CN213609897U

CN213609897U - Crystallization tube structure for organic chemistry

Info

Publication number: CN213609897U
Application number: CN202022461199.1U
Authority: CN
Inventors: 邹晓艳
Original assignee: Heilongjiang University
Current assignee: Heilongjiang University
Priority date: 2020-10-30
Filing date: 2020-10-30
Publication date: 2021-07-06
Anticipated expiration: 2030-10-30

Abstract

The utility model discloses a crystallization tube structure for organic chemistry, including base, pump machine installation room, cooling chamber, shell and heating chamber, pump machine installation room is installed to top one side of base, the booster pump is installed to the indoor bottom of pump machine installation, the second landing leg is installed to base top pump machine installation room one side, and second landing leg top installs the cooling chamber, the shell is installed to one side of base top cooling chamber, be provided with the teeter chamber by the top in the shell, the below of teeter chamber is provided with the motor installation room in the shell, the third landing leg is installed at pump machine installation room top, the heating chamber is installed at third landing leg top. The utility model discloses an install the booster pump in feed inlet one end, through the booster pump circular telegram operation, can follow the feed inlet with the material and inhale the pump internally, later transmit to the second pipeline in, avoided the work efficiency reduction that artificial charging leads to, improved the device to the work efficiency of crystallization work.

Description

Crystallization tube structure for organic chemistry

Technical Field

The utility model relates to a crystallization technology field specifically is a transistor structure for organic chemistry.

Background

After the hot saturated solution is cooled, the solute is precipitated in the form of crystals, so called crystallization, which is a long-history separation technology commonly used in industrial production of chemical industry, pharmacy, light industry and the like, and when the crystallization technology is used, crystals need to be produced first, and at this time, a crystal tube structure for organic chemistry is needed.

The existing crystal tube structures for organic chemistry have the following disadvantages:

1. the existing crystallization tube structure for organic chemistry has low feeding speed, and most of the existing crystallization tube structure is used for manual feeding, so that the working efficiency is reduced;

2. the existing crystallization tube structure for organic chemistry is often poor in working quality due to insufficient heating and cooling time during heating and cooling;

3. the existing crystallization tube structure for organic chemistry is slow in chemical reaction, so that the working time is prolonged, and therefore the crystallization tube structure for organic chemistry is provided to solve the existing problems.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide a crystal tube structure for organic chemistry to solve the problem that proposes among the above-mentioned background art.

In order to achieve the above object, the utility model provides a following technical scheme: a crystallization tube structure for organic chemistry comprises a base, a pump machine installation chamber, a cooling chamber, a shell and a heating chamber, wherein first support legs are installed at four corners of the bottom of the base, the pump machine installation chamber is installed at one side of the top of the base, a feed inlet is installed at one side of the pump machine installation chamber, a booster pump is installed at the bottom in the pump machine installation chamber, a first pipeline is installed at one end of the booster pump, a second pipeline is installed at the other end of the booster pump, a second support leg is installed at one side of the pump machine installation chamber at the top of the base, the cooling chamber is installed at the top of the second support leg, a water inlet is installed at one side of the cooling chamber by the top, a water outlet is installed at one side of the cooling chamber by the bottom, the shell is installed at one side of the cooling chamber at the top of the, a motor installation chamber is arranged below a stirring chamber in the shell, a stirring shaft is installed in the stirring chamber, one end of the stirring shaft penetrates through the inner wall and is rotatably installed at the bottom of the motor installation chamber, a stirring paddle is installed on the stirring shaft, a mounting seat is installed on one side of the bottom of the motor installation chamber, a motor is installed on the mounting seat, one end of a gear transmission assembly is installed at the output end of the motor, the stirring shaft is provided with the gear transmission assembly matched with the output end of the motor on the bottom, a third supporting leg is installed at the top of the pump installation chamber, a heating chamber is installed at the top of the third supporting leg, a first coupler is installed at the bottom of the heating chamber, a second coupler is installed at the top of the heating chamber, a heating pipe is installed in the heating chamber, and one end of a second pipeline penetrates through the, the second pipeline extends into the cooling chamber through the second coupling, and the second pipeline penetrates through the cooling chamber and is installed in a butt joint mode with one side of the shell.

Preferably, a discharging pipe is installed on one side in the motor installation chamber, one end of the discharging pipe extends to the stirring chamber, and the other end of the discharging pipe is in butt joint with the discharging port.

Preferably, an access door matched with the motor installation chamber for use is rotatably installed on one side of the shell through a hinge, and a handle is installed on one side of the access door.

Preferably, one end of the first pipeline is in butt joint with the feeding hole.

Preferably, a scale is arranged on one side of the cooling chamber.

Preferably, a cross bar is installed between the first legs.

Compared with the prior art, the beneficial effects of the utility model are that:

1. the utility model discloses an install the booster pump in feed inlet one end, through the booster pump circular telegram operation, can follow the feed inlet with the material and inhale the pump internally, later transmit to the second pipeline in, avoided the work efficiency reduction that artificial charging leads to, improved the device to the work efficiency of crystallization work.

2. The utility model discloses an install the cooling chamber at heating chamber and the base top of pump machine installation roof portion installation, heat through the water pipe inside of heating chamber in to the heating chamber, later will be in the second pipeline in the cooling chamber through the cooling chamber and cool off, when the material needs to heat or cool off, when the heating chamber or cooling chamber are carried with the material to the pump machine, close the pump machine, make the material stop in the original place, later heat or cool off, the material quality that has avoided leading to inadequately when long because of heating and refrigerated descends, the device crystallization work's operating mass has been improved greatly.

3. The utility model discloses an at the shell of base top installation, through carrying the stirring room with the material from the second pipeline, open the motor this moment, the motor passes through the rotation that gear drive assembly drove the (mixing) shaft, and the (mixing) shaft drives the stirring rake again and rotates the material that stirs in the stirring room, makes its abundant jingning chemical reaction, has avoided the operating time extension because of chemical reaction leads to slowly, has further improved the device work efficiency to crystallization work.

Drawings

Fig. 1 is a schematic view of the internal structure of the present invention;

fig. 2 is a schematic front structural view of the present invention;

FIG. 3 is a schematic view of the internal structure of the heating chamber assembly of the present invention;

fig. 4 is the internal structure schematic diagram of the motor installation chamber of the present invention.

In the figure: 1. a base; 101. a first leg; 102. a cross bar; 2. a pump mounting chamber; 201. a feed inlet; 202. a booster pump; 203. a first conduit; 204. a second conduit; 3. a cooling chamber; 301. a second leg; 302. a water inlet; 303. a water outlet; 304. a dial gauge; 4. a housing; 401. an access door; 402. a handle; 403. a discharge port; 5. a stirring chamber; 501. a stirring shaft; 502. a stirring paddle; 6. a motor installation chamber; 601. a mounting seat; 602. a motor; 603. a gear drive assembly; 604. a discharging pipe; 7. a heating chamber; 701. a third leg; 702. a first coupling; 703. a second coupling; 704. heating the tube.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "front end", "rear end", "both ends", "one end", "the other end" and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the device or element to which the reference is made must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.

In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "connected," and the like are to be construed broadly, and for example, "connected" may be either fixedly connected or detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood in specific cases to those skilled in the art.

Referring to fig. 1-4, the present invention provides an embodiment: a crystallization tube structure for organic chemistry comprises a base 1, a pump machine installation chamber 2, a cooling chamber 3, a shell 4 and a heating chamber 7, wherein four corners of the bottom of the base 1 are provided with first supporting legs 101, a cross rod 102 is arranged between the first supporting legs 101, one side of the top of the base 1 is provided with the pump machine installation chamber 2, one side of the pump machine installation chamber 2 is provided with a feeding hole 201, the bottom in the pump machine installation chamber 2 is provided with a booster pump 202, the booster pump 202 applies a very low pressure to a large-diameter air driving piston, when the pressure acts on a small-area piston, a high pressure is generated, the booster pump 202 can realize continuous operation through a two-position five-way air control reversing valve, materials can be sucked into the pump body from the feeding hole 201 through the booster pump 202 in electrified operation and then are transmitted into a second pipeline 204, and the reduction of the working efficiency caused by artificial charging is avoided, the booster pump 202 can adopt JET, one end of the booster pump 202 is provided with a first pipeline 203, one end of the first pipeline 203 is in butt joint with the feeding hole 201, the other end of the booster pump 202 is provided with a second pipeline 204, one side of a pump installation chamber 2 at the top of the base 1 is provided with a second supporting leg 301, the top of the second supporting leg 301 is provided with a cooling chamber 3, one side of the cooling chamber 3 is provided with a water inlet 302 near the top, one side of the cooling chamber 3 is provided with a water outlet 303 near the bottom, one side of the cooling chamber 3 is provided with a dial gauge 304, one side of the cooling chamber 3 at the top of the base 1 is provided with a shell 4, one side of the shell 4 is rotatably provided with an access door 401 matched with the motor installation chamber 6 through a hinge, one side of the access door 401 is provided with a handle 402, one side of the shell 4 is provided with a discharge, the stirring chamber 5 is internally provided with a stirring shaft 501, one end of the stirring shaft 501 penetrates through the inner wall and is rotatably arranged with the bottom of the motor installation chamber 6, the stirring shaft 501 is provided with a stirring paddle 502, one side of the bottom of the motor installation chamber 6 is provided with an installation seat 601, the installation seat 601 is provided with a motor 602, the motor is a device for converting electric energy into mechanical energy, the device utilizes an electrified coil (namely a stator winding) to generate a rotating magnetic field and acts on a rotor (such as a squirrel cage type closed aluminum frame) to form magnetoelectric power rotating torque, the motor 602 rotates after being electrified and operates, the stirring shaft 501 is driven to rotate by a gear transmission component 603, the stirring shaft 501 drives the stirring paddle 502 to rotate, so that the material reaction in the stirring chamber 5 is accelerated, the motor 602 can adopt NCH18-100W-50S, one end of the gear transmission component 603 is arranged at the output end of the motor 602, and the, a blanking pipe 604 is arranged on one side in the motor installation chamber 6, one end of the blanking pipe 604 extends to the stirring chamber 5, the other end of the blanking pipe 604 is in butt joint with the discharge port 403, a third supporting leg 701 is arranged on the top of the pump installation chamber 2, a heating chamber 7 is arranged on the top of the third supporting leg 701, a first coupling 702 is arranged at the bottom of the heating chamber 7, a second coupling 703 is arranged on the top of the heating chamber 7, a heating pipe 704 is arranged in the heating chamber 7, one end of a second pipeline 204 penetrates through the pump installation chamber 2 and enters the heating chamber 7 through the first coupling 702, the second pipeline 204 extends into the cooling chamber 3 through the second coupling 703, the second pipeline 204 penetrates through the cooling chamber 3 and is in butt joint with one side of the shell 4, the heating pipe 704 consumes electric energy and converts the electric energy into heat energy to heat the material to be heated, and low-temperature fluid medium enters an input port of the heating pipe, along a specific heat exchange flow channel in the electric heating container, a path designed by using the fluid thermodynamic principle is used for taking away high-temperature heat energy generated in the working process of an electric heating element, so that the temperature of a heated medium is increased, the inside of a second pipeline 204 in a heating chamber 7 is heated through the heating chamber 7, then the second pipeline 204 in a cooling chamber 3 is cooled through the cooling chamber 3, when the material needs to be heated or cooled, when a pump conveys the material to the heating chamber 7 or the cooling chamber 3, the pump is turned off, so that the material stays in place, then the material is heated or cooled, and a heating pipe 704 can adopt DN40-220W-3 KW.

The working principle is as follows: before using the device, a user firstly detects the device, confirms that the device is used after no problem exists, firstly, an external pipeline is in butt joint with the feeding hole 201, then, the booster pump 202 is opened, the booster pump 202 sucks materials, then, the materials are output to the stirring chamber 5, the materials can be heated or cooled in the process, when the materials need to be heated or cooled, the materials enter the heating chamber 7 or the cooling chamber 3 to close the booster pump 202 to enable the materials to be fixed, then, the switch of the heating chamber 7 is opened or cooling liquid is poured into the cooling chamber 3 to heat or cool the materials, then, the materials are conveyed into the stirring chamber 5, the motor 602 is started, the stirring paddle 502 is rotated to properly stir the materials in the stirring chamber 5, and then, the materials are poured out from the discharging hole 403.

It is obvious to a person skilled in the art that the invention is not restricted to details of the above-described exemplary embodiments, but that it can be implemented in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.

Claims

1. A crystal tube structure for organic chemistry, includes base (1), pump installation room (2), cooling chamber (3), shell (4) and heating chamber (7), its characterized in that: base (1) bottom four corners all installs first landing leg (101), pump machine installation room (2) are installed to top one side of base (1), feed inlet (201) are installed to one side of pump machine installation room (2), booster pump (202) are installed to the bottom in pump machine installation room (2), first pipeline (203) are installed to the one end of booster pump (202), second pipeline (204) are installed to the other end of booster pump (202), second landing leg (301) are installed to base (1) top pump machine installation room (2) one side, and cooling chamber (3) are installed at second landing leg (301) top, water inlet (302) are installed by the top to cooling chamber (3) one side, outlet (303) are installed by the bottom to cooling chamber (3) one side, shell (4) are installed to one side of base (1) top cooling chamber (3), the stirring device is characterized in that a discharge hole (403) is formed in one side of the shell (4) by the bottom, a stirring chamber (5) is arranged in the shell (4) by the top, a motor installation chamber (6) is arranged below the stirring chamber (5) in the shell (4), a stirring shaft (501) is installed in the stirring chamber (5), one end of the stirring shaft (501) penetrates through the inner wall and is rotatably installed at the bottom of the motor installation chamber (6), a stirring paddle (502) is installed on the stirring shaft (501), an installation seat (601) is installed on one side of the bottom of the motor installation chamber (6), a motor (602) is installed on the installation seat (601), one end of a gear transmission component (603) is installed at the output end of the motor (602), a gear transmission component (603) matched with the output end of the motor (602) is installed on the bottom of the stirring shaft (501), and a third supporting leg (701) is installed at, heating chamber (7) are installed at third landing leg (701) top, first shaft coupling (702) are installed to the bottom of heating chamber (7), and second shaft coupling (703) are installed at the top of heating chamber (7), install heating pipe (704) in heating chamber (7), the one end of second pipeline (204) is run through in pump installation room (2) gets into heating chamber (7) through first shaft coupling (702), second pipeline (204) extend to in cooling chamber (3) through second shaft coupling (703), and second pipeline (204) pass one side butt joint installation of cooling chamber (3) and shell (4).

2. A crystalline tube structure for organic chemistry according to claim 1, wherein: one side installs unloading pipe (604) in motor installation room (6), the one end of unloading pipe (604) extends to teeter chamber (5), and the other end and discharge gate (403) butt joint installation of unloading pipe (604).

3. A crystalline tube structure for organic chemistry according to claim 1, wherein: an access door (401) matched with the motor installation chamber (6) for use is installed on one side of the shell (4) in a rotating mode through hinges, and a handle (402) is installed on one side of the access door (401).

4. A crystalline tube structure for organic chemistry according to claim 1, wherein: one end of the first pipeline (203) is in butt joint with the feed port (201).

5. A crystalline tube structure for organic chemistry according to claim 1, wherein: and a dial gauge (304) is arranged on one side of the cooling chamber (3).

6. A crystalline tube structure for organic chemistry according to claim 1, wherein: a cross rod (102) is arranged between the first legs (101).