CN218637349U - Methyl octabromoether synthesizer - Google Patents
Methyl octabromoether synthesizer Download PDFInfo
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- CN218637349U CN218637349U CN202222131445.6U CN202222131445U CN218637349U CN 218637349 U CN218637349 U CN 218637349U CN 202222131445 U CN202222131445 U CN 202222131445U CN 218637349 U CN218637349 U CN 218637349U
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- heat
- conducting plate
- reation kettle
- conducting
- gear
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- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 title claims abstract description 19
- 238000006243 chemical reaction Methods 0.000 claims description 25
- 230000015572 biosynthetic process Effects 0.000 claims description 14
- 238000003786 synthesis reaction Methods 0.000 claims description 14
- 230000005540 biological transmission Effects 0.000 claims description 13
- 239000002184 metal Substances 0.000 claims description 5
- 238000010030 laminating Methods 0.000 claims description 2
- 239000000463 material Substances 0.000 abstract description 15
- 229930188012 Bromoether Natural products 0.000 abstract description 4
- HJCMMOODWZOXML-UHFFFAOYSA-N bromo hypobromite Chemical compound BrOBr HJCMMOODWZOXML-UHFFFAOYSA-N 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 238000003756 stirring Methods 0.000 abstract description 4
- 238000009833 condensation Methods 0.000 abstract description 3
- 230000005494 condensation Effects 0.000 abstract description 3
- 239000007769 metal material Substances 0.000 abstract description 3
- 238000009434 installation Methods 0.000 abstract 3
- 238000003780 insertion Methods 0.000 description 6
- 230000037431 insertion Effects 0.000 description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 2
- 229910052794 bromium Inorganic materials 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 239000003063 flame retardant Substances 0.000 description 2
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 210000001503 joint Anatomy 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000000979 retarding effect Effects 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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Abstract
The utility model relates to a synthesizer technical field discloses a methyl eight bromo ether synthesizer, and it includes the base, be provided with reation kettle on the base, and the reation kettle upper end sets up to the feed inlet to reation kettle's lower extreme installs the discharge gate, reation kettle is provided with the swing pinion with the junction of feed inlet, and the side of swing pinion is connected with drive gear, reation kettle's side is provided with first heat-conducting plate, second heat-conducting plate, third heat-conducting plate and fourth heat-conducting plate respectively. The utility model discloses the swing pinion with bearing connection between reation kettle and the feed inlet, the drive gear who can cooperate installation on the motor rotates the swing pinion, and then can rotate through the drive shaft of installation on the rotatory swing pinion drives the connecting rod, and the blade of the metal material of installation in the drive shaft can evenly stir when synthetic, carries out the breakage through the blade to the material after the condensation, realizes quick production.
Description
Technical Field
The utility model relates to a synthesizer technical field specifically is a methyl eight bromo ether synthesizer.
Background
The octabromomethyl ether is octabromoether with methyl component, and the octabromoether is white powder, low in toxicity, soluble in benzene, acetone, chloroform, etc., insoluble in water and hexanol, and has decomposition temperature higher than 285 deg.c, and excellent fire retarding effect. The octabromoether is used as an additive flame retardant, is a high-efficiency flame retardant containing aromatic bromine and aliphatic bromine, and has excellent thermal stability and light stability; the methyl octabromo ether needs to be subjected to synthetic treatment when being produced.
The existing synthesis device for methyl octabromoether can only carry out integral heating treatment on equipment when in use, cannot be replaced by cooling, and causes overlong standing time of the produced methyl octabromoether and reduction of production efficiency, so that the methyl octabromoether synthesis device needs to be provided for flexibly heating and cooling a reaction kettle.
Disclosure of Invention
An object of the utility model is to provide a methyl eight bromo ether synthesizer to solve the problem that proposes among the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme:
the utility model provides a methyl eight bromo ether synthesizer, its includes the base, be provided with reation kettle on the base, and the reation kettle upper end sets up to the feed inlet to reation kettle's lower extreme installs the discharge gate, reation kettle is provided with the rotary gear with the junction of feed inlet, and the side of rotary gear is connected with drive gear to install the motor on the drive gear, reation kettle's side is provided with first heat-conducting plate, second heat-conducting plate, third heat-conducting plate and fourth heat-conducting plate respectively, and installs the heater on the first heat-conducting plate, and is connected with the refrigerator on the second heat-conducting plate, install spacing track on the base, and spacing orbital side is connected with the rack, be provided with link block on the spacing track, and link block's lower extreme installs CD-ROM drive motor, install drive gear on CD-ROM drive motor's the output, the defeated material mouth is installed to the lower extreme of base.
Preferably, the upper end and the lower end of the rotating gear are provided with bearings which are respectively connected with the reaction kettle and the feed inlet, the rotating gear is in meshed connection with the transmission gear, and the transmission gear is connected with the output end of the motor.
Preferably, a connecting rod is connected in the rotating gear, a driving shaft is mounted on the connecting rod, and a blade is connected to the outer wall of the driving shaft, and the blade is made of metal.
Preferably, the outer side of the first heat-conducting plate is provided with a heat-insulating layer, the structures and the shapes of the first heat-conducting plate, the second heat-conducting plate, the third heat-conducting plate and the fourth heat-conducting plate are the same, the two sides of the third heat-conducting plate are respectively provided with a temperature-conducting inserted bar and a temperature-conducting slot, and the temperature-conducting inserted bar and the temperature-conducting slot are of a mutually-nested structure.
Preferably, first heat-conducting plate, second heat-conducting plate, third heat-conducting plate and fourth heat-conducting plate all are connected for the laminating with reation kettle's outer wall, and the equal welded mounting of the lower extreme of first heat-conducting plate, second heat-conducting plate, third heat-conducting plate and fourth heat-conducting plate has the connection slider.
Preferably, the connecting sliding block is in nested sliding connection with the limiting track, and the limiting track and the rack are designed integrally.
Preferably, the driving motor is fixed with the connecting slide block, the driving gear is connected with the output end of the driving motor, and the driving gear is meshed with the rack.
Compared with the prior art, the beneficial effects of the utility model are that:
1. the rotary gear connected with the bearing between the reaction kettle and the feed inlet can be matched with a driving transmission gear arranged on a motor to rotate the rotary gear, so that a driving shaft arranged on a connecting rod can be driven to rotate through the rotating rotary gear, a blade made of metal and arranged on the driving shaft can be uniformly stirred during synthesis, and the material is crushed through the blade after condensation, so that rapid production is realized;
2. the utility model discloses the structure with first heat-conducting plate, second heat-conducting plate, third heat-conducting plate and fourth heat-conducting plate is the same with the shape, can realize leading the heat conduction of temperature through the heat preservation that its outside has to heat and cool down first heat-conducting plate and second heat-conducting plate respectively through heater and refrigerator, and realize the quick replacement and the adjustment of synthetic temperature, the reation kettle's of being convenient for synthetic efficiency.
Drawings
Fig. 1 is a first view of the overall structure of the present invention;
fig. 2 is a second view of the overall structure of the present invention;
fig. 3 is a schematic view of a first heat-conducting plate mounting structure of the present invention;
fig. 4 is a schematic view of the structure of the limit track of the present invention;
fig. 5 is a schematic diagram of the structure in the reaction kettle of the present invention.
In the figure: 1. a base; 2. a reaction kettle; 3. a feed inlet; 4. a discharge port; 5. a rotating gear; 51. a connecting rod; 52. a drive shaft; 53. a blade; 6. a transmission gear; 7. a motor; 8. a first heat-conducting plate; 9. a second heat-conducting plate; 10. a heater; 11. a refrigerator; 12. a third heat-conducting plate; 121. a temperature-conducting inserted rod; 122. a heat conducting slot; 13. a fourth heat-conducting plate; 14. a limiting track; 15. a rack; 16. connecting the sliding block; 17. a drive motor; 18. a drive gear; 19. and a material conveying port.
Detailed Description
Referring to fig. 1-5, the present invention provides an embodiment:
a methyl octabromoether synthesizer comprises a base 1, wherein a reaction kettle 2 is arranged on the base 1, a feed inlet 3 is formed in the upper end of the reaction kettle 2, a discharge outlet 4 is formed in the lower end of the reaction kettle 2, a rotary gear 5 is arranged at the joint of the reaction kettle 2 and the feed inlet 3, a transmission gear 6 is connected to the side edge of the rotary gear 5, a motor 7 is mounted on the transmission gear 6, a first heat conduction plate 8, a second heat conduction plate 9, a third heat conduction plate 12 and a fourth heat conduction plate 13 are respectively arranged on the side edge of the reaction kettle 2, a heater 10 is mounted on the first heat conduction plate 8, a refrigerator 11 is connected to the second heat conduction plate 9, a limiting rail 14 is mounted on the base 1, a rack 15 is connected to the side edge of the limiting rail 14, a connecting sliding block 16 and the limiting rail 14 are in nested sliding connection, the limiting rail 14 and the rack 15 are integrally designed, the connecting sliding block 16 slides in the limiting rail 14, the first heat conduction plate 8 and the fourth heat conduction plate 13 (or the second heat conduction plate 9 and the third heat conduction plate 12) are pushed to be attached to the reaction kettle 2, a temperature guide insert rod 121 and a temperature guide 122 are butted to the reaction kettle 2, and a temperature guide groove is uniformly cooled (the stirring kettle 2) at the same time);
the limiting track 14 is provided with a connecting slide block 16, the lower end of the connecting slide block 16 is provided with a driving motor 17, the output end of the driving motor 17 is provided with a driving gear 18, the driving motor 17 is fixed with the connecting slide block 16, the driving gear 18 is connected with the output end of the driving motor 17, the driving gear 18 is meshed with the rack 15, the driving motor 17 drives the driving gear 18 to drive the rack 15, the connecting slide block 16 can be pushed to slide in the limiting track 14 in a limiting mode, the lower end of the base 1 is provided with a material conveying port 19, and the material discharging port 4 is opened to discharge materials through the material conveying port 19.
In one embodiment, bearings are arranged at the upper end and the lower end of the rotating gear 5 and are respectively connected with the reaction kettle 2 and the feed port 3, the rotating gear 5 is in meshed connection with the transmission gear 6, the transmission gear 6 is connected with the output end of the motor 7, and the rotating gear 5 in bearing connection between the reaction kettle 2 and the feed port 3 can be matched with the driving transmission gear 6 arranged on the motor 7 to drive the rotating gear 5;
in one embodiment, the connecting rod 51 is connected in the rotating gear 5, the driving shaft 52 is installed on the connecting rod 51, the blade 53 is connected to the outer wall of the driving shaft 52, the blade 53 is made of metal, the rotating gear 5 drives the driving shaft 52 installed on the connecting rod 51 to rotate, the blade 53 made of metal and installed on the driving shaft 52 can be uniformly stirred during synthesis, and materials are crushed through the blade 53 after condensation, so that rapid production is realized;
in one embodiment, a heat insulation layer is arranged on the outer side of the first heat conduction plate 8, the structures and the shapes of the first heat conduction plate 8, the second heat conduction plate 9, the third heat conduction plate 12 and the fourth heat conduction plate 13 are the same, heat conduction through heat insulation layers arranged outside the first heat conduction plate 8, the second heat conduction plate 9, the third heat conduction plate 12 and the fourth heat conduction plate 13 can be achieved, the first heat conduction plate 8 and the second heat conduction plate 9 are heated and cooled through the heater 10 and the refrigerator 11 respectively, the synthesis temperature can be rapidly changed and adjusted, the synthesis efficiency of the reaction kettle 2 is facilitated, the temperature guide insertion rods 121 and the temperature guide insertion grooves 122 are arranged on two sides of the third heat conduction plate 12 respectively, the temperature guide insertion rods 121 and the temperature guide insertion grooves 122 are in a mutually nested structure, and the temperature guide insertion rods 121 and the temperature guide insertion grooves 122 are in butt joint;
in one embodiment, the first heat-conducting plate 8, the second heat-conducting plate 9, the third heat-conducting plate 12 and the fourth heat-conducting plate 13 are all in fit connection with the outer wall of the reaction kettle 2, and the lower ends of the first heat-conducting plate 8, the second heat-conducting plate 9, the third heat-conducting plate 12 and the fourth heat-conducting plate 13 are all welded with connecting sliders 16, so that the positions of the first heat-conducting plate 8, the second heat-conducting plate 9, the third heat-conducting plate 12 and the fourth heat-conducting plate 13 can be stably adjusted for quick matching;
the utility model discloses a theory of operation does: firstly, all materials are guided into a reaction kettle 2 through a feeding hole 3, a motor 7 is started to drive a transmission gear 6 to drive a rotating gear 5, the rotating gear 5 drives a driving shaft 52 arranged on a connecting rod 51 to rotate at the moment, a blade 53 made of metal materials is driven by the driving shaft 52 to rotate, and uniform stirring is carried out in the synthesis process;
when the reaction kettle 2 is heated, the driving motor 17 is started to drive the driving gear 18 to drive the rack 15, at the moment, the connecting slide block 16 slides in the limiting track 14 in a limiting way, the first heat conducting plate 8 and the fourth heat conducting plate 13 are pushed to be attached to the reaction kettle 2, meanwhile, the temperature conducting inserted rod 121 and the temperature conducting slot 122 are butted with each other to conduct temperature conducting treatment, and at the moment, the reaction kettle 2 is in a heating state, so that the uniform stirring in the process is realized;
when the cooling reaction kettle 2 cools the material rapidly, only the driving motor 17 needs to drive the driving gear 18 to drive the rack 15, at this time, the connecting sliding block 16 slides in the limiting track 14 in a limiting way and pushes the first heat conducting plate 8 and the fourth heat conducting plate 13 to be away from the reaction kettle 2, then the driving motor 17 drives the driving gear 18 to drive the rack 15, at this time, the connecting sliding block 16 slides in the limiting track 14 in a limiting way, the second heat conducting plate 9 and the third heat conducting plate 12 are attached to the reaction kettle 2, meanwhile, the temperature conducting inserted rod 121 and the temperature conducting inserted slot 122 are mutually butted for conducting temperature conducting treatment, at this time, the reaction kettle 2 is in a rapid cooling state, and the material is cooled;
the starting motor 7 drives the rotating gear 5 through the driving transmission gear 6 installed on the starting motor, the rotating gear 5 drives the driving shaft 52 installed on the connecting rod 51 to rotate, the blades 53 made of metal materials installed on the driving shaft 52 crush the condensed materials, and the discharging port 4 is opened to discharge the materials through the material conveying port 19.
Claims (7)
1. A methyl octabromoether synthesis device is characterized by comprising: base (1), be provided with reation kettle (2) on base (1), and reation kettle (2) upper end sets up to feed inlet (3) to discharge gate (4) are installed to the lower extreme of reation kettle (2), reation kettle (2) are provided with rotating gear (5) with the junction of feed inlet (3), and the side of rotating gear (5) is connected with drive gear (6) to install motor (7) on drive gear (6), the side of reation kettle (2) is provided with first heat-conducting plate (8), second heat-conducting plate (9), third heat-conducting plate (12) and fourth heat-conducting plate (13) respectively, and installs heater (10) on first heat-conducting plate (8) to be connected with refrigerator (11) on second heat-conducting plate (9), install spacing track (14) on base (1), and the side of spacing track (14) is connected with rack (15), be provided with link block (16) on spacing track (14), and link block (16)'s lower extreme installs driving motor (17), install on driving motor (17) output, install drive gear (18) lower extreme (19) of base (1).
2. The synthesis device of methyl octabromoether according to claim 1, wherein: the upper end and the lower end of the rotating gear (5) are provided with bearings which are respectively connected with the reaction kettle (2) and the feed inlet (3), the rotating gear (5) is meshed with the transmission gear (6), and the transmission gear (6) is connected with the output end of the motor (7).
3. The methyl octabromoether synthesis device according to claim 1, wherein: the rotating gear (5) is internally connected with a connecting rod (51), the connecting rod (51) is provided with a driving shaft (52), the outer wall of the driving shaft (52) is connected with a blade (53), and the blade (53) is made of metal.
4. The methyl octabromoether synthesis device according to claim 1, wherein: the heat-insulating layer is arranged on the outer side of the first heat-conducting plate (8), the structures and the shapes of the first heat-conducting plate (8), the second heat-conducting plate (9), the third heat-conducting plate (12) and the fourth heat-conducting plate (13) are the same, the two sides of the third heat-conducting plate (12) are respectively provided with a temperature-conducting inserted rod (121) and a temperature-conducting slot (122), and the temperature-conducting inserted rod (121) and the temperature-conducting slot (122) are of mutually-nested structures.
5. The synthesis device of methyl octabromoether according to claim 1, wherein: first heat-conducting plate (8), second heat-conducting plate (9), third heat-conducting plate (12) and fourth heat-conducting plate (13) all are connected for the laminating with the outer wall of reation kettle (2), and the equal welded mounting of lower extreme of first heat-conducting plate (8), second heat-conducting plate (9), third heat-conducting plate (12) and fourth heat-conducting plate (13) has connection slider (16).
6. The methyl octabromoether synthesis device according to claim 1, wherein: the connecting sliding block (16) is connected with the limiting track (14) in a nested sliding mode, and the limiting track (14) and the rack (15) are designed in an integrated mode.
7. The synthesis device of methyl octabromoether according to claim 1, wherein: the driving motor (17) is fixed with the connecting slide block (16), the driving gear (18) is connected with the output end of the driving motor (17), and the driving gear (18) is in meshed connection with the rack (15).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222131445.6U CN218637349U (en) | 2022-08-15 | 2022-08-15 | Methyl octabromoether synthesizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222131445.6U CN218637349U (en) | 2022-08-15 | 2022-08-15 | Methyl octabromoether synthesizer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218637349U true CN218637349U (en) | 2023-03-17 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202222131445.6U Active CN218637349U (en) | 2022-08-15 | 2022-08-15 | Methyl octabromoether synthesizer |
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| CN (1) | CN218637349U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117299039A (en) * | 2023-11-27 | 2023-12-29 | 山东东信新材料科技股份有限公司 | Methyl octabromoether fire retardant preparation facilities |
-
2022
- 2022-08-15 CN CN202222131445.6U patent/CN218637349U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117299039A (en) * | 2023-11-27 | 2023-12-29 | 山东东信新材料科技股份有限公司 | Methyl octabromoether fire retardant preparation facilities |
| CN117299039B (en) * | 2023-11-27 | 2024-02-06 | 山东东信新材料科技股份有限公司 | Methyl octabromoether fire retardant preparation facilities |
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