CN218189558U - Multifunctional transient Joule thermal reactor device - Google Patents
Multifunctional transient Joule thermal reactor device Download PDFInfo
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- CN218189558U CN218189558U CN202221817333.XU CN202221817333U CN218189558U CN 218189558 U CN218189558 U CN 218189558U CN 202221817333 U CN202221817333 U CN 202221817333U CN 218189558 U CN218189558 U CN 218189558U
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- support frame
- vacuum body
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- 230000001052 transient effect Effects 0.000 title claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 30
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 14
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229910052802 copper Inorganic materials 0.000 claims abstract description 13
- 239000010949 copper Substances 0.000 claims abstract description 13
- 238000006243 chemical reaction Methods 0.000 claims abstract description 9
- 239000000919 ceramic Substances 0.000 claims abstract description 8
- 239000010453 quartz Substances 0.000 claims abstract description 7
- 239000000523 sample Substances 0.000 claims description 44
- 238000001816 cooling Methods 0.000 claims description 19
- 238000005520 cutting process Methods 0.000 claims description 11
- 238000007789 sealing Methods 0.000 claims description 8
- 238000003825 pressing Methods 0.000 claims description 7
- 238000005086 pumping Methods 0.000 claims description 3
- 239000011521 glass Substances 0.000 abstract description 7
- 238000000034 method Methods 0.000 description 9
- 230000000694 effects Effects 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 229910052750 molybdenum Inorganic materials 0.000 description 2
- 239000011733 molybdenum Substances 0.000 description 2
- 239000002086 nanomaterial Substances 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 2
- 229910052721 tungsten Inorganic materials 0.000 description 2
- 239000010937 tungsten Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 239000002028 Biomass Substances 0.000 description 1
- 238000000137 annealing Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009529 body temperature measurement Methods 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 229910021389 graphene Inorganic materials 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 229910001120 nichrome Inorganic materials 0.000 description 1
- 229910000623 nickel–chromium alloy Inorganic materials 0.000 description 1
- 238000004729 solvothermal method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
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Abstract
The utility model discloses a multi-functional transient state joule thermal reactor device, including the vacuum body, vacuum body inner wall symmetry is equipped with insulating fixed block, insulating fixed block top is equipped with the support copper billet, it is equipped with the support and changes the piecing, connect through ceramic frame between two support commentaries on classics piecing, it is equipped with the electrode guide rail to support commentaries on classics piecing top, electrode guide rail inner wall is equipped with the slip and is equipped with the support frame, the support frame inner wall is equipped with a plurality of locating holes, a locating hole passes through three and electrode guide rail inner wall connections of bolt among them, the support frame top is equipped with the electrode preforming, the support frame top is equipped with the recess, be equipped with the quartz slide glass between two recesses, quartz slide glass top is equipped with a plurality of heating plates, vacuum body outer wall is equipped with reaction assembly. The utility model discloses a set up and support switching piece, heating plate and quartzy slide glass, can adopt multiple mode to place, the sample of taking, enlarged the application range of this device, this device conveniently operates moreover to improve synthetic efficiency.
Description
Technical Field
The utility model relates to a joule thermal reactor technical field specifically is a multi-functional transient state joule thermal reactor device.
Background
Nanoparticles are widely used in many fields such as catalysis, new energy and biomass energy due to their excellent chemical properties. The traditional synthesis methods for synthesizing the novel nano material mainly comprise a solvothermal method, an immersion annealing method and the like. The methods generally have the defects of long preparation time, uneven samples, low yield, difficult industrialization, complex process, strict condition requirements and the like, and have become the main reasons for hindering the research progress of current college researchers and industrial researchers.
In the existing research process, a simple reactor is manufactured by utilizing joule heat effect, various novel nano materials such as high-entropy alloy, high-entropy oxide alloy and graphene are successfully prepared, and the obtained material has better performance in the field of catalytic energy storage. However, the current method has certain defects, such as single sample loading mode, slightly complex operation process and high requirement on environment during preparation, so that the current reactor device does not meet the conditions of scientific research and industrialization devices. At present, a device which can rapidly achieve vacuum environment, placement of various samples and large-current power-on heating is needed to be provided for scientific research institutes and industrial fields.
In conclusion, the existing reactor is inconvenient for taking samples in the using process, and has complex operation method and low reaction efficiency.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a multi-functional transient state joule thermal reactor device to solve the problem that proposes in the above-mentioned background art.
In order to solve the technical problem, the utility model provides a following technical scheme: the utility model provides a multi-functional transient state joule thermal reactor device, includes the vacuum body, vacuum body inner wall symmetry is equipped with insulating fixed block, insulating fixed block top is equipped with the support copper billet, it is equipped with the support switching piece to support the copper billet top, and two support connect through ceramic frame between the switching piece, it is equipped with the electrode guide rail to support the switching piece top, electrode guide rail inner wall is equipped with the slip and is equipped with the support frame, the support frame inner wall is equipped with a plurality of locating holes, one of them the locating hole pass through the bolt three with electrode guide rail inner wall connection, the support frame top is equipped with the electrode preforming, the support frame top is equipped with the recess, two be equipped with the quartz slide between the recess, quartz slide top is equipped with a plurality of heating plates, vacuum body outer wall is equipped with reaction assembly.
Further, the reaction assembly comprises an upper cover and a bottom mounting plate, the upper cover is movably arranged on the top of the vacuum body, the bottom mounting plate is arranged on the bottom of the vacuum body, a hasp and a handle are arranged at the top of the upper cover, a plurality of current binding posts, a vacuum exhaust tube, a probe water-cooling shell and a plurality of current binding posts are arranged at the bottom of the bottom mounting plate, and the probe water-cooling shell is sleeved on the outer wall of the vacuum exhaust tube.
Furthermore, the upper cover with be equipped with sealing washer one between the vacuum body, the bottom mounting panel with be equipped with sealing washer two between the vacuum body, the vacuum body bottom is equipped with a plurality of cutting ferrule joints, cutting ferrule joint extends to bottom mounting panel below, the vacuum exhaust tube with wherein cutting ferrule articulate, probe water-cooling shell inner wall is equipped with threaded connection's infrared temperature probe, measures the sample temperature.
Further, probe water-cooling shell outer wall symmetry is equipped with the pagoda joint, electric current terminal top run through in insulating fixed block inner wall, electric current terminal top with it connects to support the copper billet, the vacuum exhaust pipe outer wall is connected with the KF vacuum tube through the cutting ferrule elbow, carries gas.
Furthermore, the ceramic frame is in threaded connection with the support switching block, the electrode guide rail is connected with the support switching block through a first bolt, and the electrode pressing sheet is connected with the support frame through a second bolt and can be taken down or put on.
Furthermore, the quartz glass slide is movably connected with the support frame, the heating plate is movably connected with the quartz glass slide, and the electrode pressing plate is movably connected with the heating plate to fix the heating plate.
Compared with the prior art, the utility model discloses the beneficial effect who reaches is:
1. the utility model discloses a set up electrode guide rail, vacuum body, support switching piece, electrode preforming, support frame, support switching piece, insulating fixed block, heating plate and quartzy slide glass, can adopt multiple mode to place, the sample of taking, enlarged the application range of this device, this device is convenient to be operated moreover to improve synthesis efficiency.
2. The utility model discloses a set up upper cover, bottom mounting panel, handle, infrared temperature probe, vacuum exhaust tube, current terminal, KF vacuum tube, cutting ferrule curved expert and vacuum exhaust tube, can accurately catch sample center temperature, be equipped with probe water-cooling shell and carry out the water-cooling to reduce infrared temperature probe temperature, sealed effect can be more and more good, and whole device is small and exquisite convenient, convenient to carry, the dismouting of being convenient for.
Drawings
The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention, and together with the description serve to explain the invention and not to limit the invention. In the drawings:
FIG. 1 is a front sectional view of the whole body of the present invention;
FIG. 2 is a schematic view of the overall side view structure of the present invention;
fig. 3 is an enlarged schematic view of fig. 2 a according to the present invention;
fig. 4 is a top view of the present invention as a whole;
fig. 5 is an overall bottom view of the present invention;
in the figure: 1. a vacuum body; 2. insulating fixed blocks; 3. supporting the transfer block; 4. supporting the copper block; 5. a ceramic frame; 6. an electrode guide rail; 7. a support frame; 8. pressing an electrode into a sheet; 9. a quartz slide; 10. a heating plate; 11. an upper cover; 12. a bottom mounting plate; 13. a handle; 14. a current terminal; 15. a vacuum exhaust tube; 16. a probe water-cooling shell; 17. a ferrule fitting; 18. an infrared temperature measuring probe; 19. a pagoda joint; 20. the cutting sleeve is bent through; 21. KF16 vacuum tube.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative efforts all belong to the protection scope of the present invention.
Referring to fig. 1-5, the present invention provides a technical solution: the utility model provides a multi-functional transient state joule thermal reactor device, includes vacuum body 1, 1 inner wall symmetry of vacuum body is equipped with insulating fixed block 2, 2 tops of insulating fixed block are equipped with support copper billet 4, support 4 tops of copper billet are equipped with and support switching piece 3, and two support switching pieces 3 between connect through ceramic frame 5, it is equipped with electrode guide rail 6 to support 3 tops of switching piece, electrode guide rail 6 inner wall is equipped with the slip and is equipped with support frame 7, support frame 7 inner wall is equipped with a plurality of locating holes, one of them the locating hole pass through the bolt three with 6 inner wall connections of electrode guide rail, 7 tops of support frame are equipped with electrode preforming 8, 7 tops of support frame are equipped with the recess, two be equipped with quartz glass slide 9 between the recess, 9 tops of quartz glass slide are equipped with a plurality of heating plates 10, 1 outer wall of vacuum body is equipped with reaction assembly, ceramic frame 5 with support switching piece 3 is threaded connection, electrode guide rail 6 pass through bolt one with support switching piece 3 is connected, electrode preforming 8 through bolt two with support frame 7 is connected, can get down or load electrode preforming 8, quartz glass slide 9 with the swing joint is connected the heating plate material, and the heating plate material is convenient for heating slide 10, heating plate change.
The specific implementation mode is as follows: during the use, open upper cover 11, begin to place the sample, the sample has three kinds of placing methods, the first kind, 1 heating plate 10 tiling on the recess of support frame 7, place the sample on heating plate 10, lay 1 layer heating plate 10 on the sample again, compress tightly 2 heating plate 10 both sides with electrode preforming 8, fix with the screw, the second kind, place the slide glass in the recess of support frame 7, lay the base at the slide glass center, tile the sample on the base, install heating plate 10 in support frame 7 top, fix heating plate 10 with the preforming, can change the distance of sample apart from the base, the third kind, namely 1 heating plate 10 tiling on the recess of support frame 7, lay the base at this heating plate 10 center, after the sample is placed, upper cover 11 covers, support frame 7 moves about on electrode guide rail 6, pass through bolt three fixes on electrode guide rail 6, can match the not unidimensional heating plate according to the experimental demand, the heating plate material can select for use molybdenum, tungsten, carbon paper, nichrome is the vacuum, the body is 1, and the body is the clear, and the appearance of the multiple reaction device can be seen, the use scope of this organic glass is enlarged.
Referring to fig. 1-4, the present invention provides a technical solution: the utility model provides a multi-functional transient state joule thermal reactor device, the reaction assembly includes upper cover 11 and bottom mounting panel 12, upper cover 11 activity is located 1 top of vacuum body, bottom mounting panel 12 is located 1 bottom of vacuum body, upper cover 11 top is equipped with hasp and handle 13, and upper cover 11 is connected through hasp design quick installation with the main part, bottom mounting panel 12 bottom is equipped with a plurality of current terminals 14, vacuum exhaust tube 15, probe water-cooling shell 16 and a plurality of current terminals 14, probe water-cooling shell 16 cover is located 15 outer walls of vacuum exhaust tube, upper cover 11 with be equipped with sealing washer one between the vacuum body 1, bottom mounting panel 12 with be equipped with sealing washer two between the vacuum body 1, vacuum body 1 bottom is equipped with a plurality of cutting ferrule joints 17, cutting ferrule joint 17 extends to bottom mounting panel 12 below, vacuum cutting ferrule 15 with wherein the joint 17 is connected, probe water-cooling shell 16 inner wall is equipped with threaded connection's infrared temperature probe 18, and infrared temperature measurement probe 18 is directly hit on the sample basement, the sample temperature is measured, probe water-cooling shell 16 outer wall symmetry is equipped with precious joint 19, terminal 19 runs through the terminal 14 and the insulating block of current supports KF 20 is connected to the vacuum exhaust tube top.
The specific implementation mode is as follows: when the device is used, a sample is heated in a bridging mode inside a cavity, the bridging mode is that copper electrodes supporting copper blocks 4 are mutually independent, electrodes on two sides are bridged through molybdenum, tungsten, carbon paper, nickel-chromium alloy and the like to form a loop, the bottom end of an electrode guide rail 6 is connected to an external direct current power supply or a pulse power supply through the electrodes supporting copper blocks 4, heating is carried out without disassembly, safety and reliability are realized, an aluminum oxide sheet is further fixed in front of the electrode pressing sheet 8, heating electrodes of the electrode pressing sheets 8 on two sides are supported, temperature measuring holes are reserved in the middle of the aluminum oxide sheet, the central temperature of the sample can be accurately captured between the temperature measuring holes, in order to prevent an infrared temperature measuring probe 18 from being too high, a probe water cooling shell 16 is arranged at the bottom of the infrared temperature measuring probe 18 for water cooling, sealing rings I and II are respectively arranged above and below a vacuum body 1, an upper cover 11 and a bottom mounting plate 12 can be automatically tightened when vacuum pumping is carried out, the sealing effect can be better and better, the whole device is small and convenient, carrying is convenient, and convenient to disassemble and assemble and disassemble.
The utility model discloses a theory of operation:
referring to the attached drawings 1-5 of the specification, the utility model discloses a set up electrode guide rail 6, vacuum body 1, support switching piece 3, electrode preforming 8, support frame 7, support switching piece 3, insulating fixed block 2, heating plate 10 and quartzy slide glass 9, can adopt multiple mode to place, the sample of taking, enlarged the application range of this device, this device convenient operation moreover to improve the synthesis efficiency.
Further, refer to specification attached drawing 1-figure 4, the utility model discloses a set up upper cover 11, bottom mounting panel 12, handle 13, infrared temperature probe 18, vacuum exhaust tube 15, current terminal 14, KF16 vacuum tube 21, the curved 20 and the vacuum exhaust tube 15 of leading to of cutting ferrule, can accurately catch sample central temperature, be equipped with probe water-cooling shell 16 and carry out the water-cooling to reduce infrared temperature probe 18 temperature, sealed effect can be more and more good, whole device is small and exquisite convenient, and convenient to carry, the dismouting of being convenient for.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described above, or equivalents may be substituted for elements thereof. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (6)
1. A multifunctional transient joule thermal reactor device comprising a vacuum body (1), characterized by: vacuum body (1) inner wall symmetry is equipped with insulating fixed block (2), insulating fixed block (2) top is equipped with supports copper billet (4), it is equipped with support switching piece (3) to support copper billet (4) top, supports for two and connects through ceramic frame (5) between switching piece (3), it is equipped with electrode guide rail (6) to support switching piece (3) top, electrode guide rail (6) inner wall is equipped with to slide and is equipped with support frame (7), support frame (7) inner wall is equipped with a plurality of locating holes, one of them the locating hole pass through the bolt three with electrode guide rail (6) inner wall connection, support frame (7) top is equipped with electrode preforming (8), support frame (7) top is equipped with the recess, two be equipped with quartz slide (9) between the recess, quartz slide (9) top is equipped with a plurality of heating pieces (10), vacuum body (1) outer wall is equipped with the reaction unit spare.
2. The multifunctional transient joule thermal reactor device of claim 1 wherein: the reaction assembly comprises an upper cover (11) and a bottom mounting plate (12), wherein the upper cover (11) is movably arranged on the top of the vacuum body (1), the bottom mounting plate (12) is arranged on the bottom of the vacuum body (1), a hasp and a handle (13) are arranged on the top of the upper cover (11), a plurality of current terminals (14), a vacuum pumping tube (15), a probe water-cooling shell (16) and a plurality of current terminals (14) are arranged on the bottom of the bottom mounting plate (12), and the probe water-cooling shell (16) is sleeved on the outer wall of the vacuum pumping tube (15).
3. A multifunctional transient joule thermal reactor device according to claim 2, characterized by: the vacuum probe is characterized in that a first sealing ring is arranged between the upper cover (11) and the vacuum body (1), a second sealing ring is arranged between the bottom mounting plate (12) and the vacuum body (1), a plurality of clamping sleeve joints (17) are arranged at the bottom of the vacuum body (1), the clamping sleeve joints (17) extend to the lower portion of the bottom mounting plate (12), the vacuum exhaust tube (15) is connected with the clamping sleeve joints (17), and the inner wall of the probe water-cooling shell (16) is provided with an infrared temperature measuring probe (18) in threaded connection.
4. A multifunctional transient joule thermal reactor device according to claim 3 characterized by: probe water-cooling shell (16) outer wall symmetry is equipped with pagoda joint (19), current terminal (14) top run through in insulating fixed block (2) inner wall, current terminal (14) top with support copper billet (4) and connect, vacuum exhaust tube (15) outer wall is connected with KF16 vacuum tube (21) through cutting ferrule bend (20).
5. The multifunctional transient joule thermal reactor device of claim 1 wherein: the ceramic frame (5) is in threaded connection with the supporting and switching block (3), the electrode guide rail (6) is connected with the supporting and switching block (3) through a first bolt, and the electrode pressing sheet (8) is connected with the supporting frame (7) through a second bolt.
6. The multifunctional transient joule thermal reactor device of claim 1 wherein: the quartz glass slide (9) is movably connected with the support frame (7), the heating sheet (10) is movably connected with the quartz glass slide (9), and the electrode pressing sheet (8) is movably connected with the heating sheet (10).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221817333.XU CN218189558U (en) | 2022-07-14 | 2022-07-14 | Multifunctional transient Joule thermal reactor device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221817333.XU CN218189558U (en) | 2022-07-14 | 2022-07-14 | Multifunctional transient Joule thermal reactor device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218189558U true CN218189558U (en) | 2023-01-03 |
Family
ID=84650836
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202221817333.XU Expired - Fee Related CN218189558U (en) | 2022-07-14 | 2022-07-14 | Multifunctional transient Joule thermal reactor device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN218189558U (en) |
-
2022
- 2022-07-14 CN CN202221817333.XU patent/CN218189558U/en not_active Expired - Fee Related
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| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20230103 |