CN207307225U - A kind of rectifier unit for phenyl ethylamine recycling - Google Patents

A kind of rectifier unit for phenyl ethylamine recycling Download PDF

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Publication number
CN207307225U
CN207307225U CN201721016961.7U CN201721016961U CN207307225U CN 207307225 U CN207307225 U CN 207307225U CN 201721016961 U CN201721016961 U CN 201721016961U CN 207307225 U CN207307225 U CN 207307225U
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CN
China
Prior art keywords
phenyl ethylamine
reaction kettle
pipe device
recycling
liquid recovery
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201721016961.7U
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Chinese (zh)
Inventor
李斌
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHAYANG QINJIANG CHEMICAL Co Ltd
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SHAYANG QINJIANG CHEMICAL Co Ltd
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Filing date
Publication date
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Priority to CN201721016961.7U priority Critical patent/CN207307225U/en
Application granted granted Critical
Publication of CN207307225U publication Critical patent/CN207307225U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/10Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working

Abstract

The utility model discloses a kind of rectifier unit for phenyl ethylamine recycling, its structure includes heat-resisting connecting tube, spinner flowmeter, heater, draw pipe device, shift pipe device, reaction kettle, first liquid recovery tank, second liquid recycling can, 3rd liquid recovery tank, discharge port, phenyl ethylamine temporary storage tank, voltage-stabiliser tube, pressure regulator, condenser pipe, the first liquid recovery tank is equipped with below heater, second liquid recycling can and the 3rd liquid recovery tank, heat-resisting connecting tube is movably installed on the right side of spinner flowmeter and using interference fit, a kind of rectifier unit for phenyl ethylamine recycling of the utility model, reaction kettle is equipped with below transfer pipe device, catalytic reaction can be carried out using reaction kettle, so that phenyl ethylamine rectifying is efficiently abundant, substantially increase the organic efficiency of phenyl ethylamine.

Description

A kind of rectifier unit for phenyl ethylamine recycling
Technical field
The utility model is a kind of rectifier unit for phenyl ethylamine recycling, belongs to the rectifier unit neck of phenyl ethylamine recycling Domain.
Background technology
Rectifying can be divided into atmospheric distillation, rectification under vacuum and compression rectification according to operating pressure.Rectification under vacuum, be exactly by System pressure is reduced, declines the bubble point of mixed liquor, seethes with excitement at low pressures, to reach the temperature for reducing distillation operation.Subtract Rectifying is pressed to be suitable for the mixture of high boiling substance, and rectifying can cause the polymerization of material or mixing for decomposed metamorphic at high temperature Compound.
Prior art discloses Application No.:A kind of workbench of rectifier unit of CN201621182052.6, belongs to essence Distillation unit technical field, it is desirable to provide a kind of workbench of rectifier unit, has the advantages that to make tower reactor realize elevating function, its skill Art programme element is a kind of workbench of rectifier unit, including supporting rack, and support frame as described above bottom end bearing is connected with and supporting rack The shaft that lower surface is arranged in parallel, one end of the shaft stretch out supporting rack, cam, the branch are fixedly connected with the shaft Support upper end is equipped with the movable plate parallel with supporting rack upper surface, but the prior art cannot carry out reaction using reaction kettle urges Change, cause phenyl ethylamine rectifying efficiently inabundant, be unfavorable for phenyl ethylamine recycling.
Utility model content
In view of the deficienciess of the prior art, the utility model aim is to provide a kind of rectifying dress for phenyl ethylamine recycling Put, catalytic reaction must not be carried out using reaction kettle with solution, cause phenyl ethylamine rectifying efficiently inabundant, be unfavorable for phenyl ethylamine recycling The problem of.
To achieve these goals, the utility model is to realize by the following technical solutions:One kind is used for phenyl ethylamine The rectifier unit of recycling, its structure include heat-resisting connecting tube, spinner flowmeter, heater, draw pipe device, transfer pipe device, Reaction kettle, the first liquid recovery tank, second liquid recycling can, the 3rd liquid recovery tank, discharge port, phenyl ethylamine temporary storage tank, voltage stabilizing Pipe, pressure regulator, condenser pipe, heater lower section are equipped with the first liquid recovery tank, second liquid recycling can and the 3rd liquid Recycling can, the heat-resisting connecting tube are movably installed on the right side of spinner flowmeter and using interference fit, the phenyl ethylamine Temporary storage tank is connected by voltage-stabiliser tube, condenser pipe, heat-resisting connecting tube, spinner flowmeter with heater, and the reaction kettle passes through Transfer pipe device, absorption pipe device are connected with heater, and the absorption pipe device is movably installed in above transfer pipe device, The reaction kettle is made of motor, feed inlet, rabble, return channel, reaction kettle chamber, and the return channel is installed on reaction kettle On the right side of chamber upper end, the feed inlet is fixedly installed in below reaction kettle chamber and using interference fit, the rabble with Motor is fixedly connected.
Further, the absorption pipe device is made of three suction pipes.
Further, the transfer pipe device is made of three transfer pipes.
Further, the spinner flowmeter is installed on heater top.
Further, the phenyl ethylamine temporary storage tank is arranged right below discharge port.
Further, the phenyl ethylamine temporary storage tank is made of quartz sand material.
Further, the shell of the reaction kettle is made of stainless steel material.
Beneficial effect
A kind of rectifier unit for phenyl ethylamine recycling of the utility model, transfer pipe device lower section are equipped with reaction kettle, can profit Catalytic reaction is carried out with reaction kettle so that phenyl ethylamine rectifying is efficiently abundant, substantially increases the organic efficiency of phenyl ethylamine.
Brief description of the drawings
Upon reading the detailed description of non-limiting embodiments with reference to the following drawings, other spies of the utility model Sign, objects and advantages will become more apparent upon:
Fig. 1 is a kind of structure diagram of rectifier unit for phenyl ethylamine recycling of the utility model;
Fig. 2 is the internal structure schematic diagram of the utility model reaction kettle.
In figure:Heat-resisting connecting tube -1, spinner flowmeter -2, heater -3, draw pipe device -4, be transfer pipe device -5, anti- Answer kettle -6, the first liquid recovery tank -7, second liquid recycling can -8, the 3rd liquid recovery tank -9, discharge port -10, phenyl ethylamine temporary Deposit tank -11, voltage-stabiliser tube -12, pressure regulator -13, condenser pipe -14, motor -61, feed inlet -62, rabble -63, return channel -64, Reaction kettle chamber -65.
Embodiment
To make the technical means, creative features, achievable purpose and effectiveness that the utility model is realized easy to understand, below With reference to embodiment, the utility model is expanded on further.
Please refer to Fig.1, Fig. 2, the utility model provides a kind of technical solution:A kind of rectifying dress for phenyl ethylamine recycling Put, its structure include heat-resisting connecting tube 1, spinner flowmeter 2, heater 3, draw pipe device 4, transfer pipe device 5, reaction kettle 6, First liquid recovery tank 7, second liquid recycling can 8, the 3rd liquid recovery tank 9, discharge port 10, phenyl ethylamine temporary storage tank 11, voltage stabilizing Pipe 12, pressure regulator 13, condenser pipe 14, the lower section of the heater 3 be equipped with the first liquid recovery tank 7, second liquid recycling can 8 with 3rd liquid recovery tank 9, the heat-resisting connecting tube 1 are movably installed in the right side of spinner flowmeter 2 and using interference fit, institutes The phenyl ethylamine temporary storage tank 11 stated is connected by voltage-stabiliser tube 12, condenser pipe 14, heat-resisting connecting tube 1, spinner flowmeter 2 with heater 3 Connect, the reaction kettle 6 is connected by shifting pipe device 5, drawing pipe device 4 with heater 3, the absorption pipe device 4 It is movably installed in transfer pipe device 5 top, the reaction kettle 6 is by motor 61, feed inlet 62, rabble 63, return channel 64, anti- Kettle chamber 65 is answered to form, the return channel 64 is installed on the right side of 65 upper end of reaction kettle chamber, and the feed inlet 62 is fixedly installed in It is fixedly connected below reaction kettle chamber 65 and using interference fit, the rabble 63 with motor 61, suction pipe dress Put 4 to be made of three suction pipes, the transfer pipe device 5 is made of three transfer pipes, and the spinner flowmeter 2 is installed on 3 top of heater, the phenyl ethylamine temporary storage tank 11 are arranged right below discharge port 10, and the phenyl ethylamine temporary storage tank 11 is by stone Sand material is formed, and the shell of the reaction kettle 6 is made of stainless steel material.
The broad understanding of reaction kettle 6 described in this patent has the container physically or chemically reacted, passes through the knot to container Structure designs and parameter configuration, realizes the mixture function of the heating of technological requirement, evaporation, cooling and low high speed.
As first user uses this practicality, the liquid containing phenyl ethylamine to be extracted is first introduced into reaction kettle chamber from feed inlet 62 65, after the interior progress auxiliary catalysis of reaction kettle chamber 65, then by adding to transfer pipe device 5 with drawing the arrival heater 3 of pipe device 4 After thermal extraction, phenyl ethylamine temporary storage tank 11 is reached by spinner flowmeter 2, condenser pipe 14, is discharged finally by discharge port 10.
The heat-resisting connecting tube 1 of the utility model, spinner flowmeter 2, heater 3, draw pipe device 4, transfer pipe device 5, Reaction kettle 6, the first liquid recovery tank 7, second liquid recycling can 8, the 3rd liquid recovery tank 9, discharge port 10, phenyl ethylamine temporary storage tank 11st, voltage-stabiliser tube 12, pressure regulator 13, condenser pipe 14, motor 61, feed inlet 62, rabble 63, return channel 64, reaction kettle chamber 65, portion The component that part is universal standard part or those skilled in the art know, its structure and principle all can pass through for this technology personnel Technical manual learns or knows by normal experiment method the utility model solves the problems, such as it is that the prior art cannot utilize reaction Kettle carries out catalytic reaction, and the problem of causing phenyl ethylamine rectifying efficiently inabundant, be unfavorable for phenyl ethylamine recycling, the utility model passes through Above-mentioned component is combined with each other, a kind of rectifier unit for phenyl ethylamine recycling of the utility model, and transfer pipe device 5 lower section is equipped with Reaction kettle 6, can carry out catalytic reaction using reaction kettle so that phenyl ethylamine rectifying is efficiently abundant, substantially increases returning for phenyl ethylamine Produce effects rate, it is described in detail below:
The reaction kettle 6 is made of motor 61, feed inlet 62, rabble 63, return channel 64, reaction kettle chamber 65, described Return channel 64 be installed on the right side of 65 upper end of reaction kettle chamber, the feed inlet 62 be fixedly installed in the lower section of reaction kettle chamber 65 and Using interference fit, the rabble 63 is fixedly connected with motor 61.
The advantages of basic principle and main feature and the utility model of the utility model has been shown and described above, for For those skilled in the art, it is clear that the utility model is not limited to the details of above-mentioned one exemplary embodiment, and without departing substantially from this In the case of the spirit or essential attributes of utility model, the utility model can be realized in other specific forms.Therefore, no matter From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the utility model is by institute Attached claim rather than described above limit, it is intended that will fall in the implication and scope of the equivalency of claim All changes are embraced therein.Any reference numeral in claim should not be considered as to the involved right of limitation It is required that.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped Containing an independent technical solution, this narrating mode of specification is only that those skilled in the art should for clarity Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art It is appreciated that other embodiment.

Claims (5)

  1. A kind of 1. rectifier unit for phenyl ethylamine recycling, it is characterised in that:Its structure includes heat-resisting connecting tube (1), rotor stream Gauge (2), heater (3), draw pipe device (4), transfer pipe device (5), reaction kettle (6), the first liquid recovery tank (7), the Two liquid recovery tanks (8), the 3rd liquid recovery tank (9), discharge port (10), phenyl ethylamine temporary storage tank (11), voltage-stabiliser tube (12), pressure regulation Device (13), condenser pipe (14), the heater (3) lower section are equipped with the first liquid recovery tank (7), second liquid recycling can (8) With the 3rd liquid recovery tank (9), the heat-resisting connecting tube (1) is movably installed on the right side of spinner flowmeter (2) and used It is full of cooperation, the phenyl ethylamine temporary storage tank (11) passes through voltage-stabiliser tube (12), condenser pipe (14), heat-resisting connecting tube (1), spinner Meter (2) is connected with heater (3), and the reaction kettle (6) is by shifting pipe device (5), drawing pipe device (4) and heater (3) it is connected, the absorption pipe device (4) is movably installed in above transfer pipe device (5), and the reaction kettle (6) is by electricity Machine (61), feed inlet (62), rabble (63), return channel (64), reaction kettle chamber (65) composition, the return channel (64) installation On the right side of reaction kettle chamber (65) upper end, the feed inlet (62) is fixedly installed in below reaction kettle chamber (65) and uses interference Coordinate, the rabble (63) is fixedly connected with motor (61).
  2. A kind of 2. rectifier unit for phenyl ethylamine recycling according to claim 1, it is characterised in that:The suction pipe Device (4) is made of three suction pipes.
  3. A kind of 3. rectifier unit for phenyl ethylamine recycling according to claim 1, it is characterised in that:The transfer pipe Device (5) is made of three transfer pipes.
  4. A kind of 4. rectifier unit for phenyl ethylamine recycling according to claim 1, it is characterised in that:The rotor stream Gauge (2) is installed on heater (3) top.
  5. A kind of 5. rectifier unit for phenyl ethylamine recycling according to claim 1, it is characterised in that:The phenyl ethylamine Temporary storage tank (11) is arranged right below discharge port (10).
CN201721016961.7U 2017-08-12 2017-08-12 A kind of rectifier unit for phenyl ethylamine recycling Expired - Fee Related CN207307225U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721016961.7U CN207307225U (en) 2017-08-12 2017-08-12 A kind of rectifier unit for phenyl ethylamine recycling

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721016961.7U CN207307225U (en) 2017-08-12 2017-08-12 A kind of rectifier unit for phenyl ethylamine recycling

Publications (1)

Publication Number Publication Date
CN207307225U true CN207307225U (en) 2018-05-04

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201721016961.7U Expired - Fee Related CN207307225U (en) 2017-08-12 2017-08-12 A kind of rectifier unit for phenyl ethylamine recycling

Country Status (1)

Country Link
CN (1) CN207307225U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113499600A (en) * 2021-07-17 2021-10-15 海南富山油气化工有限公司 Intelligent control device used in production process of petroleum mixed xylene

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113499600A (en) * 2021-07-17 2021-10-15 海南富山油气化工有限公司 Intelligent control device used in production process of petroleum mixed xylene

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Granted publication date: 20180504

Termination date: 20210812