CN217854637U - Sublimation device - Google Patents
Sublimation device Download PDFInfo
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- CN217854637U CN217854637U CN202220973792.0U CN202220973792U CN217854637U CN 217854637 U CN217854637 U CN 217854637U CN 202220973792 U CN202220973792 U CN 202220973792U CN 217854637 U CN217854637 U CN 217854637U
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- reactor
- cooling tube
- bottle body
- sublimation
- bottle
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Abstract
The utility model discloses a sublimation device, which relates to the technical field of chemical experimental apparatus and comprises a reactor, a bottle stopper which can be connected with the bottle mouth in a sealing way, a cooling pipe which can partially pass through the bottle stopper and extend into the reactor, a vacuum exhaust pipe which is used for connecting and communicating with a suction device and a collecting tray which is used for collecting falling materials, wherein the reactor is provided with a bottle mouth; the vacuum suction pipe can penetrate through the bottle stopper and is communicated with the interior of the reactor, and a switch valve is arranged on the vacuum suction pipe; the collecting tray is located inside the reactor and can be suspended below the cooling tubes. Therefore, the utility model provides a sublimation device can improve product ejection of compact yield.
Description
Technical Field
The utility model relates to a chemistry experiment utensil technical field especially relates to a sublimation device.
Background
Sublimation refers to the process of changing a solid material into a gas without passing through the liquid. Some substances have a relatively high vapor pressure in the solid state and, when heated, change directly to the gaseous state without passing through the liquid state, a process known as sublimation. Sublimable substances can be separated from non-sublimable substances by means of a sublimation process, or a mixture of solids of different volatility can be separated. The sublimator utilizes the sublimation principle and is commonly used for producing chemical raw materials with higher purity requirements in the technical field of chemical raw material production. Present ordinary sublimator, the bottleneck is less, and the sublimation cavity is great, and product ejection of compact process material after the sublimation is run into the bottleneck and is easily dropped, leads to the loss product, accomplishes sublimator bottom material after the sublimation simultaneously and is difficult to the clearance.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing a sublime device to solve the problem that above-mentioned prior art exists, can improve product ejection of compact yield.
In order to achieve the above object, the utility model provides a following scheme:
the utility model provides a sublimation device, which comprises a reactor, a bottle stopper which can be connected with the bottle mouth in a sealing way, a cooling pipe which can partially pass through the bottle stopper and extend to the inside of the reactor, a vacuum exhaust pipe which is used for being connected and communicated with a suction device and a collecting tray which is used for collecting falling materials, wherein the reactor is provided with a bottle mouth; the vacuum suction pipe can penetrate through the bottle stopper and is communicated with the interior of the reactor, and a switch valve is arranged on the vacuum suction pipe; the collection tray is located inside the reactor and is capable of being suspended below the cooling tubes.
Preferably, the reactor is a long-neck ball bottle.
Preferably, the reactor comprises an upper bottle body and a lower bottle body, the upper bottle body is detachably connected to the lower bottle body in a sealing manner, and the collecting tray is fixedly connected with the upper bottle body.
Preferably, a sealing ring is arranged at the joint of the upper bottle body and the lower bottle body.
Preferably, the collecting tray further comprises a plurality of connecting pieces, one end of each connecting piece is fixedly connected with the inner wall of the upper bottle body, and the other end of each connecting piece is fixedly connected with the collecting tray.
Preferably, the cooling pipe is including outer cooling tube and the inlayer cooling tube that is linked together, outer cooling tube is located the inlayer cooling tube outside, outer cooling tube can pass the bottle plug extends inside the reactor, the coolant liquid import has been seted up on the inlayer cooling tube, the coolant liquid export has been seted up on the outer cooling tube.
The utility model discloses for prior art gain following technological effect:
the utility model provides a sublimation device through set up the catch tray in the cooling tube below, can collect the material that drops on the cooling tube, avoids the material to fall into the reactor bottom again and causes the product loss, sets up the material that the catch tray dropped on to the cooling tube simultaneously and collects, can increase the volume of throwing with volume reactor single raw materials volume of adding. Therefore, the utility model provides a sublimation device can improve product ejection of compact yield.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required to be used in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without creative efforts.
Fig. 1 is a schematic structural view of a sublimation apparatus provided by the present invention;
in the figure: 100-a sublimation device; 1-a reactor; 11-feeding the bottle body; 12-dropping the bottle body; 13-bottle mouth; 2-bottle stopper; 3-a cooling pipe; 31-outer cooling pipe; 311-coolant outlet; 32-inner layer cooling tube; 321-a coolant inlet; 4-vacuum exhaust tube; 41-a switch valve; 5-collecting a tray; 6-connecting piece.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
The utility model aims at providing a sublime device to solve the problem that prior art exists, can improve product ejection of compact yield.
In order to make the aforementioned objects, features and advantages of the present invention more comprehensible, the present invention is described in detail with reference to the accompanying drawings and the following detailed description.
The utility model provides a sublimation device 100, as shown in fig. 1, in the embodiment, the sublimation device comprises a reactor 1, a bottle stopper 2 capable of being hermetically connected to a bottle mouth 13, a cooling pipe 3 capable of partially passing through the bottle stopper 2 and extending into the reactor 1, a vacuum pumping pipe 4 connected and communicated with a suction device, and a collecting tray 5 for collecting falling materials, wherein the reactor 1 is provided with a bottle mouth 13; the vacuum pumping tube 4 can penetrate through the bottle stopper 2 and is communicated with the interior of the reactor 1, and a switch valve 41 is arranged on the vacuum pumping tube; a collecting tray 5 is located inside the reactor 1, which collecting tray 5 can be suspended below the cooling tubes 3.
Through setting up catch tray 5 in cooling tube 3 below, can collect the material that drops on cooling tube 3, avoid the material to fall into 1 bottom of reactor again and cause the product loss, set up catch tray 5 simultaneously and collect the material that drops on cooling tube 3, can increase 1 single raw materials input volume with volume reactor, further improved product material yield.
The reactor 1 is a long-neck ball bottle.
Reactor 1 includes upper flask 11 and lower flask 12, and the sealing connection that upper flask 11 can be dismantled is on lower flask 12, and collecting tray 5 and upper flask 11 fixed connection pull down upper flask 11 from lower flask 12, can be convenient for clear up the solid residue of bottom in lower flask 12.
The joint of the upper bottle body 11 and the lower bottle body 12 is provided with a sealing ring to prevent external gas from entering the reactor 1 and simultaneously avoid gas overflow in the reactor 1.
The utility model discloses an among the alternative, comparatively preferably, sublimation device 100 still includes a plurality of connecting pieces 6, and connecting piece 6 is preferably the connecting rod, and each connecting piece 6 equal one end and the 11 inner wall fixed connection of last bottle, the other end of each connecting piece 6 all with 5 fixed connection of catch tray to make 5 suspension of catch tray in cooling tube 3 below.
The utility model discloses a concrete example is applied to explain the principle and the implementation mode of the utility model, and the explanation of the above example is only used to help understand the method and the core idea of the utility model; meanwhile, for the general technical personnel in the field, according to the idea of the present invention, there are changes in the concrete implementation and the application scope. In summary, the content of the present specification should not be construed as a limitation of the present invention.
Claims (6)
1. A sublimation apparatus, characterized in that: the method comprises the following steps:
a reactor having a mouth;
the bottle stopper can be connected to the bottle opening in a sealing mode;
a cooling tube capable of partially passing through the stopper and extending into the reactor interior;
the vacuum pumping pipe is used for being connected and communicated with a pumping device, can penetrate through the bottle stopper and is communicated with the interior of the reactor, and a switch valve is arranged on the vacuum pumping pipe;
and a collection tray for collecting the falling material, the collection tray being located inside the reactor, the collection tray being capable of being suspended below the cooling tubes.
2. Sublimation apparatus according to claim 1, wherein: the reactor is a long-neck ball bottle.
3. Sublimation device according to claim 2, wherein: the reactor comprises an upper bottle body and a lower bottle body, the upper bottle body is detachably connected to the lower bottle body in a sealing mode, and the collecting disc is fixedly connected with the upper bottle body.
4. Sublimation apparatus according to claim 3, wherein: and a sealing ring is arranged at the joint of the upper bottle body and the lower bottle body.
5. Sublimation device according to claim 3, wherein: the collecting tray is characterized by further comprising a plurality of connecting pieces, one end of each connecting piece is fixedly connected with the inner wall of the upper bottle body, and the other end of each connecting piece is fixedly connected with the collecting tray.
6. Sublimation device according to claim 1, wherein: the cooling tube is including outer cooling tube and the inlayer cooling tube that is linked together, outer cooling tube is located the inlayer cooling tube outside, outer cooling tube can pass the bottle plug extends inside the reactor, the coolant liquid import has been seted up on the inlayer cooling tube, the coolant liquid export has been seted up on the outer cooling tube.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202220973792.0U CN217854637U (en) | 2022-04-25 | 2022-04-25 | Sublimation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202220973792.0U CN217854637U (en) | 2022-04-25 | 2022-04-25 | Sublimation device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN217854637U true CN217854637U (en) | 2022-11-22 |
Family
ID=84087310
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202220973792.0U Active CN217854637U (en) | 2022-04-25 | 2022-04-25 | Sublimation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN217854637U (en) |
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2022
- 2022-04-25 CN CN202220973792.0U patent/CN217854637U/en active Active
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| Date | Code | Title | Description |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: 052165 Jinsha Road, economic and Technological Development Zone, Shijiazhuang City, Hebei Province Patentee after: Hebei Haili Hengyuan New Material Co.,Ltd. Address before: 052165 No. 2 Jinsha Road, economic and Technological Development Zone, Shijiazhuang City, Hebei Province Patentee before: HEBEI HAILI FRAGRANCES CO.,LTD. |
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| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20230525 Address after: 050000, 200 meters east of the intersection of Industrial Street and Huahua North Road in the Circular Chemical Industry Park of Shijiazhuang City, Hebei Province Patentee after: Hebei Dongli New Material Co.,Ltd. Address before: 052165 Jinsha Road, economic and Technological Development Zone, Shijiazhuang City, Hebei Province Patentee before: Hebei Haili Hengyuan New Material Co.,Ltd. |