CN217015339U - Potassium fluoride production is with concentrated reaction condensation reflux unit - Google Patents
Potassium fluoride production is with concentrated reaction condensation reflux unit Download PDFInfo
- Publication number
- CN217015339U CN217015339U CN202121237040.XU CN202121237040U CN217015339U CN 217015339 U CN217015339 U CN 217015339U CN 202121237040 U CN202121237040 U CN 202121237040U CN 217015339 U CN217015339 U CN 217015339U
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- Prior art keywords
- water
- intercommunication
- potassium fluoride
- pipe
- condensation reflux
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- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 title claims abstract description 54
- 235000003270 potassium fluoride Nutrition 0.000 title claims abstract description 27
- 239000011698 potassium fluoride Substances 0.000 title claims abstract description 27
- 238000010992 reflux Methods 0.000 title claims abstract description 18
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 17
- 238000009833 condensation Methods 0.000 title claims abstract description 15
- 230000005494 condensation Effects 0.000 title claims abstract description 15
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 68
- 238000010438 heat treatment Methods 0.000 claims abstract description 27
- 239000003651 drinking water Substances 0.000 claims abstract description 6
- 235000020188 drinking water Nutrition 0.000 claims abstract description 6
- 238000005086 pumping Methods 0.000 claims description 6
- 230000005540 biological transmission Effects 0.000 claims 1
- 238000004064 recycling Methods 0.000 abstract description 5
- 238000006482 condensation reaction Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000008236 heating water Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Images
Abstract
The utility model provides a potassium fluoride production is with concentrated reaction condensation reflux unit, including concentrated cauldron, back flow, holding vessel, water pump, heating device, gas-supply pipe global and the bottom surface of concentrated cauldron all are provided with the jacket jar, the upper end intercommunication of back flow is in the lower extreme of jacket jar, the lower extreme of back flow extends to in the holding vessel, it has the drinking-water pipe to peg graft on the holding vessel, the other end of drinking-water pipe with the water pump intercommunication, the water pump intercommunication has the water-supply pipe, the water-supply pipe intercommunication communicates to the heating device who heats comdenstion water into steam, heating device intercommunication has the steam pot, the steam pot with the gas-supply pipe intercommunication, the gas-supply pipe communicate to the jacket jar. The utility model has the advantages of recycling condensed water and saving cost.
Description
Technical Field
The utility model belongs to the technical field of potassium fluoride production equipment, and particularly relates to a condensation reflux device for a concentration reaction for potassium fluoride production.
Background
Need carry out the concentration technology in the production process of potassium fluoride, evaporate unnecessary water in the potassium fluoride solvent and improve the concentration of potassium fluoride, the concentration technology has the multiple, and general concentration is realized through the heating method, and the comdenstion water that nevertheless produces after the heating concentration is direct discharges, easily causes the waste, is unfavorable for practicing thrift the cost.
SUMMERY OF THE UTILITY MODEL
The utility model aims to overcome the defects of the prior art and provide a condensation reflux device for the condensation reaction in the potassium fluoride production, which can ensure that the condensation reaction is uniformly heated in the condensation process, so that condensed water is collected and reused, and the waste of the condensed water is avoided.
The technical scheme of the utility model is as follows:
the utility model provides a potassium fluoride production is with concentrated reaction condensation reflux unit, includes concentrated cauldron, back flow, holding vessel, water pump, heating device, gas-supply pipe the global and the bottom surface of concentrated cauldron are provided with jacket jar outward, the upper end intercommunication of back flow is in the lower extreme of jacket jar, the lower extreme of back flow extends to in the holding vessel, it has the drinking-water pipe to peg graft on the holding vessel, the other end of drinking-water pipe with the water pump intercommunication, the water pump intercommunication has the upper hose, the upper hose intercommunication communicates to the heating device who heats the comdenstion water into steam, heating device intercommunication has the steam pot, the steam pot with the gas-supply pipe intercommunication, the gas-supply pipe communicates to jacket jar.
Furthermore, the lower end of the concentration kettle and the lower end of the jacket tank are both hemispherical.
Furthermore, the concentration kettles are multiple, and each concentration kettle is connected to the same storage tank through a return pipe.
Further, the steam tank is respectively communicated with jacket tanks on the plurality of concentration kettles through a plurality of gas conveying pipes.
Further, a gate valve is arranged between the water pumping pipe and the water pump.
Furthermore, a flow meter is arranged on the water feeding pipe between the water pump and the heating device.
Further, a pressure gauge is arranged in the storage tank, and a dial plate of the pressure gauge is positioned above the storage tank.
Compared with the prior art, the utility model has the beneficial effects that:
the jacket tank is additionally arranged outside the concentration kettle, the jacket tank is communicated with the steam tank, the concentration kettle is heated and concentrated by using steam, the jacket tank is filled with the steam, the concentration kettle is relatively uniformly heated, the potassium fluoride solution is condensed to form condensed water after being heated by the steam, the condensed water returns to the storage tank through the return pipe to be stored, then the condensed water is pumped to the heating device by the water pump to be heated into the steam, and the steam is introduced into the steam tank, so that the recycling of the condensed water is formed, and the water resource and the cost are saved.
In a word, the utility model has the advantages of uniform heating and recycling of condensed water.
Drawings
FIG. 1 is a schematic view of the present invention.
In the figure, 1, a concentration kettle, 2, a jacket tank, 3, a return pipe, 4, a storage tank, 5, a water pumping pipe, 6, a gate valve, 7, a water pump, 8, a water feeding pipe, 9, a heating device, 10, a gas conveying pipe, 11, a steam tank, 12, a flowmeter, 13 and a pressure gauge.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
As shown in fig. 1, a condensation reflux device for concentration reaction for potassium fluoride production comprises a concentration kettle 1, a reflux pipe 3, a storage tank 4, a water pump 7, a heating device 9, a gas pipe 10, jacket tanks 2 arranged outside the periphery and the bottom of the concentration kettle 1, wherein the upper end of the reflux pipe 3 is communicated with the lower end of the jacket tanks 2, the lower end of the reflux pipe 3 extends into the storage tank 4, a water pumping pipe 5 is inserted into the storage tank 4, the other end of the water pumping pipe 5 is communicated with the water pump 7, the water pump 7 is communicated with a water supply pipe 8, the water supply pipe 8 is communicated with the heating device 9 for heating condensed water into steam, the heating device 9 is communicated with a steam tank 11, the steam tank 11 is communicated with the gas pipe 10, and the gas pipe 10 is communicated with the jacket tanks 2;
the potassium fluoride solution in the concentration kettle 1 is heated and concentrated by using steam, an upper cover of the concentration kettle 1 is connected with an exhaust pipe to exhaust gas generated after the potassium fluoride is concentrated, the jacketed tank 2 is filled with the steam, the concentration kettle 1 is relatively uniformly heated, the steam can be condensed after the potassium fluoride solution is heated to form condensate water, the condensate water returns to the storage tank 4 through the return pipe 3 to be stored, the condensate water is pumped to the heating device 9 through the water pump 7 to be heated into steam, and the steam is introduced into the steam tank 11 to form the recycling of the condensate water, so that the water resource and the cost are saved, wherein the heating device 9 can be a common device for heating water into steam;
specifically, combine the potassium fluoride production line, set up concentrated cauldron 1 and reflux unit as two-layerly, the upper strata is the concentrated cauldron 1 and the jacket jar 2 of potassium fluoride, sets up holding vessel 4 and water pump 7 in the lower floor, and back flow 3 communicates the lower floor from jacket jar 2, if the pipeline is long enough uses the multistage pipeline to splice inadequately.
In this embodiment, the lower end of the concentration kettle 1 and the lower end of the jacket tank 2 are both made to be hemispherical, so that condensed water can flow to the bottom end of the jacket tank 2 and be discharged from the return pipe 3, and a support is arranged outside the jacket tank 2 to support and fix the jacket tank 2 and the concentration kettle 1.
In this embodiment, concentrated cauldron 1 is a plurality of, and every concentrated cauldron 1 all connects in same holding vessel 4 through back flow 3, all flows back a plurality of concentrated cauldron 1's comdenstion water together, carries out unified processing and can save space and cost.
In this embodiment, steam drum 11 is through a plurality of gas-supply pipe 10 respectively with a plurality of concentrated 2 intercommunications of jacket jars on the cauldron 1, unify and carry out steam supply to a plurality of concentrated cauldron 1, to the comdenstion water unified processing after the heating, make the backward flow circulation result of use of whole comdenstion water better, unify to the comdenstion water collection and use, be favorable to practicing thrift the cost.
In this embodiment, a gate valve 6 is disposed between the pumping pipe 5 and the water pump 7, and preferably, the gate valve 6 is an elastic seat sealing gate valve, and the flow rate in the pipeline can be adjusted while controlling the switch.
In this embodiment, a flow meter 12 is installed on the water feeding pipe 8 between the water pump 7 and the heating device 9 for displaying the flow rate of the water fed into the heating device 9, and by observing the change of the value of the flow meter 12, if the steam usage amount required for concentrating the potassium fluoride solution is reached, the gate valve 6 and the water pump 7 can be closed, thereby facilitating the control of the water in the heating device 9 and the steam amount in the steam tank 11.
In this embodiment, pressure gauge 13 is equipped with in the holding vessel 4, pressure gauge 13's dial plate is located the top of holding vessel 4, and the change through 13 dial plate readings of pressure gauge indicates the height of the interior condensate water of holding vessel 4, the memory space of the control comdenstion water of being convenient for.
When the steam condensing device is used, steam in the steam tank 11 is conveyed to the jacket tank 2, the potassium fluoride solution in the condensing kettle 1 is heated and condensed by the steam, the potassium fluoride solution is condensed into condensed water after being heated by the steam, the condensed water returns to the storage tank 4 through the return pipe 3 to be stored, then the condensed water is pumped to the heating device 9 through the water pump 7 to be heated into steam, the steam is introduced into the steam tank 11, and the steam tank 11 is communicated with the jacket tank 2 to form the recycling of the condensed water.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that various changes in the embodiments and/or modifications of the utility model can be made, and equivalents and modifications of some features of the utility model can be made without departing from the spirit and scope of the utility model.
Claims (7)
1. The utility model provides a potassium fluoride production is with concentrated reaction condensation reflux unit which characterized in that: including concentrated cauldron, back flow, holding vessel, water pump, heating device, gas-supply pipe global and the bottom surface of concentrated cauldron are provided with the jacket jar outward, the upper end intercommunication of back flow is in the lower extreme of jacket jar, the lower extreme of back flow extends to in the holding vessel, it has the drinking-water pipe that extends to its bottom to peg graft on the holding vessel, the other end of drinking-water pipe with the water pump intercommunication, the water pump intercommunication has the upper hose, the upper hose intercommunication communicates to the heating device who heats the comdenstion water into vapor, the heating device intercommunication has the steam drum, the steam drum with the gas-supply pipe intercommunication, the gas-supply pipe intercommunication extremely the jacket jar.
2. The condensation reflux device for concentration reaction in potassium fluoride production according to claim 1, wherein: the lower end of the concentration kettle and the lower end of the jacket tank are both hemispherical.
3. The condensation reflux device for concentration reaction in potassium fluoride production according to claim 1, wherein: the concentrating device comprises a plurality of concentrating kettles, and each concentrating kettle is connected to the same storage tank through a return pipe.
4. The condensation reflux device for concentration reaction in potassium fluoride production according to claim 3, wherein: the steam tank is respectively communicated with jacket tanks on the plurality of concentration kettles through a plurality of gas transmission pipes.
5. The condensation reflux device for the concentration reaction in the production of potassium fluoride according to claim 1, characterized in that: and a gate valve is arranged between the water pumping pipe and the water pump.
6. The condensation reflux device for concentration reaction in potassium fluoride production according to claim 1, wherein: a flowmeter is arranged on the water feeding pipe between the water pump and the heating device.
7. The condensation reflux device for concentration reaction in potassium fluoride production according to claim 1, wherein: the pressure gauge is arranged in the storage tank, and the dial plate of the pressure gauge is positioned above the storage tank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202121237040.XU CN217015339U (en) | 2021-06-03 | 2021-06-03 | Potassium fluoride production is with concentrated reaction condensation reflux unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202121237040.XU CN217015339U (en) | 2021-06-03 | 2021-06-03 | Potassium fluoride production is with concentrated reaction condensation reflux unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN217015339U true CN217015339U (en) | 2022-07-22 |
Family
ID=82410630
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202121237040.XU Active CN217015339U (en) | 2021-06-03 | 2021-06-03 | Potassium fluoride production is with concentrated reaction condensation reflux unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN217015339U (en) |
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2021
- 2021-06-03 CN CN202121237040.XU patent/CN217015339U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 750336 Bayin OBO Industrial Park, Alxa Economic Development Zone, Alxa League, Inner Mongolia Autonomous Region Patentee after: Inner Mongolia Xinghan New Materials Co.,Ltd. Address before: 750336 Bayin OBO Industrial Park, Alxa Economic Development Zone, Alxa League, Inner Mongolia Autonomous Region Patentee before: Inner Mongolia Xinghan Fluorine Chemical Co.,Ltd. |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A concentration reaction condensation reflux device for potassium fluoride production Granted publication date: 20220722 Pledgee: Agricultural Bank of China Limited Alashan Left Banner Wusitai Sub-branch Pledgor: Inner Mongolia Xinghan New Materials Co.,Ltd. Registration number: Y2024980004132 |