CN218012770U - Airflow stirring type molecular sieve synthesis reaction kettle - Google Patents

Airflow stirring type molecular sieve synthesis reaction kettle Download PDF

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Publication number
CN218012770U
CN218012770U CN202222189842.9U CN202222189842U CN218012770U CN 218012770 U CN218012770 U CN 218012770U CN 202222189842 U CN202222189842 U CN 202222189842U CN 218012770 U CN218012770 U CN 218012770U
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air
fixedly connected
wall
molecular sieve
reaction kettle
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CN202222189842.9U
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章芬
胡银
陈伟
王玲玲
韩飞
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Institute of Applied Chemistry Jiangxi Academy of Sciences
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Institute of Applied Chemistry Jiangxi Academy of Sciences
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Abstract

The utility model discloses an air current stirring formula molecular sieve synthesis reation kettle relates to the synthetic technical field of molecular sieve, comprising a main body, the outside fixedly connected with heating device of main part, heating device's outer wall fixedly connected with support, the top fixedly connected with monitoring devices of main part, the bottom fixedly connected with air jet system of main part, one side of air jet system is provided with the discharge gate. The utility model discloses a metal heating rod generates heat and heats equipment internal temperature, the barometer can show inside atmospheric pressure, inside atmospheric pressure can be opened if too high one-way air outlet valve and is discharged and keep near needs numerical value with control internal pressure, if the preparation is ended, can open the snuffle valve and lose heart, the air can spout equipment through the air cock through air compressor's compression inside, the gas that spouts forms the cyclone, with this stirring internal reaction material, air compressor spouts gaseous also can guarantee inside atmospheric pressure needs simultaneously.

Description

Airflow stirring type molecular sieve synthesis reaction kettle
Technical Field
The utility model relates to a molecular sieve synthesis technical field, concretely relates to air current stirring formula molecular sieve synthesis reation kettle.
Background
Molecular sieves are aluminosilicate compounds having a cubic lattice. The molecular sieve has a uniform microporous structure, the diameter of the pores is uniform, the pores can adsorb molecules smaller than the diameter of the pores and have preferential adsorption capacity for polar molecules and unsaturated molecules, so that the molecular sieve can separate the molecules with different polarity degrees, saturation degrees, molecular sizes and boiling points, namely has the function of sieving the molecules, so the molecular sieve is called, and has the advantages of high adsorption capacity, high thermal stability and the like which are not possessed by other adsorbents, so the molecular sieve is widely applied, the preparation of the molecular sieve is rapidly developed in the year, and most processes gradually replace manual work by machines. The following problems exist in the prior art:
1. in the existing airflow stirring type molecular sieve synthesis reaction kettle, the traditional high-pressure reaction kettle is a mechanical stirring type or an electromagnetic lifting stirring type, the phenomena of leakage, blockage and the like are easily generated in the working process, and the stirring efficiency is not high;
2. the existing airflow stirring type molecular sieve synthesis reaction kettle has a complex internal structure and a single function, and is high in failure rate and inconvenient to maintain.
SUMMERY OF THE UTILITY MODEL
In order to solve the technical problem, the utility model discloses the technical scheme who adopts is:
an airflow stirring type molecular sieve synthesis reaction kettle comprises a main body, wherein a heating device is fixedly connected to the outer side of the main body, a support is fixedly connected to the outer wall of the heating device, a monitoring device is fixedly connected to the upper part of the main body, an air injection device is fixedly connected to the bottom of the main body, and a discharge hole is formed in one side of the air injection device; the heating device comprises a heat preservation shell, the outer wall of the heat preservation shell is fixedly connected with the inner wall of the support, the outer wall of the heat preservation shell is provided with a screen, the inner wall of the heat preservation shell is provided with a metal heating rod, and the outer wall of the metal heating rod is provided with a limiting ring; monitoring devices is including the barometer, the bottom of barometer and the top fixed connection of main part, one side of barometer is provided with the thermometer, one side of thermometer is provided with the feed inlet, one side of feed inlet is provided with one-way air outlet valve, one side of one-way air outlet valve is provided with the release valve.
The utility model discloses technical scheme's further improvement lies in: the outer wall of heat preservation shell and the inner wall fixed connection of screen, the inner wall and the metal heating rod fixed connection of heat preservation shell, the outer wall of metal heating rod and one side fixed connection of spacing ring.
The utility model discloses technical scheme's further improvement lies in: one side of the barometer is fixedly connected with the air temperature meter, and one side of the air temperature meter is fixedly connected with the feeding hole.
The utility model discloses technical scheme's further improvement lies in: one side and the one-way air outlet valve fixed connection of feed inlet, one side and the snuffle valve fixed connection of one-way air outlet valve.
The utility model discloses technical scheme's further improvement lies in: the air injection device comprises a fixer, the outer wall of the fixer is fixedly connected with the bottom of the main body, an air injection head is arranged above the fixer, and an air faucet is arranged above the air injection head.
The utility model discloses technical scheme's further improvement lies in: an air compressor is arranged below the fixer, and an air inlet is arranged below the air compressor.
The utility model discloses technical scheme's further improvement lies in: the top of fixer is provided with the jet head, the top of jet head is provided with the air cock, the below of fixer is provided with air compressor, air compressor's below is provided with the air inlet.
Owing to adopted above-mentioned technical scheme, the utility model discloses relative prior art, the technological progress who gains is:
1. the utility model provides an air current stirring formula molecular sieve synthesis reation kettle, under the combined action through heat preservation shell, screen, metal heating rod, spacing ring, generate heat through the metal heating rod and heat the inside temperature of equipment, heat preservation shell parcel metal heating rod can furthest with heat transfer to inside, it is extravagant to reduce production, protected the screen of heat preservation shell outside simultaneously, can show and control inside temperature on the screen to in preparation different molecular sieve's needs.
2. The utility model provides an air current stirring formula molecular sieve synthesis reation kettle, under the combined action through barometer, air temperature table, one-way air outlet valve, release valve, feed inlet, the barometer can show inside atmospheric pressure, inside atmospheric pressure if too high one-way air outlet valve can be opened and is discharged and keep near needs numerical value with control inside pressure, if the preparation is over, can open release valve and lose heart, make inside atmospheric pressure resume normally to guarantee preparation personnel's safety.
3. The utility model provides an air current stirring formula molecular sieve synthesis reation kettle, under the combined action through air compressor, fixer, jet head, air cock, air inlet, the air gets into air compressor through the air inlet, inside compressed air through air compressor can spout equipment through the air cock, the angle of jet head is not perpendicular upwards, can let the gas of spouting form the cyclone to this stirring inside reaction material, air compressor spouts gaseous atmospheric pressure needs that also can guarantee inside simultaneously.
Drawings
FIG. 1 is a schematic structural diagram of an air-flow stirring type molecular sieve synthesis reaction kettle of the present invention;
fig. 2 is a schematic structural view of the heating device of the present invention;
fig. 3 is a schematic structural view of the monitoring device of the present invention;
fig. 4 is a schematic structural view of the air injection device of the present invention.
In the figure: 1. a main body; 2. a heating device; 3. a support; 4. a monitoring device; 5. a discharge port; 6. an air injection device; 21. a heat preservation shell; 22. a screen; 23. a metal heating rod; 24. a limiting ring; 41. a barometer; 42. an air temperature table; 43. a one-way air outlet valve; 44. a gas release valve; 45. a feed inlet; 61. an air compressor; 62. a holder; 63. a gas ejection head; 64. an air faucet; 65. an air inlet.
Detailed Description
The present invention will be described in further detail with reference to the following examples:
example 1
As shown in fig. 1-4, the utility model provides an air stirring type molecular sieve synthesis reaction kettle, which comprises a main body 1, wherein a heating device 2 is fixedly connected to the outer side of the main body 1, a support 3 is fixedly connected to the outer wall of the heating device 2, a monitoring device 4 is fixedly connected to the upper side of the main body 1, an air injection device 6 is fixedly connected to the bottom of the main body 1, and a discharge port 5 is arranged on one side of the air injection device 6; the heating device 2 comprises a heat preservation shell 21, the outer wall of the heat preservation shell 21 is fixedly connected with the inner wall of the support 3, the outer wall of the heat preservation shell 21 is provided with a screen 22, the inner wall of the heat preservation shell 21 is provided with a metal heating rod 23, and the outer wall of the metal heating rod 23 is provided with a limiting ring 24; the monitoring device 4 comprises a barometer 41, the bottom of the barometer 41 is fixedly connected with the top of the main body 1, one side of the barometer 41 is provided with a thermometer 42, one side of the thermometer 42 is provided with a feeding hole 45, one side of the feeding hole 45 is provided with a one-way air outlet valve 43, and one side of the one-way air outlet valve 43 is provided with an air release valve 44.
Example 2
As shown in fig. 1-4, on the basis of embodiment 1, the utility model provides a technical solution: preferably, the heating device 2 comprises a heat preservation shell 21, the outer wall of the heat preservation shell 21 is fixedly connected with the inner wall of the support 3, the outer wall of the heat preservation shell 21 is fixedly connected with the inner wall of the screen 22, the inner wall of the heat preservation shell 21 is fixedly connected with the metal heating rod 23, and the outer wall of the metal heating rod 23 is fixedly connected with one side of the limiting ring 24.
In this embodiment, generate heat through metal heating rod 23 and heat the inside temperature of equipment, heat preservation shell 21 parcel metal heating rod 23 can furthest with heat transfer to inside, reduce the production waste, protected the screen 22 of heat preservation shell 21 outside simultaneously, can show and control inside temperature on the screen 22 to in preparation different molecular sieve's needs.
Example 3
As shown in fig. 1-4, on the basis of embodiment 1, the utility model provides a technical solution: preferably, the monitoring device 4 comprises a barometer 41, the bottom of the barometer 41 is fixedly connected with the top of the main body 1, one side of the barometer 41 is fixedly connected with the thermometer 42, one side of the thermometer 42 is fixedly connected with a feed port 45, one side of the feed port 45 is fixedly connected with a one-way air outlet valve 43, and one side of the one-way air outlet valve 43 is fixedly connected with an air release valve 44.
In this embodiment, the barometer 41 can display the internal air pressure, if the internal air pressure is too high, the one-way air outlet valve 43 is opened to exhaust air to control the internal pressure to be kept near a required value, and if the preparation is finished, the air release valve 44 is opened to release air, so that the internal air pressure is restored to normal, and the safety of the preparation personnel is ensured.
Example 4
As shown in fig. 1-4, on the basis of embodiment 1, the utility model provides a technical solution: preferably, the air injection device 6 comprises a holder 62, the outer wall of the holder 62 is fixedly connected with the bottom of the main body 1, an air injection head 63 is arranged above the holder 62, an air nozzle 64 is arranged above the air injection head 63, an air compressor 61 is arranged below the holder 62, and an air inlet 65 is arranged below the air compressor 61.
In this embodiment, air enters the air compressor 61 through the air inlet 65, and the compressed air passing through the air compressor 61 can be sprayed into the interior of the equipment through the air nozzle 64, and the angle of the air spraying head 63 is not vertical upward, so that the sprayed gas can form a cyclone, thereby stirring the internal reaction material, and meanwhile, the air pressure requirement of the interior can also be ensured by the sprayed gas from the air compressor 61.
The working principle of the gas flow stirring type molecular sieve synthesis reaction kettle is described in detail below.
As shown in fig. 1-4, the metal heating rod 23 heats the internal temperature of the device, the heat preservation shell 21 wraps the metal heating rod 23 to transfer heat to the inside to the maximum extent, thereby reducing production waste, and simultaneously protecting the screen 22 outside the heat preservation shell 21, the temperature inside the device can be displayed and controlled on the screen 22, so as to meet the requirements of preparing different molecular sieves, the air pressure gauge 41 can display the internal air pressure, if the internal air pressure is too high, the one-way air outlet valve 43 can be opened to exhaust air so as to control the internal pressure to be kept near a required value, if the preparation is finished, the air escape valve 44 can be opened to release air, so that the internal air pressure is recovered to ensure the safety of preparation personnel, the air enters the air compressor 61 through the air inlet 65, the compressed air passing through the air compressor 61 can be sprayed into the device through the air nozzle 64, the angle of the air nozzle 63 is not vertically upward, the sprayed air can form a cyclone, so as to stir the internal reaction materials, and meanwhile, the air sprayed by the air compressor 61 can also ensure the internal air pressure requirements.
The present invention has been described in detail with reference to the above general description, but it will be apparent to one of ordinary skill in the art that modifications and improvements can be made to the invention. Therefore, modifications or improvements without departing from the spirit of the invention are within the scope of the invention.

Claims (7)

1. The utility model provides a synthetic reation kettle of air current stirring formula molecular sieve, includes main part (1), its characterized in that: the outer side of the main body (1) is fixedly connected with a heating device (2), the outer wall of the heating device (2) is fixedly connected with a support (3), a monitoring device (4) is fixedly connected above the main body (1), the bottom of the main body (1) is fixedly connected with an air injection device (6), and one side of the air injection device (6) is provided with a discharge hole (5);
the heating device (2) comprises a heat-insulating shell (21), the outer wall of the heat-insulating shell (21) is fixedly connected with the inner wall of the support (3), the outer wall of the heat-insulating shell (21) is provided with a screen (22), the inner wall of the heat-insulating shell (21) is provided with a metal heating rod (23), and the outer wall of the metal heating rod (23) is provided with a limiting ring (24);
monitoring devices (4) are including barometer (41), the bottom of barometer (41) and the top fixed connection of main part (1), one side of barometer (41) is provided with air temperature table (42), one side of air temperature table (42) is provided with feed inlet (45), one side of feed inlet (45) is provided with one-way air outlet valve (43), one side of one-way air outlet valve (43) is provided with release valve (44).
2. The gas flow stirring type molecular sieve synthesis reaction kettle of claim 1, wherein: the outer wall of heat preservation shell (21) and the inner wall fixed connection of screen (22), the inner wall and the metal heating rod (23) fixed connection of heat preservation shell (21), the outer wall of metal heating rod (23) and one side fixed connection of spacing ring (24).
3. The gas flow stirring type molecular sieve synthesis reaction kettle of claim 1, wherein: one side of the air pressure gauge (41) is fixedly connected with an air temperature gauge (42), and one side of the air temperature gauge (42) is fixedly connected with the feed inlet (45).
4. The gas flow stirring type molecular sieve synthesis reaction kettle according to claim 3, wherein: one side and one-way air outlet valve (43) fixed connection of feed inlet (45), one side and release valve (44) fixed connection of one-way air outlet valve (43).
5. The gas flow stirring type molecular sieve synthesis reaction kettle of claim 1, wherein: the air injection device (6) comprises a fixer (62), the outer wall of the fixer (62) is fixedly connected with the bottom of the main body (1), an air injection head (63) is arranged above the fixer (62), and an air nozzle (64) is arranged above the air injection head (63).
6. The gas flow stirring type molecular sieve synthesis reaction kettle of claim 5, wherein: an air compressor (61) is arranged below the fixer (62), and an air inlet (65) is arranged below the air compressor (61).
7. The gas flow stirring type molecular sieve synthesis reaction kettle of claim 6, wherein: the top of fixer (62) is provided with jet head (63), the top of jet head (63) is provided with air cock (64), the below of fixer (62) is provided with air compressor (61), the below of air compressor (61) is provided with air inlet (65).
CN202222189842.9U 2022-08-19 2022-08-19 Airflow stirring type molecular sieve synthesis reaction kettle Active CN218012770U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202222189842.9U CN218012770U (en) 2022-08-19 2022-08-19 Airflow stirring type molecular sieve synthesis reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202222189842.9U CN218012770U (en) 2022-08-19 2022-08-19 Airflow stirring type molecular sieve synthesis reaction kettle

Publications (1)

Publication Number Publication Date
CN218012770U true CN218012770U (en) 2022-12-13

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CN202222189842.9U Active CN218012770U (en) 2022-08-19 2022-08-19 Airflow stirring type molecular sieve synthesis reaction kettle

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