CN217418784U

CN217418784U - High-purity metal gallium crystallizer

Info

Publication number: CN217418784U
Application number: CN202220602316.8U
Authority: CN
Inventors: 张德云; 张家怡; 周柏均
Original assignee: Henan Haizhide High Tech Environmental Protection Technology Co ltd
Current assignee: Henan Haizhide High Tech Environmental Protection Technology Co ltd
Priority date: 2022-03-19
Filing date: 2022-03-19
Publication date: 2022-09-13
Anticipated expiration: 2032-03-19

Abstract

The utility model relates to the technical field of metal gallium crystallizer, and discloses a high-purity metal gallium crystallizer, which comprises a water bath tank, wherein a controller is arranged on the outer wall of the water bath tank, a bottom plate is arranged above the water bath tank, a plurality of detachable crystallization tubes are inserted on the bottom plate, a cover plate is arranged at the tube orifice of each crystallization tube, a first electric heating tube is arranged at the bottom of the cover plate, which is positioned inside the crystallization tube, a pressing plate is arranged at the top of the bottom plate, a cam is driven by a motor to rotate, the bottom plate, the pressing plate and the crystallization tubes can wholly ascend or descend along a guide pillar by matching with a spring, so as to vibrate the metal gallium inside the crystallization tubes, improve the purity of the purified metal gallium, and because the pressing plate is fixed on the bottom plate by a fixing bolt, the cover plate, the first electric heating tube and the crystallization tubes are integrated, thereby preventing air from entering the crystallization tubes in the vibration process, the stability of the gallium metal during purification is improved.

Description

High-purity metal gallium crystallizer

Technical Field

The utility model relates to a gallium metal crystallizer technical field specifically is a high-purity gallium metal crystallizer.

Background

In the patent with the patent number of CN210261935U and the patent name of high-purity gallium metal crystallizer, the patent mentions that liquid gallium in the crystallizer can be stirred by a servo motor and a screw rod which are convenient for pushing a plurality of constant-temperature stirring tubes to move up and down simultaneously. However, in the up-and-down movement process of the constant temperature stirring pipe, air can enter the crystallization pipe from the gap between the constant temperature stirring pipe and the crystallization pipe, so that the temperature inside the crystallization pipe is uneven, and dust in the air easily enters the crystallization pipe, thereby affecting the purification effect of the gallium metal.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide a high-purity metal gallium crystallizer to solve the problem that proposes among the above-mentioned background art.

In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a high-purity metal gallium crystallizer, includes the water bath, the controller is installed to the outer wall of water bath, the top of water bath is provided with the bottom plate, it has a plurality of detachable crystallization pipe to peg graft on the bottom plate, the mouth of pipe department of crystallization pipe is provided with the apron, the internally mounted that the bottom of apron is located the crystallization pipe has first electrothermal tube, the top of bottom plate is provided with the clamp plate, the cavity that holds the crystallization pipe mouth of pipe and apron is seted up to the inside of clamp plate, and passes through gim peg fixed connection between clamp plate and the apron, first electrothermal tube and controller electric connection.

Preferably, guide pillars are fixed on two sides of the top of the water bath tank, the guide pillars penetrate through the bottom plate, a fixing plate is in threaded connection with the tops of the guide pillars, a spring is sleeved outside the guide pillars and located between the fixing plate and the bottom plate, a supporting block is fixed on one side of the water bath tank through a bolt, a motor is installed at the tops of the supporting blocks, a cam is fixed on a transmission shaft of the motor and located at the bottom of the bottom plate, the cam is in contact with the bottom plate, the motor is electrically connected with the controller, the motor drives the cam to rotate, and the motor is matched with the spring, so that the bottom plate, the pressing plate and the crystallization tube can integrally ascend or descend along the guide pillars, and the distribution of metal gallium inside the crystallization tube is more uniform.

Preferably, a sealing gasket is arranged between the bottom of the cover plate and the opening of the crystallization tube, and liquid gallium in the crystallization tube can be prevented from leaking by the sealing gasket.

Preferably, the bottom of clamp plate is close to the position of its four corners and all is fixed with spacing post, the bottom of spacing post extends to the inside of water bath, when clamp plate and bottom plate upwards or when moving downwards simultaneously, utilizes the stability when spacing post can further improve clamp plate and bottom plate and remove, avoids crystal tube and water bath to produce the extrusion to play the guard action to the crystal tube.

Preferably, the inside of water bath cabinet is located the below of crystallization pipe and installs the second electrothermal tube, can further improve the speed that the inside liquid temperature of water bath cabinet heaies up through the second electrothermal tube, and one side bottom of water bath cabinet installs the water pump, the water inlet and the water bath cabinet of water pump are linked together, the water export of water pump passes through the pipe connection in one side top of water bath cabinet, second electrothermal tube and water pump all with controller electric connection, utilize the water pump can carry the inside top of water bath cabinet with the rivers of the inside below of water bath cabinet, improve the degree of consistency that is heated of crystallization pipe.

Preferably, the inside top of water bath is fixed with the diaphragm, the inside of diaphragm is located the outside of crystallization pipe and has seted up the water guide hole, the inside in water guide hole is fixed with the honeycomb duct, the bottom of honeycomb duct extends to the below of crystallization pipe, utilizes diaphragm and honeycomb duct, can accelerate rivers at the flow velocity of crystallization pipe outer wall.

Compared with the prior art, the beneficial effects of the utility model are that:

1. this high-purity metal gallium crystallizer, drive the cam through the motor and rotate, the cooperation spring, can make the bottom plate, clamp plate and crystallization tube are whole to rise or descend along the guide pillar, and then vibrate the inside metal gallium of crystallization tube, it is more even to make the metal gallium distribute, purity when improving the metal gallium purification, and simultaneously, because the clamp plate passes through the gim peg to be fixed on the bottom plate, make the apron, first electrothermal tube and crystallization tube form wholly, and then can prevent that the crystallization tube from vibrating the in-process, the air gets into in the crystallization tube, stability when improving the metal gallium purification.

2. This high-purity metal gallium crystallizer can further improve the speed that the inside liquid temperature of water bath heaies up through the second electrothermal tube, utilizes the water pump can carry the inside top of water bath with the rivers of the inside below of water bath to the inside top of water bath, and then accelerates rivers at the inside flow rate of water bath, improves the degree of consistency that is heated of crystallization pipe, utilizes diaphragm and honeycomb duct, can carry out the water conservancy diversion with rivers along the outer wall of crystallization pipe for rivers are at the outside velocity of flow of crystallization pipe.

Drawings

FIG. 1 is a schematic view of the entire structure of embodiment 1;

FIG. 2 is an enlarged view of portion A of FIG. 1;

FIG. 3 is a side view of the cam in embodiment 1;

FIG. 4 is a cross-sectional view of a crystallization tube in example 1;

fig. 5 is a schematic structural view of embodiment 2.

In the figure: 1. a water bath tank; 2. a limiting column; 3. a controller; 4. a fixing bolt; 5. pressing a plate; 6. a base plate; 7. a cover plate; 8. crystallizing the tube; 9. a spring; 10. a fixing plate; 11. a guide post; 12. a cam; 13. a motor; 14. a support block; 15. a first electric heating tube; 16. a gasket; 17. a transverse plate; 18. a second electric heating tube; 19. a water pump; 20. a flow guide pipe; 21. a water guide hole.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "front end", "rear end", "both ends", "one end", "the other end" and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the device or element to which the reference is made must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.

In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "connected," and the like are to be construed broadly, and for example, "connected" may be either fixedly connected or detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood in specific cases to those skilled in the art.

Example 1

As shown in fig. 1 to 4, the high-purity gallium metal crystallizer of the present embodiment includes a water bath 1, a controller 3 is installed on an outer wall of the water bath 1, a bottom plate 6 is installed above the water bath 1, a plurality of detachable crystallization tubes 8 are inserted into the bottom plate 6, a cover plate 7 is installed at a tube opening of the crystallization tubes 8, a first electric heating tube 15 is installed inside the crystallization tube 8 at the bottom of the cover plate 7, a pressing plate 5 is installed at a top of the bottom plate 6, a cavity for accommodating the tube opening of the crystallization tube 8 and the cover plate 7 is formed inside the pressing plate 5, the pressing plate 5 is fixedly connected with the cover plate 7 through a fixing bolt 4, the first electric heating tube 15 is electrically connected with the controller 3, the pressing plate 5 is fixed on the bottom plate 6 through the fixing bolt 4, the cover plate 7, the first electric heating tube 15 and the crystallization tube 8 can be integrated, and further, in a process of preventing the crystallization tube 8 from oscillating, air is introduced into the crystallization tube 8.

Specifically, guide pillars 11 are fixed on two sides of the top of the water bath tank 1, the guide pillars 11 penetrate through the bottom plate 6, the top of each guide pillar 11 is in threaded connection with a fixing plate 10, a spring 9 is sleeved between the fixing plate 10 and the bottom plate 6 outside the guide pillar 11, a supporting block 14 is fixed on one side of the water bath tank 1 through a bolt, a motor 13 is installed at the top of the supporting block 14, a cam 12 is fixed on a transmission shaft of the motor 13, the cam 12 is located at the bottom of the bottom plate 6, the cam 12 is in contact with the bottom plate 6, the motor 13 is electrically connected with the controller 3, the motor 13 drives the cam 12 to rotate, the spring 9 is matched, the bottom plate 6, the pressing plate 5 and the crystallization tube 8 can integrally ascend or descend along the guide pillars 11, and therefore the gallium metal inside the crystallization tube 8 is distributed more uniformly.

Furthermore, a sealing gasket 16 is arranged between the bottom of the cover plate 7 and the opening of the crystallization tube 8, and the liquid gallium inside the crystallization tube 8 can be prevented from leaking by the sealing gasket 16.

Furthermore, the bottom of clamp plate 5 is close to the position of its four corners and all is fixed with spacing post 2, and the bottom of spacing post 2 extends to the inside of water bath 1, when clamp plate 5 and bottom plate 6 upwards or when moving down simultaneously, utilizes stability when spacing post 2 can further improve clamp plate 5 and bottom plate 6 and remove, avoids crystallizing pipe 8 and water bath 1 to produce the extrusion to play the guard action to crystallizing pipe 8.

The using method of the embodiment comprises the following steps: putting gallium to be purified into the crystallization tube 8, then enabling the water bath tank 1 to work through the controller 3, heating the outside of the crystallization tube 8, and simultaneously opening the first electric heating tube 15, enabling the first electric heating tube 15 to heat the inside of the crystallization tube 8, and further improving the purity of the gallium;

in the process, the motor 13 is turned on, the transmission shaft of the motor 13 drives the cam 12 to rotate, and the cam 12 is in contact with the bottom plate 6, so that the bottom plate 6 can ascend or descend along the guide post 11 along with the rotation of the cam 12 and under the action of the spring 9, and the pressing plate 5, the bottom plate 6 and the crystallization tube 8 are integrally vibrated up and down, so that the distribution of the gallium metal is more uniform, and the purity of the gallium metal during purification is further improved;

because the pressing plate 5 is fixed on the bottom plate 6 through the fixing bolt 4, the cover plate 7, the first electric heating tube 15 and the crystallizing tube 8 are integrated, air can be prevented from entering the crystallizing tube 8 in the oscillation process of the crystallizing tube 8, and the stability of the gallium metal during purification is improved.

Example 2

The structure of the high-purity gallium metal crystallizer of the embodiment is basically the same as that of the high-purity gallium metal crystallizer of the embodiment 1, the second electric heating tube 18 is installed inside the water bath tank 1 and below the crystallization tube 8, the temperature rise rate of the liquid inside the water bath tank 1 can be further improved through the second electric heating tube 18, the water pump 19 is installed at the bottom of one side of the water bath tank 1, the water inlet of the water pump 19 is communicated with the water bath tank 1, the water outlet of the water pump 19 is connected to the top of one side of the water bath tank 1 through a pipeline, the second electric heating tube 18 and the water pump 19 are both electrically connected with the controller 3, the water flow below the inside of the water bath tank 1 can be conveyed to the upper part inside the water bath tank 1 through the water pump 19, and the heating uniformity of the crystallization tube 8 is improved; a transverse plate 17 is fixed above the inside of the water bath tank 1, a water guide hole 21 is formed in the outside of the crystallization tube 8 in the transverse plate 17, a guide tube 20 is fixed inside the water guide hole 21, the bottom end of the guide tube 20 extends to the lower part of the crystallization tube 8, and the transverse plate 17 and the guide tube 20 are used for increasing the flowing speed of water flow on the outer wall of the crystallization tube 8 (see fig. 5).

The using method of the embodiment comprises the following steps: the temperature rising rate of the liquid in the water bath tank 1 can be further improved through the second electric heating tube 18, the water flow below the interior of the water bath tank 1 can be conveyed to the upper portion of the interior of the water bath tank 1 through the water pump 19, the flowing speed of the water flow in the water bath tank is further increased, and the heating uniformity of the crystallization tube 8 is improved;

by utilizing the transverse plate 17 and the guide pipe 20, the water flow can be guided along the outer wall of the crystallization tube 8, so that the flow speed of the water flow outside the crystallization tube 8 is accelerated.

Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described above, or equivalents may be substituted for elements thereof. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims

1. A high-purity metal gallium crystallizer comprises a water bath tank (1) and is characterized in that: the utility model discloses a crystallization device, including water bath (1), controller (3) are installed to the outer wall of water bath (1), the top of water bath (1) is provided with bottom plate (6), it has a plurality of detachable crystallization pipe (8) to peg graft on bottom plate (6), the mouth of pipe department of crystallization pipe (8) is provided with apron (7), the internally mounted that the bottom of apron (7) is located crystallization pipe (8) has first electrothermal tube (15), the top of bottom plate (6) is provided with clamp plate (5), the cavity that holds crystallization pipe (8) mouth of pipe and apron (7) is seted up to the inside of clamp plate (5), and passes through gim peg (4) fixed connection between clamp plate (5) and apron (7), first electrothermal tube (15) and controller (3) electric connection.

2. The crystallizer for crystallizing high-purity metallic gallium according to claim 1, wherein: guide pillars (11) are fixed on two sides of the top of the water bath tank (1), the guide pillars (11) penetrate through the bottom plate (6), a fixing plate (10) is connected to the top of each guide pillar (11) in a threaded mode, a spring (9) is sleeved between the fixing plate (10) and the bottom plate (6) and located outside the guide pillars (11), supporting blocks (14) are fixed on one side of the water bath tank (1) through bolts, a motor (13) is installed at the top of each supporting block (14), a cam (12) is fixed on a transmission shaft of the motor (13), the cam (12) is located at the bottom of the bottom plate (6), the cam (12) is in contact with the bottom plate (6), and the motor (13) is electrically connected with the controller (3).

3. The crystallizer for crystallizing high-purity metallic gallium according to claim 1, wherein: a sealing gasket (16) is arranged between the bottom of the cover plate (7) and the mouth of the crystallization tube (8).

4. The crystallizer for crystallizing high-purity metallic gallium according to claim 1, wherein: the bottom of clamp plate (5) all is fixed with spacing post (2) near the position of its four corners, the bottom of spacing post (2) extends to the inside of water bath (1).

5. The crystallizer for crystallizing high-purity metallic gallium according to claim 1, wherein: the inside of water bath (1) is located the below of crystallization pipe (8) and installs second electrothermal tube (18), and one side bottom of water bath (1) installs water pump (19), the water inlet and the water bath (1) of water pump (19) are linked together, the water export of water pump (19) passes through the pipe connection in one side top of water bath (1), second electrothermal tube (18) and water pump (19) all with controller (3) electric connection.

6. A high purity metallic gallium crystallizer as claimed in claim 5, wherein: the inside top of water bath (1) is fixed with diaphragm (17), water guide hole (21) have been seted up to the outside that the inside of diaphragm (17) is located crystallization pipe (8), the inside of water guide hole (21) is fixed with honeycomb duct (20), the bottom of honeycomb duct (20) extends to the below of crystallization pipe (8).