CN208260753U - Reaction kettle is used in a kind of water-soluble carbon dots preparation - Google Patents

Reaction kettle is used in a kind of water-soluble carbon dots preparation Download PDF

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Publication number
CN208260753U
CN208260753U CN201820552377.1U CN201820552377U CN208260753U CN 208260753 U CN208260753 U CN 208260753U CN 201820552377 U CN201820552377 U CN 201820552377U CN 208260753 U CN208260753 U CN 208260753U
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CN
China
Prior art keywords
water
reaction container
bung
bath
reaction
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Expired - Fee Related
Application number
CN201820552377.1U
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Chinese (zh)
Inventor
张漪�
王中慧
蔡婷婷
高玉莲
王丽芳
任列香
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Luliang University
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Luliang University
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Priority to CN201820552377.1U priority Critical patent/CN208260753U/en
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Publication of CN208260753U publication Critical patent/CN208260753U/en
Expired - Fee Related legal-status Critical Current
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Abstract

The utility model discloses a kind of water-soluble carbon dots preparation reaction kettles, including reaction kettle bracket, the upper surface of the reaction kettle bracket is provided with reaction container, the bottom surface of the reaction container is connect by welding with the upper surface of reaction kettle bracket, bung is provided with above the reaction container, the bung is internally provided with sealing cover, the sealing cover is internally provided with buffer bar, one end of the buffer bar is fixedly mounted on the inside of sealing cover, the other end of the buffer bar is mounted on the inside of bung, and the sealing cover is mounted on the inside of bung by buffer bar;Using sealing cover and buffer bar, when so that bung being mounted on reaction container one end by butterfly rotation bolt and buckle, it is closer that buffer bar contacts sealing cover with reaction container, improve the leakproofness between bung and reaction container, it avoids being introduced into impurity in air inside reaction container in reaction process, the precision of reaction is improved, using spiral shape water-bath pipe, the surface area for increasing water-bath pipe, improves the rate of heating water bath.

Description

Reaction kettle is used in a kind of water-soluble carbon dots preparation
Technical field
The utility model belongs to consersion unit technical field, and in particular to reaction kettle is used in a kind of water-soluble carbon dots preparation.
Background technique
The broad understanding of reaction kettle has the container physically or chemically reacted, is designed by the structure to container and is matched with parameter Set, realize heating, evaporation that technique requires, the mixed function of cooling and low high speed, reaction kettle be widely used in petroleum, chemical industry, Rubber, pesticide, dyestuff, medicine, food, for completing the pressure of the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation Force container.During use, bung and reaction container use integral structure to existing reaction kettle, are easy to cause internal solution Residue cleaning difficulty is big, split type reaction container, poor sealing performance between bung and reaction container, so that easy and outer in reaction process The problem of environment doping in boundary's reduces reaction precision, and simultaneous reactions bucket inner wall washing difficulty is big, and cleaning takes considerable time, thus It is proposed that reaction kettle is used in a kind of water-soluble carbon dots preparation.
Utility model content
The purpose of this utility model is to provide a kind of water-soluble carbon dots preparation reaction kettles, to solve in above-mentioned background technique During use, bung and reaction container use integral structure to the reaction kettle of proposition, are easy to cause internal solution residue clear It is big to manage difficulty, split type reaction container, poor sealing performance between bung and reaction container, so that easy and external environment in reaction process The problem of doping reduces reaction precision, and simultaneous reactions bucket inner wall washing difficulty is big, and cleaning takes considerable time.
To achieve the above object, the utility model provides the following technical solutions: a kind of water-soluble carbon dots preparation reaction kettle, packet Include reaction kettle bracket, the upper surface of the reaction kettle bracket is provided with reaction container, the bottom surface of the reaction container by welding with The upper surface of reaction kettle bracket connects, and is provided with bung above the reaction container, and the bung is internally provided with sealing cover, The sealing cover is internally provided with buffer bar, and one end of the buffer bar is fixedly mounted on the inside of sealing cover, the buffering The other end of bar is mounted on the inside of bung, and the sealing cover is mounted on the inside of bung by buffer bar, the reaction container Outer surface is provided with butterfly rotation bolt, and one end of the butterfly rotation bolt is connect by welding with the outer surface of reaction container, The outer surface of the bung is provided with buckle, and the bung rotates bolt by butterfly and buckle is mounted on the top of reaction container, The outer surface of the reaction container is provided with water-bath water inlet pipe, and one end of the water-bath water inlet pipe is run through the outer surface of reaction container and set It is equipped with water-bath pipe, one end of the water-bath pipe is fixedly mounted on one end of water-bath water inlet pipe, the other end setting of the water-bath pipe There is water-bath outlet pipe, one end of the water-bath outlet pipe is fixed on one end of water-bath pipe, and the other end of the water-bath outlet pipe passes through The surface of reaction container is worn, the bottom of the reaction container is provided with stirring motor, and the stirring motor is fixedly mounted on reaction container Bottom, one end of the stirring motor are provided with stirring rod, and one end of the stirring rod is run through the surface of reaction container and is embedded into The inside of reaction container, one end of the stirring rod are provided with scraper plate, and the surface of the scraper plate is provided with scraper plate stabilizing ring, described to scrape Plate stabilizing ring is fixedly mounted on the surface of scraper plate.
Preferably, the buffer bar is provided with eight, and one end of eight buffer bars is equidistantly mounted on sealing cover Inside, and the side of buffer bar is provided with gag lever post, the both ends of the gag lever post are separately fixed at the table of bung and sealing cover Face.
Preferably, there are two the butterfly rotation bolt settings, two butterfly rotation bolts are symmetrically fixed on reaction The outer surface of bucket, the buckle are U-shaped structure.
Preferably, the water-bath pipe is helical tubular structure, and one end of water-bath pipe is extended to by the bottom of reaction container Above reaction container.
Preferably, the scraper plate is long strip shape structure, and the scraper plate stabilizing ring is cirque structure.
Compared with prior art, the utility model has the beneficial effects that using sealing cover and buffer bar, so that bung passes through When butterfly rotation bolt and buckle are mounted on reaction container one end, it is closer that buffer bar contacts sealing cover with reaction container, improves bucket Leakproofness between lid and reaction container avoids being introduced into impurity in air inside reaction container in reaction process, improves the precision of reaction, Using spiral shape water-bath pipe, increase the surface area of water-bath pipe, improve the rate of heating water bath, reduce heating time, while making to add Heat is more abundant, is that hanging plate rotates under the action of stirring using scraper plate and scraper plate stabilizing ring, improves steady in scraper plate rotation process It is qualitative, increase reaction container cleaning inside convenience, reduces reaction container cleaning inside difficulty.
Detailed description of the invention
Fig. 1 is the reaction kettle cross-sectional view of the utility model;
Fig. 2 is the cover structure schematic diagram of the utility model;
Fig. 3 is the bung attachment structure schematic diagram of the utility model;
Fig. 4 is the blade structure schematic diagram of the utility model;
In figure: 1- reaction kettle bracket, 2- reaction container, 3- bung, 4- sealing cover, 5- buffer bar, 6- butterfly rotate bolt, 7- Buckle, 8- water-bath water inlet pipe, 9- water-bath pipe, 10- water-bath outlet pipe, 11- stirring motor, 12- stirring rod, 13- scraper plate, 14- are scraped Plate stabilizing ring.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1, Fig. 2, Fig. 3 and Fig. 4 are please referred to, the utility model provides a kind of technical solution: a kind of water-soluble carbon dots preparation use Reaction kettle, including reaction kettle bracket 1, the upper surface of reaction kettle bracket 1 are provided with reaction container 2, and the bottom surface of reaction container 2 passes through weldering It connects and is connect with the upper surface of reaction kettle bracket 1, the top of reaction container 2 is provided with bung 3, and bung 3 is internally provided with sealing cover 4, sealing cover 4 is internally provided with buffer bar 5, and one end of buffer bar 5 is fixedly mounted on the inside of sealing cover 4, buffer bar 5 it is another One end is mounted on the inside of bung 3, and sealing cover 4 is mounted on the inside of bung 3, the outer surface setting of reaction container 2 by buffer bar 5 There is butterfly to rotate bolt 6, one end of butterfly rotation bolt 6 is connect by welding with the outer surface of reaction container 2, the appearance of bung 3 Face is provided with buckle 7, and bung 3 rotates bolt 6 by butterfly and buckle 7 is mounted on the top of reaction container 2, the appearance of reaction container 2 Face is provided with water-bath water inlet pipe 8, and one end of water-bath water inlet pipe 8 runs through the outer surface of reaction container 2 and is provided with water-bath pipe 9, water-bath One end of pipe 9 is fixedly mounted on one end of water-bath water inlet pipe 8, and the other end of water-bath pipe 9 is provided with water-bath outlet pipe 10, and water-bath goes out One end of water pipe 10 is fixed on one end of water-bath pipe 9, and the other end of water-bath outlet pipe 10 runs through the surface of reaction container 2, reaction container 2 Bottom be provided with stirring motor 11, stirring motor 11 is fixedly mounted on the bottom of reaction container 2, one end setting of stirring motor 11 There is stirring rod 12, one end of stirring rod 12 runs through the surface of reaction container 2 and is embedded into the inside of reaction container 2, and the one of stirring rod 12 End is provided with scraper plate 13, and the surface of scraper plate 13 is provided with scraper plate stabilizing ring 14, and scraper plate stabilizing ring 14 is fixedly mounted on scraper plate 13 Surface.
In order to increase the leakproofness being closed between bung 3 and reaction container 2, avoids bringing impurity in reaction process into, improve anti- The accuracy answered, in the present embodiment, it is preferred that buffer bar 5 is provided with eight, and one end of eight buffer bars 5 is equidistantly mounted on The inside of sealing cover 4, and the side of buffer bar 5 is provided with gag lever post, the both ends of gag lever post are separately fixed at bung 3 and sealing The surface of lid 4.
In order to improve the convenience that bung 3 is mounted on the top of reaction container 2, reduce bung 3 be mounted on 2 top of reaction container when Between, in the present embodiment, it is preferred that butterfly rotates there are two the settings of bolt 6, and two butterfly rotation bolts 6 are symmetrically fixed on reaction The outer surface of bucket 2, buckle 7 are U-shaped structure.
In order to increase the surface area of water-bath pipe 9, the efficiency of heating water bath is improved, in the present embodiment, it is preferred that water-bath pipe 9 For helical tubular structure, and one end of water-bath pipe 9 extends to 2 top of reaction container by the bottom of reaction container 2.
In order to improve the clean convenience of 2 inner wall of reaction container, reaction container cleaning time is reduced, the steady of the movement of scraper plate 13 is improved Property, in the present embodiment, it is preferred that scraper plate 13 is long strip shape structure, and scraper plate stabilizing ring 14 is cirque structure.
The working principle and process for using of the utility model: in use, bung 3 is covered the top in reaction container 2, and make butterfly Shape is rotating 7 pairs of bolt 6 and buckle just, overturns butterfly at this time and rotates bolt 6, and butterfly rotation bolt 6 is made to enter the interior of buckle 7 Portion, and one end of butterfly rotation bolt 6 is rotated, fixed reaction under the action of butterfly rotation bolt 6 and buckle 7 of bung 3 at this time The upper end of bucket 2, buffer bar 5 compresses under the action of bung 3 and sealing cover 4 at this time, and makes the upper end of sealing cover 4 Yu reaction container 2 It is close to, is passed through reaction solution in the inside of reaction container 2, starts stirring motor 11, work of the stirring rod 12 in stirring motor 11 at this time It is rotated with lower rotation, and with scraper plate 13, while one end of scraper plate 13 is slided in the inner wall of reaction container 2, while being intake in water-bath One end of pipe 8 is passed through boiling water, and boiling water is reached one end of water-bath outlet pipe 10 by water-bath water inlet pipe 8 by water-bath pipe 9, and by water-bath Outlet pipe 10 is discharged.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art, It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.

Claims (5)

1. a kind of water-soluble carbon dots preparation reaction kettle, including reaction kettle bracket (1), it is characterised in that: the reaction kettle bracket (1) Upper surface be provided with reaction container (2), the upper surface that the bottom surface of the reaction container (2) passes through welding and reaction kettle bracket (1) It connects, is provided with bung (3) above the reaction container (2), being internally provided with sealing cover (4) for the bung (3) is described close Capping (4) is internally provided with buffer bar (5), and one end of the buffer bar (5) is fixedly mounted on the inside of sealing cover (4), institute The other end for stating buffer bar (5) is mounted on the inside of bung (3), and the sealing cover (4) is mounted on bung by buffer bar (5) (3) inside, the outer surface of the reaction container (2) are provided with butterfly rotation bolt (6), and the butterfly rotates the one of bolt (6) End is connect by welding with the outer surface of reaction container (2), and the outer surface of the bung (3) is provided with buckle (7), the bung (3) top of reaction container (2) is mounted on by butterfly rotation bolt (6) and buckle (7), the outer surface of the reaction container (2) is set It is equipped with water-bath water inlet pipe (8), one end of the water-bath water inlet pipe (8) runs through the outer surface of reaction container (2) and is provided with water-bath pipe (9), one end of the water-bath pipe (9) is fixedly mounted on one end of water-bath water inlet pipe (8), and the other end of the water-bath pipe (9) is set It is equipped with water-bath outlet pipe (10), one end of the water-bath outlet pipe (10) is fixed on one end of water-bath pipe (9), the water-bath water outlet The other end for managing (10) runs through the surface of reaction container (2), and the bottom of the reaction container (2) is provided with stirring motor (11), described Stirring motor (11) is fixedly mounted on the bottom of reaction container (2), and one end of the stirring motor (11) is provided with stirring rod (12), One end of the stirring rod (12) runs through the surface of reaction container (2) and is embedded into the inside of reaction container (2), the stirring rod (12) One end be provided with scraper plate (13), the surface of the scraper plate (13) is provided with scraper plate stabilizing ring (14), the scraper plate stabilizing ring (14) it is fixedly mounted on the surface of scraper plate (13).
2. a kind of water-soluble carbon dots preparation reaction kettle according to claim 1, it is characterised in that: the buffer bar (5) sets Eight are equipped with, one end of eight buffer bars (5) is equidistantly mounted on the inside of sealing cover (4), and the side of buffer bar (5) It is provided with gag lever post, the both ends of the gag lever post are separately fixed at the surface of bung (3) and sealing cover (4).
3. a kind of water-soluble carbon dots preparation reaction kettle according to claim 1, it is characterised in that: the butterfly rotates bolt (6) there are two setting, two butterfly rotations bolt (6) are symmetrically fixed on the outer surface of reaction container (2), the buckle (7) For U-shaped structure.
4. a kind of water-soluble carbon dots preparation reaction kettle according to claim 1, it is characterised in that: the water-bath pipe (9) is Helical tubular structure, and one end of water-bath pipe (9) is extended to above reaction container (2) by the bottom of reaction container (2).
5. a kind of water-soluble carbon dots preparation reaction kettle according to claim 1, it is characterised in that: the scraper plate (13) is length Bar shaped plate structure, the scraper plate stabilizing ring (14) are cirque structure.
CN201820552377.1U 2018-04-18 2018-04-18 Reaction kettle is used in a kind of water-soluble carbon dots preparation Expired - Fee Related CN208260753U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820552377.1U CN208260753U (en) 2018-04-18 2018-04-18 Reaction kettle is used in a kind of water-soluble carbon dots preparation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820552377.1U CN208260753U (en) 2018-04-18 2018-04-18 Reaction kettle is used in a kind of water-soluble carbon dots preparation

Publications (1)

Publication Number Publication Date
CN208260753U true CN208260753U (en) 2018-12-21

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111650978A (en) * 2020-06-19 2020-09-11 临沂晟泰高分子材料有限公司 Temperature monitoring and adjusting device of synthesis reaction kettle

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111650978A (en) * 2020-06-19 2020-09-11 临沂晟泰高分子材料有限公司 Temperature monitoring and adjusting device of synthesis reaction kettle
CN111650978B (en) * 2020-06-19 2021-11-09 临沂晟泰高分子材料有限公司 Temperature monitoring and adjusting device of synthesis reaction kettle

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GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20181221

Termination date: 20200418

CF01 Termination of patent right due to non-payment of annual fee