CN218553176U - Crystallization device for preparing chemical reagent - Google Patents

Abstract

The utility model relates to a crystallization device technical field specifically is a crystallization device for chemical reagent preparation, which comprises a housin, concentration chamber, the agitator, motor I, zone of heating and crystallization case, the inner wall at the casing is installed to the zone of heating, the inner wall of zone of heating is located to the concentration chamber, the inside at the concentration chamber is installed to the agitator, motor I installs the top at the casing, one side at the casing is located to the crystallization case, the agitator is equipped with a plurality of arc poles by pivot and outside equidistance and constitutes, elevating system is installed to one side of casing, the last pump that is equipped with of elevating system, the input of pump, the export is connected with extraction tube and hose respectively, the one end and the crystallization case of hose are connected. The utility model discloses a to concentrate and crystallization step separation, change to and let the structure that the extraction tube can reciprocate in the inside of concentrated room by elevating system and replace the structure of current bottom installation discharge pipe, just so avoid chemical reagent in the discharge pipe of fractional entering bottom before concentrated, avoid influencing the quality of follow-up formation crystallization form.

Description

A crystallization device for chemical reagent preparation

Technical Field

The utility model relates to a crystallization device technical field specifically is a crystallization device for chemical reagent preparation.

Background

At present, most of the steps for forming crystals are heating and stirring, and the crystals are obtained by cooling, but the existing crystallization device has the defects, such as the patent numbers: CN201822116769.6, this utility model discloses a device is appeared with crystallization in chemical reagent preparation, including box, basin, driving motor and temperature sensor, the box inboard is provided with row material pipe, arrange material pipe one end and install the pump of taking out, basin internally mounted has the reaction test tube, the inside inlet tube that is provided with of box, the water intaking valve is installed to inlet tube one end, reaction test tube upper end is provided with the upper cover, the driving motor lower extreme is provided with the agitator, the temperature sensor below is provided with the heater, the box outside is provided with the observation window. The utility model has the advantages that: 1. by arranging the water tank, the device heats or refrigerates the reaction test tube by heating or refrigerating a medium, so that the chemical reagent is heated or cooled more uniformly, the reaction is more stable, and the practicability is high; 2. set up the pump of taking out, take out the chemical reagent after will reacting, not only improved the work efficiency of device, can also avoid user direct contact reagent, improve the security of device.

As mentioned above, the discharge pipe is not designed reasonably, and reagent liquid is easy to enter before stirring, which can affect the quality of subsequent crystallization, so we improve the problem and propose a crystallization device for chemical reagent preparation.

SUMMERY OF THE UTILITY MODEL

The utility model provides a crystallization device for chemical reagent preparation, including casing, concentration chamber, agitator, motor, zone of heating and crystallization case, the inner wall at the casing is installed to the zone of heating, concentration chamber locates the inner wall of zone of heating, the agitator is installed concentration chamber's inside, motor is installed the top of casing, the crystallization case is located one side of casing, the agitator is equipped with a plurality of arc poles by pivot and outside equidistance and constitutes, elevating system is installed to one side of casing, the last pump that is equipped with of elevating system, the input of pump, export are connected with extraction pipe and hose respectively, the one end of hose with the crystallization case is connected.

As a preferred technical scheme of the utility model, the feed liquor pipe is installed to one side at casing top, the bottom of feed liquor pipe is run through the casing is arranged in the inside of concentration chamber, the top of feed liquor pipe is the funnel shape.

As an optimal technical scheme of the utility model, the controller is installed on the top of casing opposite side, the output shaft of motor one runs through the casing pass through the shaft coupling with the top of agitator links firmly, motor one with controller electric connection.

As an optimized technical scheme of the utility model, the laminating of zone of heating the outer wall of concentrating chamber, zone of heating and controller electric connection.

As a preferred technical scheme of the utility model, elevating system includes two mounting panels, lead screw, two motors and support, two the mounting panel is fixed top and the bottom that is close to crystallization box one side respectively, the lead screw is installed two between the mounting panel, the support cover is established the outside of lead screw is connected rather than the transmission, the bottom at one of them mounting panel is installed to motor two, the top at the support is installed to the pump, elevating system and pump all with controller electric connection.

As a preferred technical scheme of the utility model, the extraction tube is the type of falling U, one of them fixed gusset plate that is equipped with of department of bending of extraction tube, the one end of extraction tube is run through the inside of concentrating chamber is arranged in to the casing, the one end of hose with the import at crystallization tank top links firmly and is linked together.

As a preferred technical scheme of the utility model, refrigerating plant is installed to the inside bottom of crystallization case, refrigerating plant's top activity is equipped with and holds the groove, the positive swing joint of crystallization case has the chamber door.

The utility model has the advantages that: this kind of a crystallization device for chemical reagent preparation through with concentration and crystallization step separation, changes to and lets the structure that the extraction tube can reciprocate in the inside of concentrated room by elevating system and replaces the structure of current bottom installation discharge pipe, just so avoids chemical reagent in the discharge pipe of fractional entering bottom before the concentration, avoids influencing the quality of follow-up formation crystal form.

Drawings

The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention, and together with the description serve to explain the invention and not to limit the invention. In the drawings:

FIG. 1 is a schematic view of a crystallization apparatus for chemical reagent preparation according to the present invention;

FIG. 2 is a schematic diagram of the configuration of the concentrated solution extracted by the crystallization apparatus for chemical reagent preparation and the internal planar structure of the crystallization chamber according to the present invention.

In the figure: 1. a housing; 2. a concentration chamber; 3. a stirrer; 4. a first motor; 5. a heating layer; 6. a crystallization box; 7. a refrigeration device; 8. a lifting mechanism; 81. mounting a plate; 82. a screw rod; 83. a second motor; 84. a support; 9. pumping; 10. an extraction pipe; 11. a hose; 12. a controller; 13. a liquid inlet pipe; 14. a reinforcing plate; 15. and (4) a containing groove.

Detailed Description

The preferred embodiments of the present invention will be described in conjunction with the accompanying drawings, and it will be understood that they are presented herein only to illustrate and explain the present invention, and not to limit the present invention.

Example (b): as shown in figure 1 and figure 2, the utility model relates to a crystallization device for chemical reagent preparation, which comprises a housin 1, concentration chamber 2, agitator 3, a motor 4, zone of heating 5 and crystallization case 6, the inner wall at casing 1 is installed to zone of heating 5, concentration chamber 2 locates the inner wall of zone of heating 5, agitator 3 installs the inside at concentration chamber 2, the top at casing 1 is installed to a motor 4, one side of casing 1 is located to crystallization case 6, agitator 3 is equipped with a plurality of arc poles by pivot and outside equidistance and constitutes, elevating system 8 is installed to one side of casing 1, be equipped with pump 9 on elevating system 8, pump 9's input, the export is connected with extraction pipe 10 and hose 11 respectively, hose 11's one end is connected with crystallization case 6

A liquid inlet pipe 13 is arranged on one side of the top of the shell 1, the bottom end of the liquid inlet pipe 13 penetrates through the shell 1 and is arranged in the concentration chamber 2, and the top end of the liquid inlet pipe 13 is funnel-shaped; the top end of the other side of the shell 1 is provided with a controller 12, an output shaft of the motor I4 penetrates through the shell 1 and is fixedly connected with the top end of the stirrer 3 through a coupler, and the motor I4 is electrically connected with the controller 12; the heating layer 5 is attached to the outer wall of the concentration chamber 2, and the heating layer 5 is electrically connected with the controller 12; chemical reagents are poured into the concentrating chamber 2 from the liquid inlet pipe 13, the chemical reagents are convenient to pour by arranging the top of the liquid inlet pipe 13 to be in a funnel shape, and the chemical reagents are prevented from being spilled when being poured; the controller 12 is started to control the motor I4 to be in a working state, namely, an output shaft of the motor I4 drives the stirrer 3 to rotate in the concentration chamber 2 through the coupler, and the rotating speed of the stirrer 3 can be adjusted through the controller 12; since the chemical agent is simultaneously heated and stirred at a temperature, the evaporable liquid in the chemical agent is removed over a period of time, and a thick liquid is formed.

The lifting mechanism 8 comprises two mounting plates 81, a screw rod 82, a second motor 83 and a support 84, the two mounting plates 81 are respectively fixed at the top end and the bottom end close to one side of the crystallization box 6, the screw rod 82 is mounted between the two mounting plates 81, the support 84 is sleeved outside the screw rod 82 and is in transmission connection with the screw rod, the second motor 83 is mounted at the bottom of one of the mounting plates 81, the pump 9 is mounted at the top of the support 84, and the lifting mechanism 8 and the pump 9 are both electrically connected with the controller 12; the extraction pipe 10 is in an inverted U shape, a reinforcing plate 14 is fixedly arranged at one bent part of the extraction pipe 10, one end of the extraction pipe 10 penetrates through the shell 1 and is arranged inside the concentration chamber 2, and one end of the hose 11 is fixedly connected and communicated with an inlet at the top of the crystallization box 6; the controller 12 also controls the lifting mechanism 8 to work, that is, the output shaft of the second motor 83 drives the screw rod 82 to rotate between the two mounting plates 81 through the coupler, the screw rod 82 drives the support 84 outside the screw rod 82 to move upwards or downwards when rotating, and one side of the support 84 is connected with the shell 1 in a low position, so that the support 81 is blocked by the shell 1 along with the rotation of the screw rod 82 and cannot rotate along with the screw rod, the support 84 moves outside the screw rod 82, and the pumping pipe 10 is connected with the pumping pump 9 because the pumping pump 9 is mounted on the support 84 and further performs lifting movement together, so that the pumping pipe 10 can move towards the inside of the concentration chamber 2 until moving to the bottommost part to pump the chemical reagent forming thick liquid; the reinforcing plate 14 functions to reinforce the extraction pipe 10 in the form of an inverted U.

A refrigerating device 15 is arranged at the bottom end inside the crystallization box 6, a containing groove 16 is movably arranged at the top of the refrigerating device 15, and the front surface of the crystallization box 6 is movably connected with a box door; the inside of crystallization case 6 is carried by hose 11 again to the thick liquid of extraction, gets into the inside that holds groove 16 promptly, and refrigerating plant 15 is controlled by controller 12 and is begun refrigeration work, leads cold to holding groove 16, lets its inside thick liquid form of being cooled and forms the crystallization form, and it can to take out to open the positive chamber door of crystallization case 6 at last.

In the description of the present invention, it should be noted that the terms "vertical", "upper", "lower", "horizontal", and the like indicate the directions or positional relationships based on the directions or positional relationships shown in the drawings, which are only for the convenience of describing the present invention and simplifying the description, but do not indicate or imply that the device or element referred to must have a specific direction, be constructed and operated in a specific direction, and thus, should not be construed as limiting the present invention.

In the description of the present invention, it should also be noted that, unless otherwise explicitly specified or limited, the terms "disposed," "mounted," "connected," and "connected" are to be construed broadly, and may be, for example, fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood according to specific situations by those skilled in the art.

Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described in the foregoing embodiments, or equivalents may be substituted for elements thereof. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (7)

1. The utility model provides a crystallization device for chemical reagent preparation, includes casing (1), concentrated room (2), agitator (3), motor (4), zone of heating (5) and crystallization case (6), the inner wall in casing (1) is installed in zone of heating (5), concentrated room (2) are located the inner wall of zone of heating (5), agitator (3) are installed the inside of concentrated room (2), install motor (4) the top of casing (1), crystallization case (6) are located one side of casing (1), agitator (3) are equipped with a plurality of arc poles by pivot and outside equidistance and constitute, its characterized in that, elevating system (8) are installed to one side of casing (1), be equipped with on elevating system (8) and take out pump (9), the input of take out pump (9), export are connected with extraction tube (10) and hose (11) respectively, the one end of hose (11) with crystallization case (6) are connected.

2. The crystallization device for chemical reagent preparation according to claim 1, wherein a liquid inlet pipe (13) is installed at one side of the top of the housing (1), the bottom end of the liquid inlet pipe (13) penetrates through the housing (1) and is placed inside the concentration chamber (2), and the top end of the liquid inlet pipe (13) is funnel-shaped.

3. The crystallization device for preparing chemical reagents according to claim 1, wherein a controller (12) is installed at the top end of the other side of the housing (1), the output shaft of the motor I (4) penetrates through the housing (1) and is fixedly connected with the top end of the stirrer (3) through a coupling, and the motor I (4) is electrically connected with the controller (12).

4. The crystallization device for chemical reagent preparation according to claim 1, wherein the heating layer (5) is attached to the outer wall of the concentration chamber (2), and the heating layer (5) is electrically connected with the controller (12).

5. The crystallization device for preparing the chemical reagent according to claim 1, wherein the lifting mechanism (8) comprises two mounting plates (81), a screw rod (82), a second motor (83) and a support (84), the two mounting plates (81) are respectively fixed at the top end and the bottom end of one side of the crystallization box (6), the screw rod (82) is installed between the two mounting plates (81), the support (84) is sleeved outside the screw rod (82) and is in transmission connection with the screw rod, the second motor (83) is installed at the bottom of one of the mounting plates (81), the pump (9) is installed at the top of the support (84), and the lifting mechanism (8) and the pump (9) are both electrically connected with the controller (12).

6. The crystallization device for preparing the chemical reagent according to claim 1, wherein the extraction pipe (10) is in an inverted U shape, a reinforcing plate (14) is fixedly arranged at one bending part of the extraction pipe (10), one end of the extraction pipe (10) penetrates through the shell (1) and is arranged inside the concentration chamber (2), and one end of the hose (11) is fixedly connected and communicated with an inlet at the top of the crystallization tank (6).

7. The crystallization device for chemical reagent preparation according to claim 1, wherein a refrigeration device (7) is installed at the bottom end inside the crystallization box (6), a containing groove (15) is movably arranged at the top of the refrigeration device (7), and a box door is movably connected to the front surface of the crystallization box (6).

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