CN218157808U - Protection device of tail gas analysis instrument in chlorination process production - Google Patents

Protection device of tail gas analysis instrument in chlorination process production Download PDF

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Publication number
CN218157808U
CN218157808U CN202222168095.0U CN202222168095U CN218157808U CN 218157808 U CN218157808 U CN 218157808U CN 202222168095 U CN202222168095 U CN 202222168095U CN 218157808 U CN218157808 U CN 218157808U
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China
Prior art keywords
gas
tail gas
detected
liquid separator
tail
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CN202222168095.0U
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Chinese (zh)
Inventor
毋萧杰
任磊
齐满富
杨霄
邓世堂
张立东
刘森
张振华
张磊
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Henan Billions Advanced Material Co Ltd
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Henan Billions Advanced Material Co Ltd
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Abstract

The utility model discloses a protection device of a tail gas analysis instrument in chlorination production, which comprises a gas marking bottle, a gas-liquid separator, a drying device and a filtering device which are connected in sequence from the gas direction; the standard gas bottle is filled with a chlorine gas detection agent solution and is used for cooling the tail gas to be detected and detecting whether the tail gas to be detected contains chlorine gas; the gas-liquid separator is used for removing moisture in the tail gas to be detected from the standard gas bottle; the drying device is used for drying the tail gas to be detected from which the moisture is removed by the gas-liquid separator; and the filtering device is used for filtering and removing impurities from the dried tail gas to be detected. Through the utility model provides a protection device can avoid getting moisture, impurity in the tail gas that awaits measuring, get into analytical instrument including production material etc to reduce the damage that causes the instrument and meter, prolong analytical instrument's life.

Description

Protection device of tail gas analysis instrument in chlorination process production
Technical Field
The utility model belongs to the technical field of instrumentation, concretely relates to protection device of tail gas analysis instrument in chlorination process production.
Background
In the production process of titanium dioxide by chlorination method, CO/CO in chlorination tail gas 2 And O 2 The content control is an important index for controlling the chemical reaction in the chlorination furnace, which puts high requirements on the content measurement of the gas in the chlorination tail gas, and the used tail gas analysis instrument is expensive, so that the service life of the analysis instrument is prolonged while the measurement precision and stability are ensured, the stability of a production system can be increased to a great extent, and the cost can be saved. However, in actual production, the chlorinated tail gas is often directly conveyed to an analysis meter, which causes damage to a sensor of the analysis meter due to moisture and impurities contained in the measurement gas in the process of daily accumulation and long-term accumulation, and can directly cause damage in severe cases, thereby affecting the accuracy and stability of measurement.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide a protection device of a tail gas analysis instrument in the chlorination process production for overcoming the defects of the prior art.
The purpose of the utility model is realized by the following technical scheme:
a protection device of a tail gas analysis instrument in chlorination production comprises a standard gas bottle, a gas-liquid separator, a drying device and a filtering device which are sequentially connected in the gas direction;
a chlorine gas detection agent solution is contained in the standard gas bottle and is used for cooling the tail gas to be detected and detecting whether the tail gas to be detected contains chlorine gas or not;
the gas-liquid separator is used for removing moisture in the tail gas to be detected from the standard gas cylinder;
the drying device is used for drying the tail gas to be detected from which the moisture is removed by the gas-liquid separator;
and the filtering device is used for filtering and removing impurities from the dried tail gas to be detected.
Preferably, the gas marking bottle is provided with a first gas inlet pipe and a first gas outlet pipe, the first gas inlet pipe extends into the bottom of the chlorine gas detection agent solution, the gas outlet pipe is positioned at the top of the gas marking bottle, and the pipe orifice of the gas outlet pipe is positioned above the chlorine gas detection agent solution.
Preferably, the middle upper part of the gas-liquid separator is provided with a second air inlet pipe and a second air outlet pipe, and the bottom of the gas-liquid separator is provided with a sewage discharge pipeline and a sewage discharge valve.
Preferably, the drying device is filled with a color-changing drying agent.
Preferably, a metal filter element is arranged in the filter device.
Through the utility model provides a protection device can avoid getting moisture, impurity in the tail gas that awaits measuring, get into analytical instrument including production material etc to reduce the damage that causes the instrument and meter, prolong analytical instrument's life.
Drawings
FIG. 1 is a schematic diagram of a framework structure of a protective device of an exhaust gas analyzer in the chlorination process provided by the present application;
wherein, 1-mark gas cylinder; 2-a gas-liquid separator; 3-a blowdown valve; 4-a drying device; 5-a filtering device.
Detailed Description
The utility model provides a protection device of a tail gas analysis instrument in chlorination production, as shown in figure 1, comprising a gas marking bottle 1, a gas-liquid separator 2, a drying device 4 and a filtering device 5 which are connected in sequence from the gas coming direction;
the gas standard bottle 1 is internally provided with a chlorine gas detection agent solution, the chlorine gas detection agent solution is preferably a potassium iodide solution, tail gas to be detected firstly enters the gas standard bottle, is cooled by the chlorine gas detection agent solution, and meanwhile, when chlorine gas leaks from the chlorination furnace, the potassium iodide solution can timely detect the chlorine gas and generate color change so as to remind detection personnel to timely treat the problem of chlorine gas leakage from the chlorination furnace.
Preferably, a first air inlet pipe and a first air outlet pipe are arranged on the standard gas bottle, the first air inlet pipe extends into the bottom of the chlorine gas detection agent solution, the air outlet pipe is positioned at the top of the standard gas bottle, and the pipe opening of the air outlet pipe is positioned above the chlorine gas detection agent solution. The air inlet pipe is arranged deep to the bottom of the chlorine gas detection agent solution, so that the tail gas to be detected can be fully contacted with the chlorine gas detection agent solution, and the tail gas is fully cooled and whether the chlorine gas is contained or not is detected. And whether the sampling of the tail gas to be detected is smooth or not can be judged by observing the size and the speed of the bubbles in the chlorine gas detection agent solution.
The gas-liquid separator 2 is used for removing moisture in the tail gas to be detected from the standard gas bottle; preferably, the middle upper part of the gas-liquid separator is provided with a second air inlet pipe and a second air outlet pipe, and the bottom of the gas-liquid separator is provided with a sewage discharge pipeline and a sewage discharge valve 3.
The drying device 4 is used for drying the tail gas to be detected, the moisture of which is removed by the gas-liquid separator; preferably, the drying device intussuseption is filled with the drier that discolours, and the drier that discolours can demonstrate different colours according to different humidities, and convenient in time is changed. And the color-changing drying agent can be repeatedly recycled, so that the cost is saved.
And the filtering device 5 is used for filtering the dried tail gas to be detected to remove impurities in the tail gas to be detected, and preferably, a corrosion-resistant metal filter element is arranged in the filtering device.
When the utility model is used, the chlorination tail gas to be detected firstly enters the standard gas bottle, the potassium iodide liquid in the bottle firstly cools the tail gas, and whether the sampling gas is smooth or not is conveniently observed through the eyes of meat, and the color can be changed in time when the chlorination furnace is permeated with chlorine, so that the detection is convenient; then loop through gas-liquid separator and leave the moisture removal, through drying device further drying moisture removal, through the solid impurity in the filter equipment removal tail gas, carry into the instrument at last and carry out the content analysis, through this a series of processing, can avoid moisture, the impurity in the sample gas, get into analytical instrument including production material etc. to reduce the damage that causes analytical instrument, prolong analytical instrument's life.
While the preferred embodiments of the present invention have been described, additional variations and modifications in those embodiments may occur to those skilled in the art once they learn of the basic inventive concepts. It is therefore intended that the following appended claims be interpreted as including the preferred embodiment and all such alterations and modifications as fall within the scope of the invention. It will be apparent to those skilled in the art that various changes and modifications may be made without departing from the spirit and scope of the invention. Thus, if such modifications and variations of the present invention fall within the scope of the claims of the present invention and their equivalents, the present invention is also intended to include such modifications and variations.

Claims (5)

1. A protection device of a tail gas analysis instrument in chlorination production is characterized by comprising a standard gas bottle, a gas-liquid separator, a drying device and a filtering device which are sequentially connected in the gas direction;
a chlorine gas detection agent solution is contained in the standard gas bottle and is used for cooling the tail gas to be detected and detecting whether the tail gas to be detected contains chlorine gas or not;
the gas-liquid separator is used for removing moisture in the tail gas to be detected from the standard gas bottle;
the drying device is used for drying the tail gas to be detected from which the moisture is removed by the gas-liquid separator;
and the filtering device is used for filtering and removing impurities from the dried tail gas to be detected.
2. The protection device for the tail gas analyzer in the chlorination process production as claimed in claim 1,
the gas marking bottle is provided with a first gas inlet pipe and a first gas outlet pipe, the first gas inlet pipe extends into the bottom of the chlorine gas detection agent solution, the gas outlet pipe is located at the top of the gas marking bottle, and the pipe orifice of the gas outlet pipe is located above the chlorine gas detection agent solution.
3. The protection device for the tail gas analyzer in the chlorination process production as claimed in claim 1,
and the middle upper part of the gas-liquid separator is provided with a second air inlet pipe and a second air outlet pipe, and the bottom of the gas-liquid separator is provided with a sewage discharge pipeline and a sewage discharge valve.
4. The protection device for the tail gas analyzer in the chlorination process production as claimed in claim 1,
and the drying device is filled with a color-changing drying agent.
5. The protection device for the tail gas analyzer in the chlorination process production as claimed in claim 1,
and a metal filter element is arranged in the filtering device.
CN202222168095.0U 2022-08-17 2022-08-17 Protection device of tail gas analysis instrument in chlorination process production Active CN218157808U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202222168095.0U CN218157808U (en) 2022-08-17 2022-08-17 Protection device of tail gas analysis instrument in chlorination process production

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202222168095.0U CN218157808U (en) 2022-08-17 2022-08-17 Protection device of tail gas analysis instrument in chlorination process production

Publications (1)

Publication Number Publication Date
CN218157808U true CN218157808U (en) 2022-12-27

Family

ID=84551192

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202222168095.0U Active CN218157808U (en) 2022-08-17 2022-08-17 Protection device of tail gas analysis instrument in chlorination process production

Country Status (1)

Country Link
CN (1) CN218157808U (en)

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