CN218131907U - High-reporting device for chlorination decarboxylation reaction - Google Patents
High-reporting device for chlorination decarboxylation reaction Download PDFInfo
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- CN218131907U CN218131907U CN202222577775.8U CN202222577775U CN218131907U CN 218131907 U CN218131907 U CN 218131907U CN 202222577775 U CN202222577775 U CN 202222577775U CN 218131907 U CN218131907 U CN 218131907U
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Abstract
The utility model discloses a chlorination decarboxylation reaction height reports device, including the cauldron body, kettle cover, be equipped with row material pipe, control by temperature change probe on the cauldron body, the embedded hot plate that is provided with on the lateral wall of the cauldron body is provided with hot plate power supply on the hot plate, is provided with the controller on the outer wall of the cauldron body, is equipped with the buzzer siren on the controller, is provided with blast pipe, agitator motor on the kettle cover, feeding pipe, is provided with into tub valve on the feeding pipe, is equipped with the main shaft on the agitator motor, is equipped with the stirring vane on the main shaft, is equipped with the mixing hole on the stirring vane, turns over material piece, floor. Through setting up automatically controlled formula valve structure and buzzer siren, when the high temperature, can be timely will throw the pipe valve of advancing on the material pipe and close, avoid the carboxylic acid to continue to instil into reation kettle and cause the raw materials extravagant, reduce the cost in business, improved the degree of mixing of stirring structure between to carboxylic acid and relevant reactant, and then improved the reaction efficiency of chlorination decarboxylation.
Description
Technical Field
The utility model relates to a chlorination decarboxylation reaction technical field specifically is chlorination decarboxylation reaction height reports device.
Background
Most of the chlorination decarboxylation reactions belong to ionic reaction processes, and waste compounds can be utilized in a high-value mode through the decarboxylation reactions, so that the method is beneficial to development of new energy and environmental protection, and can be widely applied to the fields of chemical industry, biology, medicines, foods and the like.
The reaction of losing carboxyl in carboxylic acid molecule and releasing carbon dioxide is called chlorination decarboxylation reaction, a certain amount of soda lime is added in a reaction kettle in advance, then a heating plate is arranged on the side wall of the reaction kettle, liquid carboxylic acid is dripped in through a feeding pipe, and stirring and mixing are carried out simultaneously, so that the chlorination decarboxylation reaction is realized.
In the process of reaction, need monitor heating temperature, if the inside heater strip trouble of hot plate, heat all the time, the high temperature will cause the carbon chain fracture, influences normal chlorination decarboxylation reaction, consequently, can set up the height and report the device on reation kettle.
However, most of the existing high-report devices for chlorination and decarboxylation reactions do not have an electric control type valve structure, and when the temperature is too high, carboxylic acid is dripped into a reaction kettle, so that the waste of carboxylic acid raw materials is caused, and the enterprise cost is increased;
in addition, the mixing degree of the stirring structure for the carboxylic acid and related reactants is low, so that the reaction efficiency of chlorination and decarboxylation is reduced.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a chlorination decarboxylation reaction reports device to solve among the prior art carboxylic acid still instils into reation kettle and causes the waste of carboxylic acid raw materials and improved the cost of enterprise, because the stirring structure is lower and reduced the problem of chlorination decarboxylation's reaction efficiency to the degree of mixing between carboxylic acid and the relevant reactant.
In order to achieve the above purpose, the utility model provides a following technical scheme: chlorination decarboxylation reaction height reports device, including the cauldron body, kettle cover, be equipped with row material pipe, control by temperature change probe on the cauldron body, the embedded hot plate that is provided with on the lateral wall of the cauldron body, be provided with hot plate power supply on the hot plate, be provided with the controller on the outer wall of the cauldron body, be equipped with the buzzer siren on the controller, be provided with blast pipe, agitator motor, feeding pipe on the kettle cover, be provided with into pipe valve on the feeding pipe, the last main shaft that is equipped with of agitator motor, be equipped with the stirring vane on the main shaft, be equipped with the mixing hole on the stirring vane, turn over material piece, floor.
Preferably, the temperature control probe, the controller, the buzzer alarm, the pipe inlet valve, the stirring motor and the heating plate power supply are electrically connected, the model of the buzzer alarm is HRB-N80, the buzzer alarm can give out buzzing alarm sound, the warning efficiency of the high-altitude alarm device is improved, the pipe inlet valve is an electric control type pipeline valve, the model is XH-D971XP-16, and the electric control device is connected with the PLC in the controller through a lead, so that the PLC controls the pipe inlet valve and the pipe outlet valve to be opened and closed.
Preferably, the lower end face of the feeding pipe is not in contact with the stirring sheet, so that the stirring sheet rotating at a high speed is prevented from colliding with the feeding pipe.
Preferably, the heating plate is embedded in the side wall of the kettle body, the heating plate body is made of aluminum alloy and has excellent thermal conductivity, and the outer wall of the heating plate body is provided with a thermal insulation layer to avoid heat dissipation.
Preferably, the stirring piece is four of circumference range, the section of looking up of stirring piece is arc column structure, and agitator motor starts the back, can drive the main shaft clockwise rotation, and then drives the stirring piece clockwise rotation of arc column structure, realizes effectively stirring and mixes.
Preferably, the mixing holes are three groups which are transversely arranged, each group is seven which are vertically arranged and run through each stirring sheet, the turning sheets are two groups which are bilaterally symmetrical and are arranged on the side wall of each stirring sheet, each group of turning sheets is six which are vertically arranged and are staggered with the mixing holes, the turning sheets and the stirring sheets are made of forty-five steel materials, and the stirring holes are high-quality carbon structural steel and have higher strength and deformation resistance.
Preferably, the rib plates are triangular structural plates and are symmetrically arranged at corner connecting parts between each stirring piece and the main shaft, so that structural stability between the stirring pieces and the main shaft is improved.
Compared with the prior art, the beneficial effects of the utility model are that:
1. the utility model discloses a set up automatically controlled formula valve structure and buzzer siren, when the high temperature, the pipe valve that advances that will be timely on the feeding pipe is closed, avoids the carboxylic acid to continue to instil into reation kettle and cause the raw materials extravagant, has reduced cost in business.
2. The utility model discloses a stirring piece that has four arc column structures of circumference arrangement that sets up to set up mixing hole and stirring piece structure on the stirring piece, improved the degree of mixing of stirring structure between to carboxylic acid and relevant reactant, and then improved chlorination decarboxylation's reaction efficiency.
Drawings
FIG. 1 is a sectional view of the whole structure of the present invention;
fig. 2 is a bottom sectional view of the stirring plate structure with mixing holes and stirring plates in fig. 1 according to the present invention;
fig. 3 is a block diagram of the present invention.
In the figure: the device comprises a kettle body 1, a discharge pipe 11, a temperature control probe 12, a controller 2, a buzzer alarm 21, a kettle cover 3, an exhaust pipe 30, a stirring motor 31, a main shaft 32, a feeding pipe 4, a pipe inlet valve 41, a stirring sheet 5, a mixing hole 51, a material turning sheet 52, a rib plate 53, a heating plate 6 and a heating plate 61.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Example 1
Referring to fig. 1, 2 and 3, the chlorination and decarboxylation reaction high-grade newspaper device in the drawings comprises a kettle body 1 and a kettle cover 3, wherein a discharging pipe 11 and a temperature control probe 12 are arranged on the kettle body 1, a heating plate 6 is embedded in the side wall of the kettle body 1, a heating plate power supply 61 is arranged on the heating plate 6, a controller 2 is arranged on the outer wall of the kettle body 1, a buzzer alarm 21 is arranged on the controller 2, an exhaust pipe 30, a stirring motor 31 and a feeding pipe 4 are arranged on the kettle cover 3, a pipe feeding valve 41 is arranged on the feeding pipe 4, a main shaft 32 is arranged on the stirring motor 31, a stirring sheet 5 is arranged on the main shaft 32, and a mixing hole 51, a stirring sheet 52 and a rib plate 53 are arranged on the stirring sheet 5.
The buzzer alarm 21 is HRB-N80, and can give out a buzzer alarm sound, so that the warning efficiency of the high-speed alarm device is improved.
The pipe inlet valve 41 is an electric control type pipeline valve with the model number of XH-D971XP-16, and an electric control device of the pipe inlet valve is connected with a PLC in the controller 2 through a lead so as to realize the opening and closing by the PLC control.
The lower end surface of the feeding pipe 4 is not contacted with the stirring sheet 5, so that the collision of the stirring sheet 5 rotating at a high speed with the feeding pipe 4 is avoided.
The heating plate 6 is embedded in the side wall of the kettle body 1, a hollow cavity is formed in the heating plate 6, a dry-burning heating wire is arranged in the hollow cavity, and after the kettle is powered on, heating in the kettle body 1 is achieved.
The heating plate 6 body is made of aluminum alloy, has excellent thermal conductivity, and is provided with a thermal insulation layer on the outer wall thereof, so that heat is prevented from being dissipated outwards.
Four stirring pieces 5 are arranged circumferentially, the bottom cross section of each stirring piece 5 is an arc-shaped structure, referring to fig. 2, after the stirring motor 31 is started, the main shaft 32 is driven to rotate clockwise, and then the stirring pieces 5 with the arc-shaped structures are driven to rotate clockwise, so that effective stirring and mixing are realized.
The material mixing holes 51 are three groups which are transversely arranged, each group is seven which are vertically arranged and run through each stirring sheet 5, the material stirring sheets 52 are two groups which are bilaterally symmetrical and are arranged on the side wall of each stirring sheet 5, each group of material stirring sheets 52 is six which are vertically arranged and are arranged in a staggered mode with the material mixing holes 51, when the stirring sheets 5 rotate, carboxylic acid and related reaction raw materials can pass through the material mixing holes 51, further mixing and stirring are achieved, the material stirring sheets 52 are matched for stirring and mixing the reaction raw materials, and the degree of mixing of the stirring structure between the carboxylic acid and the related reaction materials is improved.
The mixing holes 51 are of a large size to allow the passage of the carboxylic acid and the associated reaction feed.
The material turning pieces 52 and the stirring pieces 5 are made of forty-five steel, are high-quality carbon structural steel and have higher strength and deformation resistance.
The rib plates 53 are triangular structural plates and symmetrically arranged at corner connecting parts between each stirring piece 5 and the main shaft 32, so that structural stability between the stirring pieces 5 and the main shaft 5 is improved.
The rib plate 53 is made of carbon fiber, has good anti-pulling capability and light weight, and has a triangular structure with high stability.
When used in this embodiment: the temperature control probe 12 can monitor the temperature in the kettle body 1 and transmit a temperature signal to a PLC in the controller 2 in real time through a signal wire,
if 6 inside heater strips of hot plate break down, heat always, when the temperature value in the cauldron body 1 is higher than when presetting the temperature value on the PLC in controller 2, PLC can be timely will throw material pipe 4 on advance tub valve 41 and close, PLC can close agitator motor 31 simultaneously and cut off hot plate power supply 61 to start buzzer siren 21 and report to the police the suggestion, avoid carboxylic acid to continue instil into cauldron body 1 and cause the raw materials extravagant, the cost of enterprise has been reduced.
In addition, when the chlorination and decarboxylation reaction is carried out, the stirring motor 31 is started, the stirring sheet 5 is driven to rotate at a high speed through the main shaft 32, the carboxylic acid and related reaction raw materials in the kettle body 1 can penetrate through the material mixing hole 51, further mixing and stirring are achieved, the stirring sheet 52 is matched for stirring and mixing the reaction raw materials, the mixing degree of the stirring structure for the carboxylic acid and the related reaction materials is improved, and further the chlorination and decarboxylation reaction efficiency is improved.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. Chlorination decarboxylation reaction high report device, characterized by, includes:
the kettle comprises a kettle body (1) and a kettle cover (3), wherein a discharging pipe (11) and a temperature control probe (12) are arranged on the kettle body (1), a heating plate (6) is embedded and arranged on the side wall of the kettle body (1), a heating plate power supply (61) is arranged on the heating plate (6), a controller (2) is arranged on the outer wall of the kettle body (1), a buzzer alarm (21) is arranged on the controller (2), an exhaust pipe (30), a stirring motor (31) and a feeding pipe (4) are arranged on the kettle cover (3), a feeding pipe valve (41) is arranged on the feeding pipe (4), a main shaft (32) is arranged on the stirring motor (31), stirring blades (5) are arranged on the main shaft (32), and a mixing hole (51), a stirring blade (52) and a rib plate (53) are arranged on the stirring blade (5).
2. The chlorination decarboxylation reaction reporting apparatus according to claim 1, wherein: the temperature control probe (12), the controller (2), the buzzer alarm (21), the pipe inlet valve (41), the stirring motor (31) and the heating plate power supply (61) are electrically connected.
3. The chlorination decarboxylation reaction reporting apparatus according to claim 1, wherein: the lower end surface of the feeding pipe (4) is not contacted with the stirring sheet (5).
4. The chlorination decarboxylation reaction reporting apparatus according to claim 1, wherein: the heating plate (6) is embedded in the side wall of the kettle body (1).
5. The Chlorination decarboxylation reaction high report device of claim 1, characterized in that: the stirring pieces (5) are four in circumferential arrangement, and the upward-looking cross section of each stirring piece (5) is of an arc-shaped structure.
6. The Chlorination decarboxylation reaction high report device of claim 1, characterized in that: the mixing holes (51) are arranged in three groups in a transverse mode, each group is seven and penetrates through each stirring sheet (5), the turning sheets (52) are arranged in two groups in bilateral symmetry and are arranged on the side wall of each stirring sheet (5), and each group of turning sheets (52) is six and is arranged in a vertical mode and staggered with the mixing holes (51).
7. The chlorination decarboxylation reaction reporting apparatus according to claim 1, wherein: the rib plates (53) are triangular structural plates and are symmetrically arranged at corner connecting parts between each stirring sheet (5) and the main shaft (32).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222577775.8U CN218131907U (en) | 2022-09-28 | 2022-09-28 | High-reporting device for chlorination decarboxylation reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222577775.8U CN218131907U (en) | 2022-09-28 | 2022-09-28 | High-reporting device for chlorination decarboxylation reaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218131907U true CN218131907U (en) | 2022-12-27 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202222577775.8U Active CN218131907U (en) | 2022-09-28 | 2022-09-28 | High-reporting device for chlorination decarboxylation reaction |
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| Country | Link |
|---|---|
| CN (1) | CN218131907U (en) |
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- 2022-09-28 CN CN202222577775.8U patent/CN218131907U/en active Active
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