CN218307894U - A stirring mechanism for 8-hydroxyquinoline reaction vessel - Google Patents

Abstract

The utility model relates to a reaction vessel technical field discloses an rabbling mechanism that 8-hydroxyquinoline reaction vessel was used includes the reaction barrel, the fixed surface of reaction barrel is connected with the base, sealed lid has been cup jointed at the top of reaction barrel, the inner wall fixedly connected with sealing washer of sealed lid, the top fixedly connected with feed nozzle of sealed lid, the stirring hole has been seted up to the surface of sealing washer. The utility model has the advantages of it is following and effect: motor drive motor pivot drives the glass stick and rotates in the inside in stirring hole, the glass ball that makes the surface under the rotation is followed and is rotated, increase and the area of contact of raw materials, the glass ball is under rotating, it mixes to drive the raw materials, it is more even to make it mix, and glass ball and glass stick can not touch the inner wall of retort, chemical reaction efficiency between the messenger raw materials obtains improving, can be when the stirring through the feed inlet, carry out the material loading to the inside of retort, the staff of being convenient for supplements the content of raw materials at any time.

Description

A stirring mechanism for 8-hydroxyquinoline reaction vessel

technical field

The utility model relates to the technical field of reaction vessels, in particular to a stirring mechanism for 8-hydroxyquinoline reaction vessels.

Background technique

During the preparation process, 8-hydroxyquinoline is synthesized from o-aminophenol, o-nitrophenol, anhydrous glycerin and concentrated sulfuric acid. It is insoluble in water and ether, soluble in ethanol, acetone, chloroform, benzene or dilute acid, can sublimate.

In the prior art, Chinese Patent Publication No. CN210496297U is a reaction vessel capable of high temperature resistance, including a reaction vessel made of metal material, the reaction vessel is provided with a reaction chamber and a material delivery port, and the reaction vessel is connected with a And the sealing cover made of metal material is connected with a locking piece for locking the sealing cover on the reaction vessel, which can improve the ability to resist deformation under high temperature conditions and improve the stability of use in high temperature environments Effect.

However, when this utility model is used in actual use, when it is used to prepare 8-hydroxyquinoline, the staff needs to manually use a glass rod to stir the raw materials, which is inconvenient to operate, and the glass rod is easy to bump into a wall, and manual stirring may cause improper mixing between raw materials. Uniformity may affect the preparation effect, and it is not convenient to clean the inside of the reaction vessel, so it needs to be improved.

Utility model content

The purpose of this utility model is to provide a stirring mechanism for the 8-hydroxyquinoline reaction vessel, which can make the raw materials mix more evenly, and the glass ball and the glass rod will not touch the inner wall of the reaction barrel, so that the chemical reaction between the raw materials The reaction efficiency is improved.

The above-mentioned technical purpose of the utility model is achieved by the following technical solutions: a stirring mechanism for the 8-hydroxyquinoline reaction vessel, comprising a reaction barrel, the outer surface of the reaction barrel is fixedly connected with a base, and the reaction barrel The top of the sealing cover is sleeved with a sealing cover, the inner wall of the sealing cover is fixedly connected with a sealing ring, the top of the sealing cover is fixedly connected with a feeding nozzle, the outer surface of the sealing ring is provided with a stirring hole, and the sealing ring is provided with a stirring hole. The top is fixedly connected with a support frame, the top of the support frame is fixedly connected with a motor, the output end of the motor is fixedly connected with a motor shaft, the bottom of the motor shaft is fixedly connected with a glass rod, and the glass rod runs through the stirring hole Inside, glass balls are fixedly connected to the outer surface of the glass rod.

By adopting the above technical scheme, when the staff is in use, put the prepared raw materials into the reaction barrel, cover the sealing cover on the top of the reaction barrel, the sealing ring makes the sealing effect of the sealing cover better, when the raw materials need to be stirred and mixed , the staff starts the motor, the motor drives the motor shaft to drive the glass rod to rotate inside the stirring hole, and the glass ball on the surface follows the rotation to increase the contact area with the raw material. The glass ball drives the raw material to mix under the rotation, so that The mixing is more uniform, and the glass balls and glass rods will not touch the inner wall of the reaction barrel, so that the chemical reaction efficiency between the raw materials is improved. While stirring, the inside of the reaction barrel can be loaded, which is convenient for the staff to replenish the content of raw materials at any time, and facilitates the progress of the preparation.

The utility model is further configured as follows: a water tank is provided on one side of the reaction barrel, and a water inlet is opened on the top of the water tank.

By adopting the above technical scheme, when the preparation is finished, the staff fills the water tank with water through the water inlet.

The utility model is further configured as follows: a water pump is fixedly connected to the bottom of the inner wall of the water tank, and one end of the water pump is fixedly connected to a water inlet pipe.

By adopting the above-mentioned technical scheme, the staff starts the water pump to generate suction, and the water inlet pipe starts to absorb water.

The utility model is further configured as follows: the other end of the water pump is fixedly connected with an outlet pipe, the outer surface of the water tank is fixedly connected with a water pressure pipe, and one end of the water pressure pipe is fixedly connected with a ferrule.

By adopting the above technical scheme, water flows into the pressurized water pipe from the water outlet pipe, and the ferrule and the glass pipe are clamped.

The further setting of the utility model is that: the outer surface of the reaction barrel is provided with a glass tube, and the outer surface of the glass tube is provided with a valve.

By adopting the above technical scheme, the staff opens the valve, water enters the reaction tank through the glass tube, and closes the valve when the water level is appropriate, the staff rotates the glass rod and glass ball, and the water flow generates rotational force to clean the inside of the reaction tank .

The further setting of the utility model is that: the glass tube extends to the outer surface of the base, and the glass tube is engaged with the inner wall of the ferrule.

By adopting the above technical scheme, after cleaning, the staff will separate the ferrule from the glass tube, and open the valve again, so that the sewage will flow out from the glass tube, which is convenient for cleaning the inside of the reaction tank, and the operation can be repeated to make the reaction tank clean. Much cleaner.

The beneficial effects of the utility model are:

1. In the present utility model, the device can be used in the use of reaction barrel, base, sealing cover, sealing ring, feeding nozzle, stirring hole, support frame, motor, motor shaft, glass rod and glass ball. When the staff is in use, put the prepared raw materials into the reaction barrel, and cover the sealing cover on the top of the reaction barrel. The sealing ring makes the sealing effect of the sealing cover better. When the raw materials need to be stirred and mixed, the staff starts Motor, the motor drives the motor shaft to drive the glass rod to rotate inside the stirring hole, and the glass ball on the surface will follow the rotation to increase the contact area with the raw material. In order to be uniform, and the glass balls and glass rods will not touch the inner wall of the reaction barrel, so that the chemical reaction efficiency between the raw materials is improved. The material of the reaction barrel is glass, and the surface is equipped with scale marks. At the same time, feeding the inside of the reaction barrel is convenient for the staff to replenish the content of raw materials at any time, and facilitates the progress of the preparation.

2. In this utility model, through the cooperative arrangement among the water tank, water inlet, water pump, water inlet pipe, water outlet pipe, pressurized water pipe, ferrule, glass tube and valve, when the device is in use, the staff can pass through the water inlet, Fill the water tank with water, the staff starts the water pump to generate suction, the water inlet pipe starts to absorb water, the water flows into the pressure water pipe from the outlet pipe, the ferrule and the glass tube are clamped, the staff opens the valve, and the water enters the reaction barrel through the glass tube , when the water level is right, close the valve, and the staff will rotate the glass rod and glass ball, and the water flow will generate a rotational force to clean the inside of the reaction barrel. After washing, the staff will separate the ferrule from the glass tube, and open the valve again. The sewage flows out from the glass tube, which is convenient for cleaning the inside of the reaction barrel, and the operation can be repeated, so that the reaction barrel can be cleaned more cleanly.

Description of drawings

In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the accompanying drawings that need to be used in the description of the embodiments will be briefly introduced below. Obviously, the accompanying drawings in the following description are only some implementations of the present invention. For example, those of ordinary skill in the art can also obtain other drawings based on these drawings on the premise of not paying creative efforts.

Fig. 1 is the structural representation of the utility model;

Fig. 2 is the enlarged schematic diagram of the structure at A in Fig. 1 of the present utility model;

Fig. 3 is a structural schematic diagram of the utility model sealing cover;

Fig. 4 is a structural schematic diagram of the utility model water tank.

In the figure, 1. Reaction barrel; 2. Base; 3. Sealing cover; 4. Sealing ring; 5. Feeding nozzle; 6. Stirring hole; 7. Support frame; 8. Motor; 9. Motor shaft; 10. Glass rod; 11. glass ball; 12. water tank; 13. water inlet; 14. water pump; 15. water inlet pipe; 16. water outlet pipe;

detailed description

The technical solutions of the present utility model will be clearly and completely described below in conjunction with specific embodiments. Apparently, the described embodiments are only some of the embodiments of the present invention, but not all of them. Based on the embodiments of the present utility model, all other embodiments obtained by persons of ordinary skill in the art without making creative efforts belong to the scope of protection of the present utility model.

With reference to Fig. 1-4, a kind of stirring mechanism that 8-hydroxyquinoline reaction vessel is used comprises reaction vat 1, and the outer surface of reaction vat 1 is fixedly connected with base 2, and the top of reaction vat 1 is sleeved with sealing cover 3, The inner wall of the sealing cover 3 is fixedly connected with a sealing ring 4, the top of the sealing cover 3 is fixedly connected with a feeding nozzle 5, the outer surface of the sealing ring 4 is provided with a stirring hole 6, and the top of the sealing cover 3 is fixedly connected with a support frame 7, supporting The top of the frame 7 is fixedly connected with a motor 8, the output end of the motor 8 is fixedly connected with a motor shaft 9, the bottom of the motor shaft 9 is fixedly connected with a glass rod 10, the glass rod 10 runs through the inside of the stirring hole 6, and the outer surface of the glass rod 10 The glass ball 11 is fixedly connected. When the staff is in use, they put the prepared raw materials into the reaction barrel 1, cover the sealing cover 3 on the top of the reaction barrel 1, and the sealing ring 4 makes the sealing effect of the sealing cover 3 better. When stirring and mixing the raw materials, the staff starts the motor 8, and the motor 8 drives the motor shaft 9 to drive the glass rod 10 to rotate inside the stirring hole 6, and the glass ball 11 on the surface rotates to increase the contact area with the raw material. Under the rotation of the glass ball 11, the raw materials are driven to mix, so that the mixing is more uniform, and the glass ball 11 and the glass rod 10 will not touch the inner wall of the reaction barrel 1, so that the chemical reaction efficiency between the raw materials is improved, and the reaction The barrel 1 is made of glass, and the surface is provided with a scale line. Through the feeding nozzle 5, the inside of the reaction barrel 1 can be loaded while stirring, so that the staff can replenish the content of raw materials at any time, and facilitate the progress of the preparation. The reaction barrel One side of 1 is provided with a water tank 12, and the top of the water tank 12 is provided with a water inlet 13. After the preparation is completed, the staff fills the water tank 12 with water through the water inlet 13, and the bottom of the inner wall of the water tank 12 is fixedly connected with a water pump 14. One end of the water pump 14 is fixedly connected with a water inlet pipe 15, the staff starts the water pump 14 to generate suction, the water inlet pipe 15 starts to absorb water, the other end of the water pump 14 is fixedly connected with a water outlet pipe 16, and the outer surface of the water tank 12 is fixedly connected with a pressure water pipe 17, One end of the pressure water pipe 17 is fixedly connected with a ferrule 18, water flows into the pressure water pipe 17 from the water outlet pipe 16, the ferrule 18 is clamped with the glass tube 19, the outer surface of the reaction barrel 1 is provided with a glass tube 19, and the outer surface of the glass tube 19 There is a valve 20 on the surface, the staff opens the valve 20, water enters the reaction barrel 1 through the glass tube 19, and when the water level is suitable, the valve 20 is closed, the staff rotates the glass rod 10 and the glass ball 11, and the water flow generates a rotational force, which is The inside of the reaction barrel 1 is cleaned, the glass tube 19 extends to the outer surface of the base 2, and the glass tube 19 is clamped with the inner wall of the ferrule 18. After cleaning, the staff separates the ferrule 18 from the glass tube 19 and the valve 20 again Open to allow sewage to flow out from the glass tube 19, which is convenient for cleaning the inside of the reaction barrel 1, and the operation can be repeated to make the reaction barrel 1 cleaner.

In the utility model, through the reaction barrel 1, the base 2, the sealing cover 3, the sealing ring 4, the feeding nozzle 5, the stirring hole 6, the support frame 7, the motor 8, the motor shaft 9, the glass rod 10 and the glass ball 11 The matching setting can make the device in use, when the staff is in use, put the prepared raw materials into the reaction tank 1, cover the sealing cover 3 on the top of the reaction tank 1, and the sealing ring 4 can make the sealing effect of the sealing cover 3 Better, when the raw materials need to be stirred and mixed, the staff starts the motor 8, and the motor 8 drives the motor rotating shaft 9 to drive the glass rod 10 to rotate inside the stirring hole 6, and the glass ball 11 on the surface is rotated to increase and The contact area of the raw materials, the glass ball 11 is rotating, driving the raw materials to mix, making it more uniform, and the glass ball 11 and the glass rod 10 will not touch the inner wall of the reaction barrel 1, so that the chemical reaction between the raw materials The efficiency is improved. The material of the reaction barrel 1 is glass, and the surface is provided with a scale line. Through the feeding nozzle 5, the inside of the reaction barrel 1 can be loaded while stirring, so that the staff can replenish the content of raw materials at any time and facilitate the preparation. The progress of the water tank 12, the water inlet 13, the water pump 14, the water inlet pipe 15, the water outlet pipe 16, the pressure water pipe 17, the ferrule 18, the glass pipe 19 and the valve 20 can make the device in use, The staff fills the water tank 12 with water through the water inlet 13, the staff starts the water pump 14 to generate suction, the water inlet pipe 15 starts to absorb water, the water flows into the pressure water pipe 17 from the water outlet pipe 16, and the ferrule 18 and the glass pipe 19 are clamped , the staff opens the valve 20, water enters the reaction barrel 1 through the glass tube 19, closes the valve 20 when the water level is suitable, the staff rotates the glass rod 10 and the glass ball 11, and the water flow generates a rotational force, which affects the inside of the reaction barrel 1. After cleaning, the staff will separate the ferrule 18 from the glass tube 19, and open the valve 20 again to allow the sewage to flow out from the glass tube 19, which is convenient for cleaning the inside of the reaction tank 1, and the operation can be repeated to make the reaction tank 1 Cleaned is cleaner.

Although the embodiments of the present invention have been shown and described, those skilled in the art can understand that various changes and modifications can be made to these embodiments without departing from the principle and spirit of the present invention , replacements and modifications, the scope of the present utility model is defined by the appended claims and their equivalents.

Claims (6)

1. a stirring mechanism that 8-hydroxyquinoline reaction vessel is used, comprises reaction barrel (1), it is characterized in that: the outer surface of described reaction barrel (1) is fixedly connected with base (2), and described reaction barrel ( The top of 1) is sleeved with a sealing cover (3), the inner wall of the sealing cover (3) is fixedly connected with a sealing ring (4), and the top of the sealing cover (3) is fixedly connected with a feeding nozzle (5), The outer surface of the sealing ring (4) is provided with a stirring hole (6), the top of the sealing cover (3) is fixedly connected with a support frame (7), and the top of the support frame (7) is fixedly connected with a motor ( 8), the output end of the motor (8) is fixedly connected with a motor shaft (9), the bottom of the motor shaft (9) is fixedly connected with a glass rod (10), and the glass rod (10) runs through the stirring hole ( 6) inside, the outer surface of the glass rod (10) is fixedly connected with a glass ball (11). 2. the stirring mechanism that a kind of 8-hydroxyquinoline reaction vessel according to claim 1 is used is characterized in that: a side of described reaction barrel (1) is provided with water tank (12), and described water tank (12) There is a water inlet (13) at the top. 3. the stirring mechanism that a kind of 8-hydroxyquinoline reaction vessel according to claim 2 is used is characterized in that: the bottom of described water tank (12) inner wall is fixedly connected with water pump (14), and described water pump (14) One end is fixedly connected with water inlet pipe (15). 4. the agitating mechanism that a kind of 8-hydroxyquinoline reaction vessel according to claim 3 is used is characterized in that: the other end of described water pump (14) is fixedly connected with outlet pipe (16), and described water tank (12 ) is fixedly connected with a pressure water pipe (17), and one end of the pressure water pipe (17) is fixedly connected with a ferrule (18). 5. the stirring mechanism that a kind of 8-hydroxyquinoline reaction vessel according to claim 1 is used, is characterized in that: the outer surface of described reaction vat (1) offers glass tube (19), and described glass tube ( 19) is provided with a valve (20) on its outer surface. 6. the stirring mechanism that a kind of 8-hydroxyquinoline reaction vessel according to claim 5 is used is characterized in that: described glass tube (19) extends to the outer surface of base (2), and described glass tube (19) ) is clamped with the inner wall of the ferrule (18).

Images