CN217473538U

CN217473538U - Sulfonation reaction kettle capable of controlling temperature

Info

Publication number: CN217473538U
Application number: CN202221620140.5U
Authority: CN
Inventors: 于俊俊; 姚小龙
Original assignee: Laizhou Jinxing Chemical Co ltd
Current assignee: Laizhou Jinxing Chemical Co ltd
Priority date: 2022-06-27
Filing date: 2022-06-27
Publication date: 2022-09-23
Anticipated expiration: 2032-06-27

Abstract

The utility model discloses a sulfonation reaction cauldron of steerable temperature belongs to reation kettle technical field, including braced frame, braced frame's top fixedly connected with bracing piece, the top fixedly connected with reation kettle body of bracing piece, the top fixedly connected with unloading pipe of reation kettle body, the bottom fixedly connected with unloading pipe of reation kettle body, be provided with the valve on the unloading pipe, the logical groove of slip has been seted up to braced frame's side, it is provided with folding assembly to slide to lead to the inslot, a plurality of filter screen poles of fixedly connected with between the folding assembly at symmetric state, network structure is constituteed to a plurality of filter screen poles, braced frame's bottom fixedly connected with supporting leg. The utility model discloses a be provided with braced frame, folding assembly, filter screen pole, nut piece and two-way screw rod, can adjust the clearance between the filter screen pole, and then the network structure's that the adjustment filter screen pole is constituteed filter fineness, and the convenience is filtered the impurity of equidimension not.

Description

Sulfonation reaction kettle capable of controlling temperature

Technical Field

The utility model relates to a reation kettle technical field especially relates to the sulfonation reaction cauldron of steerable temperature.

Background

Tobias acid, a white needle crystal, slightly soluble in cold water, soluble in hot water, very slightly soluble in ethanol and ether, and its sodium and ammonium salts are very soluble in water.

The preparation of tobias acid needs to go on in the controllable reation kettle of temperature, and tobias acid need add multiple reactant one by one in the preparation process, every adds a reactant, just can produce a chemical reaction and produce impurity in the reation kettle, the impurity particle that different reactant reaction produced is not of uniform size, in order to avoid impurity to cause the influence to the product that the reaction obtained each time, all can filter the impurity in the gained thing after chemical reaction each time, filter screen structure in the controllable reation kettle of current temperature is comparatively simple, only can filter an impurity, filter the filter screen of different precision need be changed to every filtration, thereby make filtering operation become loaded down with trivial details, influence the preparation efficiency of tobias acid, consequently, the sulfonation reaction cauldron of a steerable temperature is proposed and the above-mentioned problem is solved.

SUMMERY OF THE UTILITY MODEL

The utility model aims at solving the problems in the prior art and providing a sulfonation reaction kettle capable of controlling the temperature.

In order to realize the purpose, the utility model adopts the following technical scheme:

temperature-controllable's sulfonation reaction cauldron, including braced frame, braced frame's top fixedly connected with bracing piece, the top fixedly connected with reation kettle body of bracing piece, the top fixedly connected with unloading pipe of reation kettle body, the bottom fixedly connected with unloading pipe of reation kettle body, be provided with the valve on the unloading pipe, the logical groove of sliding has been seted up to braced frame's side, the logical inslot of sliding is provided with folding assembly, is in a plurality of filter screen poles of fixedly connected with between the folding assembly of symmetric state, and is a plurality of the network structure is constituteed to the filter screen pole, braced frame's bottom fixedly connected with supporting leg.

Preferably, the through hole has been seted up in the top center department of reation kettle body, the top of reation kettle body is provided with agitator motor, agitator motor's fixed surface is connected with the collar, fixedly connected with locating lever between the collar and the top of reation kettle body.

Preferably, the output end of the stirring motor is fixedly connected with a driving shaft, one end of the driving shaft penetrates through the through hole and extends into the reaction kettle body, and the surface of the driving shaft is fixedly connected with a stirring rod.

Preferably, the folding assembly comprises a connecting channel steel which is connected in the sliding through groove in a sliding mode and a transmission rod which is connected in the connecting channel steel in a rotating mode.

Preferably, the transmission rods in the same connecting channel steel are V-shaped, and the adjacent transmission rods are in rotary connection.

Preferably, one side of the supporting frame is located on two sides of the folding assembly and is connected with a nut block in a sliding mode, a transfer groove is formed in one side of the nut block, and the transfer groove is connected with the transmission rod on the outermost side in a rotating mode.

Preferably, the nut block is internally and threadedly connected with a bidirectional screw, and one end of the bidirectional screw is fixedly connected with a knob.

Compared with the prior art, the beneficial effects of the utility model are that:

1. the utility model discloses a be provided with agitator motor, drive shaft and puddler, can realize this internal stirring function of reactant of reation kettle to accelerate the reaction rate of reactant.

2. The utility model discloses a be provided with braced frame, folding assembly, filter screen pole, nut piece and two-way screw rod, can adjust the clearance between the filter screen pole, and then the network structure's that the adjustment filter screen pole is constituteed filter fineness, and the convenience is filtered the impurity of equidimension not.

Drawings

FIG. 1 is a schematic view of a three-dimensional structure of a temperature-controllable sulfonation reaction kettle according to the present invention;

FIG. 2 is a schematic view of the internal structure of the reaction kettle in the temperature-controllable sulfonation reaction kettle of the present invention;

fig. 3 is a schematic view of a connection structure of a folding component and a filter rod in the temperature-controllable sulfonation reaction kettle of the present invention;

fig. 4 is an enlarged schematic structural diagram of a position a in the sulfonation reaction kettle with controllable temperature according to the present invention.

In the figure: 1. a support frame; 101. a sliding through groove; 2. a transmission rod; 3. a support bar; 4. a screen rod; 5. supporting legs; 6. a discharging pipe; 7. a stirring motor; 8. a reaction kettle body; 9. a knob; 10. a bidirectional screw; 11. a stirring rod; 12. a drive shaft; 13. a nut block.

Detailed Description

The technical solution in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, rather than all embodiments, and all other embodiments obtained by a person of ordinary skill in the art without creative work belong to the protection scope of the present invention based on the embodiments of the present invention.

Referring to fig. 1-4, sulfonation reaction kettle of steerable temperature, including braced frame 1, braced frame 1's top fixedly connected with bracing piece 3, bracing piece 3's top fixedly connected with reation kettle body 8, reation kettle body 8's top fixedly connected with unloading pipe 6, reation kettle body 8's bottom fixedly connected with unloading pipe 6, be provided with the valve on the unloading pipe 6, the logical groove 101 of sliding has been seted up to braced frame 1's side, the logical inslot 101 of sliding is provided with folding assembly, a plurality of filter screen poles 4 of fixedly connected with between the folding assembly that is in the symmetric state, the network structure is constituteed to a plurality of filter screen poles 4, braced frame 1's bottom fixedly connected with supporting leg 5.

The through hole has been seted up in the top center department of reation kettle body 8, and reation kettle body 8's top is provided with agitator motor 7, and agitator motor 7's fixed surface is connected with the collar, fixedly connected with locating lever between collar and reation kettle body 8's the top, and collar and locating lever can realize agitator motor 7's installation function.

Stirring motor 7's output fixedly connected with drive shaft 12, the inside that the through hole extended to reation kettle body 8 is passed to the one end of drive shaft 12, and the fixed surface of drive shaft 12 is connected with puddler 11, and stirring motor 7 cooperation drive shaft 12 and puddler 11 can realize the stirring function of reation kettle body 8 interior reactant.

Folding assembly includes the connection channel-section steel of sliding connection in the logical groove 101 that slides and rotates the transfer line 2 of connection in connecting the channel-section steel, and folding assembly can realize the equidistance translation function of a plurality of filter screen poles 4.

The transfer line 2 in the same connection channel-section steel is the V font, rotates between the adjacent transfer line 2 to be connected, can guarantee that folding assembly can realize folding function.

A side face of the supporting frame 1 is located on two sides of the folding assembly and is connected with a nut block 13 in a sliding mode, a side face of the nut block 13 is provided with a transfer groove, the transfer groove is connected with a transmission rod 2 on the outermost side in a rotating mode, a bidirectional screw rod 10 is connected with an inner thread of the nut block 13, a knob 9 is fixedly connected to one end of the bidirectional screw rod 10, the bidirectional screw rod 10 can drive the nut blocks 13 on two sides to move in opposite directions or move in opposite directions, and the driving function of the folding assembly is achieved.

The filter screen rod 4 is made of stainless steel material, has a certain rust-proof and corrosion-proof function, and has strong hardness.

The reaction kettle body 8 is provided with an observation window for observing the size of impurities in the obtained material.

The utility model discloses when using, pour the reactant into reation kettle body 8 through unloading pipe 6 in, then open agitator motor 7, agitator motor 7 drives drive shaft 12 and puddler 11 and rotates, realizes the stirring function of reactant, the reaction rate of reactant with higher speed.

After the reaction of the reactants is completed, a transition container (similar containers such as a material receiving box and the like) is placed below a mesh structure formed by filter screen rods 4, then a valve on a discharging pipe is opened, so that the materials obtained by the reaction are discharged through the discharging pipe and fall into the transition container, impurities in the materials can be filtered by the mesh structure, then the obtained materials and new reactants are put into a reaction kettle body 8 through a discharging pipe 6 again, after the reaction is finished, the size of the impurities in the obtained materials can be observed through an observation window, according to the size of impurity particles, a knob 9 can be rotated, the knob 9 drives a bidirectional screw rod 10 to rotate, so that nut blocks 13 on two sides move towards opposite directions or in opposite directions, and simultaneously one end of a transmission rod 2 can be driven to move under the combined action of the rotary connection between the transmission rods 2 and the sliding connection of a connection channel steel and a sliding through groove 101, make folding assembly realize extension and shrink function, and then drive the motion of filter screen pole 4, realize adjusting the function in clearance between the filter screen pole 4, and then realize adjusting the pore size on the network structure that filter screen pole 4 constitutes, make the pore size on the network structure that filter screen pole 4 constitutes be less than the size of impurity, thereby need not to change filter screen structure and can realize the filtering capability to different granule size impurity, thereby improved the preparation efficiency of tuo's sour greatly.

The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.

Claims

1. Sulfonation reaction kettle of steerable temperature, including braced frame (1), its characterized in that, the top fixedly connected with bracing piece (3) of braced frame (1), the top fixed connection of bracing piece (3) has reation kettle body (8), the top fixedly connected with unloading pipe (6) of reation kettle body (8), row's material pipe is arranged to the bottom fixedly connected with of reation kettle body (8), it is provided with the valve on the row's material pipe, the logical groove of sliding (101) has been seted up to the side of braced frame (1), be provided with folding assembly in the logical groove of sliding (101), be in a plurality of filter screen poles of fixedly connected with (4) between the folding assembly of symmetric state, a plurality of the network structure is constituteed in filter screen pole (4), the bottom fixedly connected with supporting leg (5) of braced frame (1).

2. The temperature-controllable sulfonation reaction kettle of claim 1, wherein: the through hole has been seted up at the top center department of reation kettle body (8), the top of reation kettle body (8) is provided with agitator motor (7), the fixed surface of agitator motor (7) is connected with the collar, fixedly connected with locating lever between the top of collar and reation kettle body (8).

3. The temperature-controllable sulfonation reaction kettle of claim 2, wherein: the output end fixedly connected with drive shaft (12) of agitator motor (7), the inside that the through-hole extended to reation kettle body (8) is passed to the one end of drive shaft (12), the fixed surface of drive shaft (12) is connected with puddler (11).

4. The temperature-controllable sulfonation reaction kettle of claim 1, wherein: the folding assembly comprises a connecting channel steel which is connected in the sliding through groove (101) in a sliding mode and a transmission rod (2) which is connected in the connecting channel steel in a rotating mode.

5. The temperature-controllable sulfonation reaction kettle of claim 4, wherein: the transmission rods (2) in the same connecting channel steel are V-shaped, and the adjacent transmission rods (2) are connected in a rotating mode.

6. The temperature-controllable sulfonation reaction kettle of claim 5, wherein: a nut block (13) is slidably connected to one side face of the supporting frame (1) on two sides of the folding assembly, a transfer groove is formed in one side face of the nut block (13), and the transfer groove is rotatably connected with the transmission rod (2) on the outermost side.

7. The temperature-controlled sulfonation reaction kettle of claim 6, wherein: the nut block (13) is internally threaded with a bidirectional screw (10), and one end of the bidirectional screw (10) is fixedly connected with a knob (9).