid pump 2022 homonymy, and coolant liquid holding vessel 5 bottom is equipped with the interface and is connected with second liquid pump 2022, after the evaporation to evaporation bottle 3 inside material finishes, open through controlling second automatically controlled liquid valve 2021, and the cooling liquid that will cool liquid holding vessel 5 inside store is imported into heating chamber 2 inside under the work of second liquid pump 2022, thereby carry out rapid cooling to evaporation bottle 3 inside material, after the cooling finishes, the heat conduction liquid that is stored in the inside heat conduction liquid holding vessel 4 is reintroduced into heating chamber 2 with the cooling liquid extraction, the operation of entering next heating evaporation is convenient.
The cooling liquid storage tank 5 is internally provided with the heat exchange tube 501, one side, close to the cooling liquid storage tank 5, of the outer part of the box body 1 is provided with the air cooling supply device 502, the air supply end of the air cooling supply device 502 is connected with the air inlet end of the heat exchange tube 501, the air exhaust pipe orifice 5011 of the heat exchange tube 501 extends to the outer part of the box body 1, the pipe part, located inside the cooling liquid storage tank 5, of the heat exchange tube 501 is spirally wound, cooling gas is led into the heat exchange tube 501 under the operation of the air cooling supply device 502, cooling liquid after heat exchange inside the cooling liquid storage tank 5 is cooled, the cooling liquid is convenient to cool down, the outer wall of the cooling liquid storage tank 5 is provided with the cooling fins 503, the rear side wall of the box body 1 is provided with the cooling fan 504 corresponding to the position of the cooling liquid storage tank 5, the front side of the box body 1 is provided with the cooling grid 505 corresponding to the position of the cooling fan 504, and cooling of the cooling liquid stored inside the cooling liquid storage tank 5 is assisted.
Working principle: according to the utility model, materials are added into the evaporation bottle 3 along the feeding adapter 303, and under the operation of the motor 305, the driven gear 304 and the driving gear 306 are driven by the toothed belt 307, so that the evaporation bottle 3 is driven to rotate, the materials stored in the evaporation bottle 3 are centrifugally rotated, the uniform heating is ensured, and the evaporation efficiency is improved;
according to the utility model, after evaporation of materials in the evaporation bottle 3 is finished, the first electric control liquid valve 2011 is controlled to be opened, under the working of the first liquid pump 2012, heat conduction liquid stored in the heating chamber 2 is pumped into the heat conduction liquid storage tank 4 for storage, the second electric control liquid valve 2021 is controlled to be opened, and under the working of the second liquid pump 2022, cooling liquid stored in the cooling liquid storage tank 5 is led into the heating chamber 2, so that the materials in the evaporation bottle 3 are rapidly cooled, after the cooling is finished, the cooling liquid is pumped into the cooling liquid storage tank 5 again by the second liquid pump 2022, and the heat conduction liquid stored in the heat conduction liquid storage tank 4 is led into the heating chamber 2 again, so that the next heating evaporation operation is facilitated;
according to the utility model, cooling gas is introduced into the heat exchange tube 501 under the operation of the air cooling supply equipment 502, so that cooling liquid subjected to heat exchange inside the cooling liquid storage tank 5 is cooled, the cooling liquid is convenient to cool for the next time, the outer wall of the cooling liquid storage tank 5 is provided with the cooling fins 503, the rear side wall of the box body 1 is provided with the cooling fan 504 corresponding to the cooling liquid storage tank 5, and the front side of the box body 1 is provided with the cooling grid 505 corresponding to the cooling fan 504, so that cooling of cooling liquid stored inside the cooling liquid storage tank 5 is assisted.
Of course, the present utility model can be implemented in various other embodiments, and based on this embodiment, those skilled in the art can obtain other embodiments without any inventive effort, which fall within the scope of the present utility model.
Claims (6)
1. The utility model provides a tricalcium phosphate liposome preparation rotary evaporation device, which comprises a box body (1), a serial communication port, box (1) inside is equipped with heating chamber (2), heating chamber (2) inside is equipped with evaporation bottle (3), evaporation bottle (3) top is connected with the feed liquor pipe, feed liquor pipe upper end is switched with feed adapter (303) that are fixed in box (1) top, heating chamber (2) bottom is equipped with row material adapter (301), and evaporation bottle (3) bottom is connected with the feed liquor pipe and arranges material adapter (301) and switches mutually, row material adapter (301) bottom is equipped with row material automatically controlled valve (302), the middle part outside of heating chamber (2) is provided with electrical heating plate (203), bottom one side of heating chamber (2) is equipped with first drain interface (201), the outer port of first drain interface (201) is connected with first automatically controlled liquid valve (2011), the other end of first automatically controlled liquid valve (2011) is connected with first liquid pump (2012), box (1) inside and with first liquid pump (2012) homonymy be equipped with drain pipe and row material adapter (301) and switch, drain material electrical control valve (202) are equipped with heat conduction liquid interface (202), second drain interface (202) are kept away from first drain interface (2012), second drain interface (202) are equipped with first drain interface (201), the other end of the second electric control liquid valve (2021) is connected with a second liquid pump (2022), a cooling liquid storage tank (5) is arranged inside the box body (1) and on the same side as the second liquid pump (2022), and an interface is arranged at the bottom of the cooling liquid storage tank (5) and is connected with the second liquid pump (2022).
2. The rotary evaporation device for preparing tricalcium phosphate liposome according to claim 1, wherein a driven gear (304) is arranged in the middle of a liquid inlet pipe connected with the top of the evaporation bottle (3), a motor (305) is arranged on one side of the top of the inner cavity of the box body (1), a driving gear (306) is arranged on an output shaft of the motor (305), and the driven gear (304) and the driving gear (306) are in transmission through a toothed belt (307).
3. The rotary evaporation device for preparing tricalcium phosphate liposome according to claim 1, wherein the heat-conducting liquid storage tank (4) is provided with heat-insulating cotton (401) in a wrapping manner, and the heat-insulating cotton (401) is closely attached to the outer wall of the heat-conducting liquid storage tank (4).
4. The rotary evaporation device for preparing tricalcium phosphate liposome according to claim 1, wherein a heat exchange tube (501) is arranged inside the cooling liquid storage tank (5), an air cooling supply device (502) is arranged on one side, close to the cooling liquid storage tank (5), of the outside of the box body (1), an air supply end of the air cooling supply device (502) is connected with an air inlet end of the heat exchange tube (501), and an air exhaust tube opening (5011) of the heat exchange tube (501) extends to the outside of the box body (1).
5. The rotary evaporation device for preparing tricalcium phosphate liposome as claimed in claim 4, wherein the heat exchange tube (501) is disposed in a spiral coil shape at a tube portion inside the cooling liquid storage tank (5).
6. The rotary evaporation device for preparing tricalcium phosphate liposome as claimed in claim 4, wherein the outer wall of the cooling liquid storage tank (5) is provided with a heat dissipation fin (503), the rear side wall of the box body (1) is provided with a heat dissipation fan (504) corresponding to the cooling liquid storage tank (5), and the front side of the box body (1) is provided with a heat dissipation grid (505) corresponding to the heat dissipation fan (504).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202223134975.2U CN219251672U (en) | 2022-11-24 | 2022-11-24 | Tricalcium phosphate liposome preparation rotary evaporation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202223134975.2U CN219251672U (en) | 2022-11-24 | 2022-11-24 | Tricalcium phosphate liposome preparation rotary evaporation device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219251672U true CN219251672U (en) | 2023-06-27 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202223134975.2U Active CN219251672U (en) | 2022-11-24 | 2022-11-24 | Tricalcium phosphate liposome preparation rotary evaporation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219251672U (en) |
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2022
- 2022-11-24 CN CN202223134975.2U patent/CN219251672U/en active Active
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