CN218608085U - High-efficient solvent recovery distillation plant - Google Patents

High-efficient solvent recovery distillation plant Download PDF

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Publication number
CN218608085U
CN218608085U CN202221993984.4U CN202221993984U CN218608085U CN 218608085 U CN218608085 U CN 218608085U CN 202221993984 U CN202221993984 U CN 202221993984U CN 218608085 U CN218608085 U CN 218608085U
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fixedly connected
distillation
box
cooling
pipe
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CN202221993984.4U
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肖贺廷
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Ptg Advanced Catalyst Co ltd
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Ptg Advanced Catalyst Co ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/10Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working

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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model discloses a high-efficient solvent recovery distillation plant, which comprises a supporting table, brace table's top fixedly connected with distillation retort, electromagnetic heater is all installed to the inside both sides of distillation retort, the bottom of distillation retort is run through and is equipped with the first row of material pipe rather than fixed connection, the top of distillation retort is run through and is equipped with rather than fixed connection's gas conveying pipe, brace table's top fixedly connected with cooling box, the bottom of cooling box is run through and is equipped with the second row of material pipe rather than fixed connection, be equipped with rabbling mechanism in the distillation retort, be equipped with cooling mechanism between cooling box and the storage box. The utility model can stir the solvent through the stirring mechanism, and can stir the solvents with different heights, and the solvent is heated uniformly; can cool off the liquefaction to steam through cooling body, and the area of contact that can increase air conditioning and steam through the spiral setting of cooling tube, it is effectual to the steam liquefaction.

Description

High-efficient solvent recovery distillation plant
Technical Field
The utility model relates to a distillation technical field especially relates to a high-efficient solvent recovery distillation plant.
Background
The prior art discloses a distillation solvent device is retrieved to high efficiency that application number is CN201821225253.9, comprising a base plate, the bottom plate top sets up the distillation case, electromagnetic heater is all installed to the inside both sides of distillation case, one side of distillation case is provided with the cooler bin, the distillation case top is provided with first air duct, and the end of first air duct runs through to the inside bottom of cooler bin, one side that the distillation case was kept away from to the cooler bin is provided with the bin, the air pump is installed at the top of bin, the end of bleeding of air pump is provided with the third air duct that runs through to the bin inside, the end of giving vent to anger of air pump is provided with the second air duct, the end of second air duct runs through to the inside top of cooler bin.
In the patent, the solvent can be heated by the electromagnetic heater, but the solvent far away from the electromagnetic heater needs to be heated for a long time, so that the solvent is heated unevenly, and the heating and distillation effects are poor; in cooling, cold air is introduced into the cooling box to cool the steam, but introduction of cold air into the cooling box increases the air pressure in the cooling box, which is likely to cause danger.
In order to solve the above problems, the present application provides an efficient solvent recovery distillation apparatus.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the defects in the prior art, and provides a high-efficiency solvent recovery distillation device which can stir the solvent through a stirring mechanism and can stir the solvents with different heights, and the solvent is heated uniformly; can cool off the liquefaction to steam through cooling body, and the spiral through the cooling tube sets up the area of contact that can increase air conditioning and steam, and is effectual to the steam liquefaction.
In order to realize the purpose, the utility model adopts the following technical scheme:
the utility model provides a high-efficient solvent recovery distillation plant, includes a supporting bench, the top fixedly connected with distillation retort of brace table, electromagnetic heater is all installed to the inside both sides of distillation retort, the top of distillation retort is run through and is equipped with rather than fixed connection's feeder hopper, the bottom of distillation retort is run through and is equipped with rather than fixed connection's first row of material pipe, first row of material pipe runs through the brace table and rather than fixed connection, the top of distillation retort is run through and is equipped with rather than fixed connection's gas delivery pipe, brace table's top fixedly connected with cooling box, gas delivery pipe runs through the cooling box and rather than fixed connection, the material pipe is arranged to the second that is equipped with rather than fixed connection to the bottom of cooling box, the material pipe is arranged to the second runs through brace table and rather than fixed connection, brace table's top fixedly connected with storage box, be equipped with rabbling mechanism in the distillation retort, rabbling mechanism includes the motor with the bottom fixed connection of brace table, the output fixedly connected with telescopic link of motor, the telescopic link runs through brace table and distillation box and rather than rotating connection, the top fixedly connected with reciprocating lead screw, the reciprocating screw of reciprocating connection of reciprocating screw, the outer wall of reciprocating screw is equipped with a plurality of cooling box and cooling rod between the outer wall mechanism.
Preferably, rabbling mechanism include with the bottom fixed connection's of brace table motor, the output fixedly connected with telescopic link of motor, the telescopic link runs through brace table and distillation box and is connected rather than rotating, the reciprocal lead screw of top fixedly connected with of telescopic link, the outer wall cover of reciprocal lead screw is equipped with the fixed plate, the inner wall fixed connection of fixed plate and distillation box, the top fixedly connected with rotary rod of reciprocal lead screw, a plurality of puddlers of outer wall fixedly connected with of rotary rod.
Preferably, the outer walls of the feed hopper, the first discharging pipe and the second discharging pipe are all provided with valves.
Preferably, a plurality of the stirring rods are equally spaced apart.
Preferably, a plurality of the stirring rods are equally spaced apart.
Preferably, the side wall of the storage tank is provided with a drain pipe fixedly connected with the storage tank in a penetrating way.
Compared with the prior art, the utility model, its beneficial effect does:
1. the output through the motor drives telescopic link, reciprocal lead screw, rotary rod and stirring rod and rotates, can stir the solvent through the stirring rod rotation, makes it be heated evenly, and reciprocates and can stir the solvent of co-altitude not through the limit rotation of stirring rod, and stirring effect is good, makes it be heated more evenly.
2. Steam enters into the cooler bin through gas delivery pipe and carries out cooling operation, start the fan in this process, effect through the fan can be with the air conditioning in the storage box through first connecting pipe, the second connecting pipe is injected into in the cooler bin, at last flow back to in the storage box through the third connecting pipe, the steam that produces through the air conditioning in the cooler bin can be liquefied, and the spiral setting through the cooler bin can increase the area of contact of steam and cold air, it is effectual to liquefy, cold air through the third connecting pipe backward flow once more with the ice-cube contact in the storage box guarantee the air become the cold air, guarantee subsequent liquefaction effect.
In conclusion, the solvent can be stirred by the stirring mechanism, and the solvents with different heights can be stirred, so that the solvent is heated uniformly; can cool off the liquefaction to steam through cooling body, and the spiral through the cooling tube sets up the area of contact that can increase air conditioning and steam, and is effectual to the steam liquefaction.
Drawings
FIG. 1 is a cross-sectional view of a high efficiency solvent recovery distillation apparatus according to the present invention;
fig. 2 is a front view of the high-efficiency solvent recovery distillation apparatus provided by the present invention.
In the figure: 1 supporting table, 2 distilling boxes, 3 electromagnetic heaters, 4 feed hoppers, 5 first discharging pipes, 6 gas conveying pipes, 7 cooling boxes, 8 second discharging pipes, 9 storage boxes, 10 motors, 11 telescopic rods, 12 reciprocating screw rods, 13 fixing plates, 14 rotating rods, 15 stirring rods, 16 first connecting pipes, 17 fans, 18 second connecting pipes, 19 cooling pipes and 20 third connecting pipes.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
Referring to fig. 1-2, a high-efficient solvent recovery distillation plant, including a supporting bench 1, the top fixedly connected with distillation box 2 of supporting bench 1, electromagnetic heater 3 is all installed to the inside both sides of distillation box 2, can heat the solvent through electromagnetic heater 3, thereby carry out the distillation operation to it, the top of distillation box 2 is run through and is equipped with feeder hopper 4 rather than fixed connection, pour into the solvent into through feeder hopper 4, the bottom of distillation box 2 is run through and is equipped with rather than fixed connection's first row of material pipe 5, first row of material pipe 5 runs through supporting bench 1 and distillation box 2 and rather than fixed connection, can retrieve the solvent after the distillation through first row of material pipe 5.
The top of distillation box 2 is run through and is equipped with rather than fixed connection's gas delivery pipe 6, prop up supporting bench 1's top fixedly connected with cooler bin 7, gas delivery pipe 6 runs through cooler bin 7 and rather than fixed connection, the bottom of cooler bin 7 is run through and is equipped with rather than fixed connection's second row material pipe 8, it can collect liquefied liquid to arrange material pipe 8 through the second, the feeder hopper 4, the valve is all installed to the outer wall that material pipe 8 was arranged to first row material pipe 5 and second, row material pipe 8 runs through supporting bench 1 and rather than fixed connection.
The top of the supporting table 1 is fixedly connected with a storage tank 9, ice cubes are stored in the storage tank 9, cold air is generated through the ice cubes and used for subsequent steam liquefaction, and a drain pipe fixedly connected with the storage tank 9 penetrates through the side wall of the storage tank 9 and can discharge water generated by melting of the ice cubes to the outside.
Be equipped with rabbling mechanism in the distillation case 2, the rabbling mechanism include with the bottom fixed connection's of brace table 1 motor 10, motor 10's output fixedly connected with telescopic link 11, telescopic link 11 runs through brace table 1 and distillation case 2 and is connected rather than rotating, the reciprocal lead screw 12 of top fixedly connected with of telescopic link 11, the outer wall cover of reciprocal lead screw 12 is equipped with fixed plate 13, fixed plate 13 and distillation case 2's inner wall fixed connection, the top fixedly connected with rotary rod 14 of reciprocal lead screw 12, a plurality of stirring rods 15 of the outer wall fixedly connected with of rotary rod 14, a plurality of stirring rods 15 are equidistant distribution, reciprocate through 15 limits of stirring rod rotation and can stir the solvent of co-altitude not, make it be heated evenly.
Be equipped with cooling body between cooler bin 7 and the storage box 9, cooling body is including running through storage box 9 and rather than fixed connection's first connecting pipe 16, first connecting pipe 16 fixedly connected with fan 17, fan 17 is installed on the lateral wall of cooler bin 7, fan 17 fixedly connected with second connecting pipe 18, second connecting pipe 18 runs through cooler bin 7 and rather than fixed connection, second connecting pipe 18 fixedly connected with cooling tube 19, cooling tube 19 is the heliciform setting, can increase the area of contact of cold air and steam, can make steam meet the cold liquefaction, cooling tube 19 fixedly connected with third connecting pipe 20, third connecting pipe 20 runs through cooler bin 7 and storage box 9 and rather than fixed connection, the cold air flows back in storage box 9 through third connecting pipe 20, cool off the air once more with the ice-cube contact, guarantee subsequent liquefaction effect.
The utility model discloses in, the staff opens the valve on the feeder hopper 4, inject the solvent into the distillation box 2 through the feeder hopper 4, close the valve on the feeder hopper 4, can heat the solvent in the distillation box 2 through the electromagnetic heater 3, start motor 10, drive telescopic link 11 through the output of motor 10, reciprocal lead screw 12, rotary rod 14 and stirring rod 15 rotate, can stir the solvent through the rotation of stirring rod 15, make it be heated evenly, can drive reciprocal lead screw 12 through the cooperation of reciprocal lead screw 12 and fixed plate 13, rotary rod 14, stirring rod 15 reciprocates while rotating (telescopic link 11 contracts or stretches out in this process), can stir the solvent of different heights through reciprocating while rotating of stirring rod 15, the stirring effect is good, make it be heated more evenly; can produce steam when heating the distillation, steam enters into cooling tank 7 through gas delivery pipe 6 and carries out cooling operation, start fan 17 in this process, can pass through first connecting pipe 16 with the air conditioning in the storage box 9 through fan 17's effect, second connecting pipe 18 pours into in the cooling tube 19 into, flow back into in the storage box 9 through third connecting pipe 20 at last, the steam that produces through the distillation can be liquefied to the air conditioning in the cooling tube 19, and the area of contact that can increase steam and cold air through the spiral setting of cooling tube 19, it is effectual to liquefy, cold air through third connecting pipe 20 backward flow contacts with the ice-cube in the storage box 9 once more and guarantees that the air becomes cold air, guarantee subsequent liquefaction effect, open the valve on first blow-off pipe 5 and the second blow-off pipe 8, can collect the distilled solvent in distillation tank 2, it can to discharge steam liquefied liquid through second blow-off pipe 8.

Claims (6)

1. The high-efficiency solvent recovery distillation device comprises a support table (1) and is characterized in that a distillation box (2) is fixedly connected to the top of the support table (1), electromagnetic heaters (3) are installed on two sides of the interior of the distillation box (2), a feed hopper (4) fixedly connected with the distillation box (2) penetrates through the top of the distillation box (2), a first discharging pipe (5) fixedly connected with the distillation box (2) penetrates through the bottom of the distillation box (2), the first discharging pipe (5) penetrates through the support table (1) and is fixedly connected with the support table, a gas conveying pipe (6) fixedly connected with the distillation box (2) penetrates through the top of the distillation box (2), a cooling box (7) is fixedly connected with the top of the support table (1), the gas conveying pipe (6) penetrates through the cooling box (7) and is fixedly connected with the cooling box, a second discharging pipe (8) fixedly connected with the cooling box (7) penetrates through the bottom of the cooling box (7), the second discharging pipe (8) penetrates through the support table (1) and is fixedly connected with the support table, a storage box (9) is fixedly connected with the top of the support table (1), a stirring mechanism is arranged in the distillation box (2), and a cooling mechanism is arranged between the cooling box (7) and the storage box (9);
rabbling mechanism include with motor (10) of the bottom fixed connection of brace table (1), the output fixedly connected with telescopic link (11) of motor (10), telescopic link (11) run through brace table (1) and distillation tank (2) and rotate rather than being connected, the reciprocal lead screw (12) of top fixedly connected with of telescopic link (11), the outer wall cover of reciprocal lead screw (12) is equipped with fixed plate (13), the inner wall fixed connection of fixed plate (13) and distillation tank (2), the top fixedly connected with rotary rod (14) of reciprocal lead screw (12), a plurality of stirring rod (15) of outer wall fixedly connected with of rotary rod (14).
2. A high efficiency solvent recovery distillation apparatus according to claim 1, wherein the cooling mechanism comprises a first connection pipe (16) passing through and fixedly connected to the storage tank (9), the first connection pipe (16) is fixedly connected to a fan (17), the fan (17) is installed on a side wall of the cooling tank (7), the fan (17) is fixedly connected to a second connection pipe (18), the second connection pipe (18) passes through and fixedly connected to the cooling tank (7), the second connection pipe (18) is fixedly connected to a cooling pipe (19), the cooling pipe (19) is fixedly connected to a third connection pipe (20), and the third connection pipe (20) passes through and is fixedly connected to the cooling tank (7) and the storage tank (9).
3. The high-efficiency solvent recovery distillation device as claimed in claim 1, wherein valves are mounted on the outer walls of the feed hopper (4), the first discharge pipe (5) and the second discharge pipe (8).
4. The apparatus according to claim 1, wherein the stirring rods (15) are equally spaced.
5. A high efficiency solvent recovery distillation apparatus according to claim 2, wherein said cooling tubes (19) are arranged in a spiral configuration.
6. A high efficiency solvent recovery distillation apparatus according to claim 1, wherein the side wall of the storage tank (9) is provided with a drain pipe fixedly connected thereto.
CN202221993984.4U 2022-07-29 2022-07-29 High-efficient solvent recovery distillation plant Active CN218608085U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202221993984.4U CN218608085U (en) 2022-07-29 2022-07-29 High-efficient solvent recovery distillation plant

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202221993984.4U CN218608085U (en) 2022-07-29 2022-07-29 High-efficient solvent recovery distillation plant

Publications (1)

Publication Number Publication Date
CN218608085U true CN218608085U (en) 2023-03-14

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CN202221993984.4U Active CN218608085U (en) 2022-07-29 2022-07-29 High-efficient solvent recovery distillation plant

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117797498A (en) * 2024-03-01 2024-04-02 连云港贵科药业有限公司 Reduced pressure distillation device for capecitabine intermediate

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117797498A (en) * 2024-03-01 2024-04-02 连云港贵科药业有限公司 Reduced pressure distillation device for capecitabine intermediate

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