CN218574988U

CN218574988U - Superfine palladium powder preparation device

Info

Publication number: CN218574988U
Application number: CN202221876492.7U
Authority: CN
Inventors: 陈新喜; 陈北海; 王宗华
Original assignee: Jiangxi Longtianong Nonferrous Metal Co ltd
Current assignee: Jiangxi Longtianong Nonferrous Metal Co ltd
Priority date: 2022-07-19
Filing date: 2022-07-19
Publication date: 2023-03-07
Anticipated expiration: 2032-07-19

Abstract

The utility model discloses an ultrafine palladium powder preparation facilities, the power distribution box comprises a box body, the box top is provided with the case lid, be provided with the motor case in the middle of the case lid top, the motor incasement is provided with the motor, the output of motor bottom is connected with the axis of rotation, axis of rotation outer wall symmetry equidistance is provided with the puddler, just the puddler is in the box, case lid bilateral symmetry is provided with the fixed plate, a fixed plate is provided with the gim peg with one side symmetry that the case lid carried on the back mutually, just the gim peg tail end runs through fixed plate and box threaded connection, case lid top left side intercommunication has the inlet pipe, through the heating pipe and carry out the circulation of cold water in the cavity, can be better heat up or cool down in the box to the temperature of solution in the better retaining box, and be convenient for carry out the dismouting between box and the case lid, thereby when taking out the palladium powder of the unreacted completion in filter screen top, be convenient for clear up the device.

Description

Superfine palladium powder preparation device

Technical Field

The utility model relates to a palladium powder preparation technical field particularly, relates to an ultra-fine palladium powder preparation facilities.

Background

The superfine palladium powder is an indispensable raw material for metal-doped conductive slurry and is also a synthetic raw material for various palladium compounds.

In the prior art, in the preparation process of the superfine palladium powder, the particle size of the obtained palladium powder is influenced without controlling the temperature, and if the palladium powder is completely reacted, the palladium powder is discharged, so that the waste of the palladium powder is caused.

An effective solution to the problems in the related art has not been proposed yet.

SUMMERY OF THE UTILITY MODEL

To the problem in the correlation technique, the utility model provides a superfine palladium powder preparation facilities to overcome the above-mentioned technical problem that current correlation technique exists.

Therefore, the utility model discloses a specific technical scheme as follows:

the utility model provides an ultrafine palladium powder preparation facilities, includes the box, the box top is provided with the case lid, be provided with the motor case in the middle of the case lid top, be provided with the motor in the motor case, the output of motor bottom is connected with the axis of rotation, axis of rotation outer wall symmetry equidistance is provided with the puddler, just the puddler is in the box, case lid bilateral symmetry is provided with the fixed plate, the fixed plate is provided with the gim peg with the bilateral symmetry of case lid back of the body, just the gim peg tail end runs through fixed plate and box threaded connection, case lid top left side intercommunication has the inlet pipe, be provided with first control valve on the inlet pipe, box left and right sides symmetry is provided with the mounting panel, the heating pipe has been inlayed to one side that the mounting panel was laminated with the box mutually, box inner chamber bottom surface symmetry is provided with the backup pad, the backup pad top is provided with the filter screen, filter screen top left side and right side all symmetry are provided with the montant, just montant top and case lid are laminated mutually, the bottom is provided with square board, the cavity has seted up in the square board, square board left and right sides symmetry is provided with the pipe, the pipe is linked together with the cavity, be provided with the third system collecting pipe on the pipe, square board bottom symmetry is provided with the bolt, the discharging pipe, the square board, the round hole is provided with the round hole in the middle of box, the round hole of control pipe.

Preferably, a transparent window is arranged on the front side of the box body.

Preferably, a gap is left between the rotating shaft and the vertical rod.

Preferably, a cross rod is arranged between the front vertical rod and the rear vertical rod, and the top of the cross rod is attached to the box cover.

Preferably, a gap is left between the filter screen and the rotating shaft.

Preferably, a gap is left between the square plate and the second control valve.

The utility model has the advantages that:

1. through the heating pipe and carry out the circulation of cold water in the cavity, can be better heat up or lower the temperature to in the box to the better temperature that keeps solution in the box, and be convenient for carry out the dismouting between box and the case lid, thereby when taking out the palladium powder of the unreacted completion in filter screen top, be convenient for clear up the device.

2. Through setting up the transparent window, be convenient for know the reaction condition of palladium powder in the box, through setting up the horizontal pole, be convenient for take out the filter screen.

Drawings

In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required to be used in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without creative efforts.

Fig. 1 is a schematic view of an overall structure of an apparatus for preparing palladium ultrafine powder according to an embodiment of the present invention;

fig. 2 is a schematic view of an internal structure of an apparatus for preparing palladium ultrafine powder according to an embodiment of the present invention;

FIG. 3 is a schematic view of the connection of the filter net of the apparatus for preparing palladium ultrafine powder according to the embodiment of the present invention;

fig. 4 is a schematic view of a square plate of an apparatus for preparing ultra-fine palladium powder according to an embodiment of the present invention.

In the figure:

1. a box body; 2. a box cover; 3. a motor case; 4. a motor; 5. a rotating shaft; 6. a stirring rod; 7. a fixing plate; 8. a fixing bolt; 9. a feed pipe; 10. a first control valve; 11. mounting a plate; 12. heating a tube; 13. a support plate; 14. a filter screen; 15. a vertical rod; 16. a square plate; 17. a chamber; 18. a conduit; 19. a third control valve; 20. a bolt; 21. a circular hole; 22. a discharge pipe; 23. a second control valve; 24. a transparent window; 25. a cross bar.

Detailed Description

For further explanation of the embodiments, the drawings are provided as part of the disclosure and serve primarily to illustrate the embodiments and, together with the description, to explain the principles of operation of the embodiments, and to provide further explanation of the invention and advantages thereof, it will be understood by those skilled in the art that various other embodiments and advantages of the invention are possible, and that elements in the drawings are not to scale and that like reference numerals are generally used to designate like elements.

According to the embodiment of the utility model, a superfine palladium powder preparation facilities is provided.

Example one

As shown in figures 1-4, the device for preparing ultrafine palladium powder according to the embodiment of the present invention comprises a box body 1, a box cover 2 is arranged on the top of the box body 1, a motor box 3 is arranged in the middle of the top of the box cover 2, a motor 4 is arranged in the motor box 3, the output end of the bottom of the motor 4 is connected with a rotating shaft 5, stirring rods 6 are symmetrically and equidistantly arranged on the outer wall of the rotating shaft 5, the stirring rod 6 is positioned in the box body 1, the two sides of the box cover 2 are symmetrically provided with fixing plates 7, one side of each fixing plate 7, which is opposite to the box cover 2, is symmetrically provided with fixing bolts 8, the tail end of a fixed bolt 8 penetrates through a fixed plate 7 to be in threaded connection with a box body 1, the left side of the top of a box cover 2 is communicated with a feeding pipe 9, a first control valve 10 is arranged on the feeding pipe 9, mounting plates 11 are symmetrically arranged on the left side and the right side of the box body 1, a heating pipe 12 is embedded in one side, which is attached to the box body 1, of the mounting plates 11, a supporting plate 13 is symmetrically arranged on the bottom surface of an inner cavity of the box body 1, a filter screen 14 is arranged on the top of the supporting plate 13, vertical rods 15 are symmetrically arranged on the left side and the right side of the top of the filter screen 14, the top of the vertical rod 15 is attached to the box cover 2, the bottom of the box body 1 is provided with a square plate 16, a cavity 17 is arranged in the square plate 16, the left side and the right side of the square plate 16 are symmetrically provided with guide pipes 18, the guide pipes 18 are communicated with the cavity 17, the guide pipes 18 are provided with third control valves 19, the bottom of the square plate 16 is symmetrically provided with bolts 20, and the tail end of the bolt 20 runs through the square plate 16 to be in threaded connection with the box body 1, a round hole 21 which is run through from top to bottom is formed in the middle of the square plate 16, a discharge pipe 22 is arranged in the round hole 21, the top end of the discharge pipe 22 is communicated with the inner cavity of the box body 1, a second control valve 23 is arranged on the discharge pipe 22, a transparent window 24 is arranged on the front side of the box body 1, and the reaction condition of palladium powder in the box body 1 is known.

Example two

As shown in FIGS. 1-4, the device for preparing palladium ultrafine powder according to the embodiment of the present invention comprises a box body 1, a box cover 2 is disposed on the top of the box body 1, a motor box 3 is disposed in the middle of the top of the box cover 2, a motor 4 is disposed in the motor box 3, an output end of the bottom of the motor 4 is connected with a rotating shaft 5, stirring rods 6 are symmetrically disposed on the outer wall of the rotating shaft 5 at equal intervals, the stirring rods 6 are disposed in the box body 1, fixing plates 7 are symmetrically disposed on both sides of the box cover 2, fixing bolts 8 are symmetrically disposed on one side of the fixing plates 7 opposite to the box cover 2, the tail ends of the fixing bolts 8 penetrate through the fixing plates 7 and are in threaded connection with the box body 1, a feeding pipe 9 is communicated with the left side of the top of the box cover 2, a first control valve 10 is disposed on the feeding pipe 9, mounting plates 11 are symmetrically disposed on both sides of the box body 1, a heating pipe 12 is embedded in one side of the mounting plate 11, a supporting plate 13 is symmetrically disposed on the bottom surface of the inner cavity of the box body 1, the top of the supporting plate 13 is provided with a filter screen 14, the left side and the right side of the top of the filter screen 14 are symmetrically provided with vertical rods 15, the top of each vertical rod 15 is attached to the box cover 2, the bottom of the box body 1 is provided with a square plate 16, a cavity 17 is formed in the square plate 16, the left side and the right side of the square plate 16 are symmetrically provided with guide pipes 18, the guide pipes 18 are communicated with the cavity 17, the guide pipes 18 are provided with third control valves 19, the bottom of the square plate 16 is symmetrically provided with bolts 20, the tail ends of the bolts 20 penetrate through the square plate 16 to be in threaded connection with the box body 1, the middle of the square plate 16 is provided with a circular hole 21 which is vertically communicated, a discharge pipe 22 is arranged in the circular hole 21, the top end of the discharge pipe 22 is communicated with the inner cavity of the box body 1, the discharge pipe 22 is provided with a second control valve 23, a gap is reserved between the rotating shaft 5 and the vertical rods 15, and the rotating shaft 5 is prevented from contacting with the vertical rods 15 to influence each other, be provided with horizontal pole 25 between two montants 15 that correspond around, and horizontal pole 25 top and case lid 2 are laminated mutually, and the operator holds horizontal pole 25, takes out montant 15 and filter screen 14, leaves the clearance between filter screen 14 and the axis of rotation 5, prevents that filter screen 14 and axis of rotation 5 from contacting and receive the damage.

EXAMPLE III

As shown in figures 1-4, the device for preparing ultrafine palladium powder according to the embodiment of the present invention comprises a box body 1, a box cover 2 is arranged on the top of the box body 1, a motor box 3 is arranged in the middle of the top of the box cover 2, a motor 4 is arranged in the motor box 3, the output end of the bottom of the motor 4 is connected with a rotating shaft 5, stirring rods 6 are symmetrically and equidistantly arranged on the outer wall of the rotating shaft 5, the stirring rod 6 is positioned in the box body 1, the two sides of the box cover 2 are symmetrically provided with fixing plates 7, one side of each fixing plate 7, which is opposite to the box cover 2, is symmetrically provided with fixing bolts 8, the tail end of a fixed bolt 8 penetrates through a fixed plate 7 to be in threaded connection with a box body 1, the left side of the top of a box cover 2 is communicated with a feeding pipe 9, a first control valve 10 is arranged on the feeding pipe 9, mounting plates 11 are symmetrically arranged on the left side and the right side of the box body 1, a heating pipe 12 is embedded in one side, which is attached to the box body 1, of the mounting plates 11, a supporting plate 13 is symmetrically arranged on the bottom surface of an inner cavity of the box body 1, a filter screen 14 is arranged on the top of the supporting plate 13, vertical rods 15 are symmetrically arranged on the left side and the right side of the top of the filter screen 14, the top of the vertical rod 15 is attached to the box cover 2, the bottom of the box body 1 is provided with a square plate 16, a cavity 17 is arranged in the square plate 16, the left side and the right side of the square plate 16 are symmetrically provided with guide pipes 18, the guide pipes 18 are communicated with the cavity 17, the guide pipes 18 are provided with third control valves 19, the bottom of the square plate 16 is symmetrically provided with bolts 20, and the tail end of the bolt 20 penetrates through the square plate 16 to be in threaded connection with the box body 1, a round hole 21 which is through up and down is formed in the middle of the square plate 16, a discharge pipe 22 is arranged in the round hole 21, the top end of the discharge pipe 22 is communicated with the inner cavity of the box body 1, a second control valve 23 is arranged on the discharge pipe 22, a gap is reserved between the square plate 16 and the second control valve 23, and the second control valve 23 is better located in the round hole 21.

To sum up, with the aid of the above-mentioned technical scheme of the utility model, this device is when using, open first control valve 10, lead palladium powder and dispersant to in the box 1 through inlet pipe 9, be motor 4 and the power supply of heating pipe 12 through external power supply, it stirs palladium powder and dispersant to open motor 4, when the temperature is lower, open heating pipe 12, solution to in the box 1 heats, when the temperature is higher, open third control valve 19, pour into cavity 17 with cold water through being located left pipe 18, and discharge through being located the pipe 18 on right side, cool down the solution in the box 1, thereby adjust the temperature in the box 1 as required, after the reaction is accomplished, open second control valve 23, pass through discharging pipe 22 with solution and discharge, after the discharge is accomplished, screw out gim peg 8, with case lid 2 and box 1 separation, propose filter screen 14 through horizontal pole 25, thereby be convenient for collect the palladium powder that 14 tops of filter screen have not reacted.

The above description is only for the preferred embodiment of the present invention, and should not be taken as limiting the invention, and any modifications, equivalent replacements, improvements, etc. made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims

1. The device for preparing the superfine palladium powder is characterized by comprising a box body (1), wherein a box cover (2) is arranged at the top of the box body (1), a motor box (3) is arranged in the middle of the top of the box cover (2), a motor (4) is arranged in the motor box (3), the output end of the bottom of the motor (4) is connected with a rotating shaft (5), stirring rods (6) are symmetrically and equidistantly arranged on the outer wall of the rotating shaft (5), the stirring rods (6) are positioned in the box body (1), fixing plates (7) are symmetrically arranged on two sides of the box cover (2), fixing bolts (8) are symmetrically arranged on one sides of the fixing plates (7) opposite to the box cover (2), the tail ends of the fixing bolts (8) penetrate through the fixing plates (7) and are in threaded connection with the box body (1), the left side of the top of the box cover (2) is communicated with a feed pipe (9), a first control valve (10) is arranged on the feed pipe (9), mounting plates (11) are symmetrically arranged on the left side and the right side of the box body (1), a heating pipe (12) is embedded on one side of the mounting plate (11) opposite to one side of the box body (1), a supporting plate (13) is symmetrically arranged on the bottom of the box body (1), a left side of the inner cavity (13), the inner cavity (14) and the filtering net (14) are symmetrically arranged on the left side of the filtering net (14), and the filtering net (14) symmetrically arranged on the filtering net (14), just montant (15) top is laminated with case lid (2) mutually, box (1) bottom is provided with square board (16), cavity (17) have been seted up in square board (16), square board (16) left and right sides symmetry is provided with pipe (18), pipe (18) are linked together with cavity (17), be provided with third control valve (19) on pipe (18), square board (16) bottom symmetry is provided with bolt (20), just bolt (20) tail end runs through square board (16) and box (1) threaded connection, round hole (21) that link up from top to bottom are seted up in the middle of square board (16), be provided with discharging pipe (22) in round hole (21), discharging pipe (22) top is linked together with box (1) inner chamber, be provided with second control valve (23) on discharging pipe (22).

2. The apparatus for preparing palladium ultrafine powder according to claim 1, wherein a transparent window (24) is provided at the front side of the chamber (1).

3. The apparatus for preparing palladium micropowder of claim 1, wherein a gap is left between the rotating shaft (5) and the vertical rod (15).

4. The device for preparing ultrafine palladium powder according to claim 1, wherein a cross bar (25) is arranged between two corresponding vertical bars (15) and the top of the cross bar (25) is attached to the box cover (2).

5. The apparatus for preparing palladium micropowder of claim 1, wherein a gap is left between the filter screen (14) and the rotating shaft (5).

6. The apparatus for preparing palladium micropowder according to claim 1, wherein a gap is left between the square plate (16) and the second control valve (23).