CN216918850U - Catalytic cracking desulfurization waste water suspended solid processing apparatus - Google Patents
Catalytic cracking desulfurization waste water suspended solid processing apparatus Download PDFInfo
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- CN216918850U CN216918850U CN202123425463.7U CN202123425463U CN216918850U CN 216918850 U CN216918850 U CN 216918850U CN 202123425463 U CN202123425463 U CN 202123425463U CN 216918850 U CN216918850 U CN 216918850U
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Abstract
The utility model relates to a catalytic cracking desulfurization wastewater suspended matter treatment device, which comprises a high-density settler, a first mixer, a second mixer, a sludge buffer tank, a vacuum drum dehydrator and a slag slurry collecting tank, wherein the utility model adopts sludge reflux to improve the flocculation efficiency of suspended matters; through gravity sedimentation and inclined tube sedimentation, the sedimentation effect is improved, and the quality of clear water is ensured; the high vacuum degree formed by the vacuum drum dehydrator improves the solid content of the delivered mud cakes, reduces the subsequent treatment difficulty and reduces the occupied area of the device.
Description
Technical Field
The utility model relates to the field of catalytic cracking flue gas desulfurization wastewater treatment, in particular to a catalytic cracking desulfurization wastewater suspended matter treatment device.
Background
In recent years, along with the increasing severity of environmental problems, the nation has paid more attention to environmental protection problems, and the emission standards of atmospheric pollution areas are continuously improved, so that the environmental protection technology is continuously improved and advanced.
The flue gas discharged by the petroleum refining industry occupies a large proportion of the emission of atmospheric pollutants, wherein the flue gas discharged by a regenerator of a catalytic cracking unit is the largest air pollution source of a refinery, and the flue gas comprises particulate matters, sulfur oxides, nitrogen oxides, carbon monoxide and the like. The catalytic cracking regeneration flue gas is generated by the following steps: carbon deposits are generated on the surface of the catalyst in the catalytic cracking and catalytic cracking reaction processes, and the carbon deposits on the catalyst need to be regenerated and burnt in a regenerator, so that the activity of the catalyst is recovered; the carbon deposit is burnt out by using air through a regenerator, the entrained catalyst is separated from the regenerated flue gas through a cyclone separator, the regenerated flue gas is exhausted after energy is recovered through a smoke machine and a waste heat boiler, and the catalytic cracking regenerated flue gas is generated in the process. The catalytic cracking regenerated flue gas has the characteristics of wide fluctuation range of sulfur content, large particle size range of particles, high content of particles below submicron level and the like, and the main component of the particles is catalyst powder, contains heavy metals and needs to be effectively treated.
In the prior art, a wet removal process is generally adopted for purification treatment of catalytic cracking regenerated flue gas, and the regenerated flue gas is washed by a large amount of circulating absorption liquid to remove particles and sulfides in the regenerated flue gas and then is discharged into the atmosphere. In the wet desulphurization process, the fine catalyst particles are washed and absorbed by the desulphurization circulating slurry and are enriched in the desulphurization circulating slurry, and a certain amount of desulphurization circulating slurry needs to be discharged and further treated in order to maintain a balanced system.
At present, aiming at the treatment of suspended particles in catalytic cracking desulfurization wastewater, a gravity natural sedimentation method or a filtration membrane filtration method is mainly adopted, the specification of gravity sedimentation equipment is large, the investment is high, the service life of a filtration membrane of the filtration membrane filtration method is short, and the operation cost is high. For example, in the catalytic cracking flue gas desulfurization wastewater treatment process disclosed in the utility model with the application number of CN201110153423.3, an expanded tubular filter and a filter box are adopted for treating suspended matters in desulfurization wastewater, so that the filter element of the expanded tubular filter has short service life and frequent replacement in the operation of the device, and the operation cost of the device is increased; the filter box occupies a large area, the solid content of the mud cakes is low, and the difficulty in further processing the catalyst mud cakes is increased.
SUMMERY OF THE UTILITY MODEL
The utility model aims to solve the technical problem of providing a catalytic cracking desulfurization wastewater treatment device which can improve the treatment efficiency of catalytic cracking desulfurization wastewater suspended matters, reduce the treatment cost, improve the solid content of mud cakes and reduce the occupied area of equipment aiming at the current situation of the prior art.
The technical scheme adopted by the utility model for solving the technical problems is as follows:
a catalytic cracking desulfurization waste water suspended solid processing apparatus includes:
the high-density settler is used for carrying out fractional settlement on the desulfurization wastewater;
the first mixer is arranged at the upstream of the high-density settler and is used for mixing the desulfurization wastewater with a flocculating agent from a battery limit zone;
the second mixer is arranged between the first mixer and the high-density settler and is used for mixing part of the concentrated sludge from the first mixer and the bottom of the high-density settler and conveying the mixed sludge to the high-density settler;
the sludge buffer tank is arranged at the downstream of the high-density settler and is used for further concentrating part of concentrated sludge output from the bottom of the high-density settler;
the vacuum drum dehydrator is arranged at the downstream of the sludge buffer tank and is used for receiving the concentrated sludge output from the bottom of the sludge buffer tank and carrying out liquid-solid separation on the concentrated sludge;
the slag slurry collecting tank is arranged at the downstream of the vacuum drum dehydrator, is connected with the top of the vacuum drum dehydrator so as to receive the liquid phase separated by the vacuum drum dehydrator, and is connected with the top of the sludge buffer tank so as to receive the liquid phase separated by the sludge buffer tank; the slag slurry collecting tank is also connected with the downstream of the first mixer and the upstream of the second mixer through pipelines.
Preferably, the high-density settler comprises a gravity settling zone, an inclined tube settling zone and a clear water zone which are sequentially arranged from bottom to top, the second mixer is communicated with the gravity settling zone, and the clear water zone is connected with a pipeline for outputting clear liquid.
Preferably, the high-density settler is further provided with a first stirrer and a mud scraper, the first stirrer is located in the middle of the gravity settling area, and the mud scraper is located at the bottom of the gravity settling area and arranged close to the inner bottom of the high-density settler.
Preferably, the sludge buffer tank is connected with the bottom of the high-density settler, a valve for controlling the flow of fluid is arranged between the sludge buffer tank and the high-density settler, and a second stirrer is arranged in the sludge buffer tank.
Preferably, a rotatable drum is arranged in the vacuum drum dehydrator, filter cloth covers the periphery of the drum, the drum is hollow and connected with a vacuum pump and a separation tank, and a scraper used for scraping and collecting filter cakes on the outer wall of the filter cloth is further arranged in the vacuum drum dehydrator.
Preferably, a third stirrer for stirring the materials is further arranged in the vacuum drum dehydrator.
Preferably, the bottom of the separation tank is connected with a slurry collecting tank, and a fourth stirrer is arranged in the slurry collecting tank.
Preferably, a slurry collecting tank pump for conveying the liquid phase upwards is arranged between the slurry collecting tank and the second mixer.
Preferably, a sludge reflux pump is arranged between the high-density settler and the second mixer.
A method for catalytically cracking desulfurization wastewater suspended matters comprises the following steps:
the desulfurization wastewater from the catalytic cracking flue gas desulfurization system is conveyed to a high-density settler through a pipeline, wherein the temperature is 50-80 ℃, the pressure is 0.2-0.5 Mpag, and the content of suspended matters is 500-5000 mg/L.
The flocculating agent from the battery limits is mixed into the desulfurization wastewater from the catalytic cracking flue gas desulfurization system through a pipeline, and is fully mixed with the desulfurization wastewater through a mixer to continuously form suspended solid floc.
And (3) pressurizing the concentrated sludge from the high-density settler to 0.2-0.5 Mpag by a sludge reflux pump, and fully mixing the concentrated sludge with the desulfurization wastewater by a mixer to further accelerate the generation of suspended matter flocs.
The high-density settler is divided into a gravity settling area, an inclined tube settling area and a clear water area, and is provided with a stirrer and a mud scraper.
The desulfurization wastewater sent into the high-density settler firstly enters a gravity settling zone at the middle lower part of the high-density settler, and formed large-particle suspended matter flocs settle at the bottom of the high-density settler under the action of gravity.
And (3) allowing the desulfurized wastewater after primary sedimentation to enter a high-density settler inclined tube sedimentation area, allowing small-particle suspended matter flocs generated in the desulfurized wastewater to deposit on the surface of an inclined tube and slide to the bottom of the high-density settler, allowing the settled clear water to enter a clear water area of the high-density settler and be conveyed to the downstream through a pipeline, wherein the concentration of the clear water suspended matter is less than or equal to 50 mg/L.
The solid content of the concentrated sludge settled at the bottom of the high-density settler is 2-15% (mass fraction, the same applies below) and is divided into two strands, one strand is sent to a sludge reflux pump through a pipeline to be pressurized and finally mixed into the desulfurization wastewater; one stream of the sludge treatment system sends concentrated sludge to a sludge buffer tank at regular time through a time sequence control valve.
The flow of the return sludge accounts for 5 to 20 percent of the total amount of the generated sludge.
The sludge buffer tank is provided with a stirrer, the concentrated sludge entering the sludge buffer tank is further concentrated, clear liquid formed at the upper part overflows to a slag slurry collecting tank through a pipeline, the solid content of the further concentrated sludge at the bottom is improved to 3-20%, and the further concentrated sludge is sent into the vacuum drum dehydrator through the control of a switch valve.
The vacuum drum dehydrator is provided with a vacuum pump and a separation tank, concentrated sludge entering the vacuum drum dehydrator is attached to the surface of filter cloth covered on the surface of the rotating drum which rotates continuously, negative pressure is formed inside the rotating drum through the vacuum pump, a liquid phase enters the inside of the rotating drum through the filter cloth under vacuum adsorption, enters the separation tank through a pipeline and is finally discharged to a slurry collecting tank through the pipeline; the solid particles are intercepted by the filter cloth and form a filter cake on the surface of the filter cloth, the filter cake on the filter cloth is scraped off and collected by a scraper on the rotary drum along with the rotation of the rotary drum, and the solid content of the collected filter cake is 45-65 percent.
The slag slurry collecting tank is provided with a stirrer, and liquid phases collected by the slag slurry collecting tank and coming from the slag slurry buffer tank and the liquid separating tank are pressurized to 0.2-0.5 Mpag by the slag slurry collecting tank pump and are converged into desulfurization wastewater coming from a boundary area.
Compared with the prior art, the utility model has the following advantages:
1. the sludge backflow is adopted, so that the flocculation efficiency of suspended matters is improved;
2. the sedimentation effect is improved and the quality of the clear water is ensured through gravity sedimentation and inclined tube sedimentation;
3. the high vacuum degree formed by the vacuum drum dehydrator improves the solid content of the mud cake delivered outside, reduces the subsequent treatment difficulty and reduces the occupied area of the device.
Drawings
FIG. 1 is a flow chart of an embodiment of the present invention.
Detailed Description
The utility model is described in further detail below with reference to the accompanying examples.
Example 1:
as shown in fig. 1, the device for treating suspended solids in desulfurization wastewater from catalytic cracking of the present embodiment comprises:
the high-density settler 1 is used for carrying out fractional settlement on the desulfurization wastewater;
a first mixer 16, arranged upstream of the high-density settler 1, for mixing the desulfurized wastewater with a flocculant from a battery-limits zone;
the second mixer 17 is arranged between the first mixer and the high-density settler 1 and is used for mixing part of the concentrated sludge from the first mixer 16 and from the bottom of the high-density settler 1 and conveying the mixed sludge to the high-density settler 1;
the sludge buffer tank 2 is arranged at the downstream of the high-density settler 1 and is used for further concentrating part of concentrated sludge output from the bottom of the high-density settler 1;
the vacuum drum dehydrator 4 is arranged at the downstream of the sludge buffer tank 2 and is used for receiving the concentrated sludge output from the bottom of the sludge buffer tank 2 and carrying out liquid-solid separation on the concentrated sludge;
the slurry collecting tank 7 is arranged at the downstream of the vacuum drum dehydrator 4, is connected with the top of the vacuum drum dehydrator 4 so as to receive the liquid phase separated by the vacuum drum dehydrator 4, and is connected with the top of the sludge buffer tank 2 so as to receive the liquid phase separated by the sludge buffer tank 2; the slurry collecting tank 7 is also connected with the downstream of the first mixer 16 and the upstream of the second mixer 17 through pipelines.
The high-density settler 1 comprises a gravity settling zone 11, an inclined tube settling zone 12 and a clear water zone 13 which are sequentially arranged from bottom to top, the second mixer 17 is communicated with the gravity settling zone 11, and the clear water zone 13 is connected with a pipeline for outputting clear liquid.
Still be provided with first agitator and mud scraper 14 in the high density settler 1, first agitator is located gravity settling zone 11 middle part, mud scraper 14 is located gravity settling zone 11 bottom and presses close to the interior bottom arrangement of high density settler 1.
The sludge buffer tank 2 is connected with the bottom of the high-density settler 1, a valve 15 for controlling the flow of fluid is arranged between the sludge buffer tank 2 and the high-density settler, and a second stirrer 22 is arranged in the sludge buffer tank 2.
A rotary drum 42 capable of rotating is arranged in the vacuum rotary drum dehydrator 4, the periphery of the rotary drum is covered with filter cloth, the interior of the rotary drum is hollow and is connected with a vacuum pump 6 and a separating tank 5, and a scraper 43 used for scraping and collecting filter cakes on the outer wall of the filter cloth is also arranged in the vacuum rotary drum dehydrator 4.
The vacuum drum dehydrator 4 is further provided with a third stirrer 41 for stirring the material.
The bottom of the separation tank 5 is connected with a slurry collecting tank 7, and a fourth stirrer 71 is arranged in the slurry collecting tank 7.
A slurry collecting tank pump 8 for conveying the liquid phase upwards is arranged between the slurry collecting tank 7 and the second mixer 17.
A sludge reflux pump 3 is arranged between the high-density settler 1 and the second mixer 17.
The method for treating the catalytic cracking desulfurization wastewater suspended solids comprises the following steps:
the desulfurization waste water from the catalytic cracking flue gas desulfurization system is conveyed to the high-density settler 1 through a pipeline, wherein the temperature is 58 ℃, the pressure is 0.4Mpag, and the content of suspended matters is 3000 mg/L.
The flocculating agent from the battery limits is mixed into the desulfurization wastewater from the catalytic cracking flue gas desulfurization system through a pipeline and is fully mixed with the desulfurization wastewater through the first mixer 16 to form suspended solid flocs.
The concentrated sludge from the high-density settler is pressurized to 0.4Mpag by a sludge reflux pump 3 and is fully mixed with the desulfurization wastewater by a second mixer 17, so that the generation of suspended matter flocs is further accelerated.
The desulfurization wastewater sent into the high-density settler 1 firstly enters a gravity settling zone 11 at the middle lower part of the high-density settler, and large-particle suspended matter flocs formed are settled at the bottom of the high-density settler under the action of gravity.
The desulfurized wastewater after the preliminary sedimentation enters a high-density settler inclined tube sedimentation zone 12, small particle suspended solid floc generated in the desulfurized wastewater is deposited on the surface of an inclined tube and slides to the bottom of the high-density settler, and settled clear water enters a high-density settler clear water zone 13 and is conveyed to the downstream through a pipeline, wherein the concentration of the clear water suspended solid is 20 mg/L.
The solid content of the concentrated sludge settled at the bottom of the high-density settler 1 is 3wt percent and divided into two strands, one strand is sent to a sludge reflux pump 3 through a pipeline to be pressurized and finally mixed into the desulfurization wastewater; one stream is used for sending the concentrated sludge to the sludge buffer tank 2 through a time sequence control valve 15.
The flow of the sludge sent to the return sludge pump 3 accounts for 10 percent of the total amount of the generated sludge.
The sludge buffer tank 2 is provided with a stirrer 22, the concentrated sludge entering the sludge buffer tank 2 is further concentrated, clear liquid formed at the upper part overflows to a slag slurry collecting tank 7 through a pipeline, the solid content of the sludge further concentrated at the bottom is improved to 5 wt%, and the sludge is sent into the vacuum drum dehydrator 4 through the control of a switch valve 21.
The concentrated sludge entering the vacuum drum dehydrator 4 is attached to the surface of the filter cloth covered on the surface of the rotating drum 42 which rotates continuously, negative pressure is formed inside the rotating drum 42 through the vacuum pump 6, and the liquid phase enters the inside of the rotating drum 42 through the filter cloth under vacuum adsorption, enters the separation tank 5 through a pipeline and is finally discharged to the slurry collecting tank 7 through the pipeline; the solid particles are intercepted by the filter cloth and form a filter cake on the surface of the filter cloth, the filter cake on the filter cloth is scraped off and collected by a scraper 43 on the rotary drum along with the rotation of the rotary drum 42, and the solid rate of the collected filter cake is 50 percent.
The liquid phase collected by the slag slurry collecting pool 7 and coming from the slag slurry buffer tank 2 and the liquid separating tank 5 is pressurized to 0.4Mpag by the slag slurry collecting pool pump 8 and is converged into the desulfurization wastewater coming from the battery limits.
Directional terms such as "front," "rear," "upper," "lower," "left," "right," "side," "top," "bottom," and the like are used in the description and claims of the present invention to describe various example structural portions and elements of the utility model, but are used herein for convenience of description only and are to be determined based on the example orientations shown in the drawings. Because the disclosed embodiments of the present invention may be oriented in different directions, the directional terms are used for descriptive purposes and are not to be construed as limiting, e.g., "upper" and "lower" are not necessarily limited to directions opposite to or coincident with the direction of gravity.
Claims (9)
1. A catalytic cracking desulfurization waste water suspended solid processing apparatus which characterized in that includes:
the high-density settler (1) is used for carrying out fractional settlement on the desulfurization wastewater;
a first mixer (16) arranged upstream of the high-density settler (1) for mixing the desulfurized wastewater with a flocculant from a battery-limits zone;
the second mixer (17) is arranged between the first mixer and the high-density settler (1) and is used for mixing part of concentrated sludge from the first mixer (16) and from the bottom of the high-density settler (1) and conveying the mixed sludge to the high-density settler (1);
the sludge buffer tank (2) is arranged at the downstream of the high-density settler (1) and is used for further concentrating part of concentrated sludge output from the bottom of the high-density settler (1);
the vacuum drum dehydrator (4) is arranged at the downstream of the sludge buffer tank (2) and is used for receiving the concentrated sludge output from the bottom of the sludge buffer tank (2) and carrying out liquid-solid separation on the concentrated sludge;
the slag slurry collecting tank (7) is arranged at the downstream of the vacuum drum dehydrator (4), is connected with the top of the vacuum drum dehydrator (4) so as to receive the liquid phase separated by the vacuum drum dehydrator (4), and is connected with the top of the sludge buffer tank (2) so as to receive the liquid phase separated by the sludge buffer tank (2); the slag slurry collecting tank (7) is also connected with the downstream of the first mixer (16) and the upstream of the second mixer (17) through pipelines.
2. The apparatus for treating suspended solid of desulfurization wastewater from catalytic cracking as claimed in claim 1, wherein: high density settler (1) is including the gravity settling zone (11), pipe chute settling zone (12) and clear water district (13) that arrange in proper order from bottom to top, second blender (17) are linked together with gravity settling zone (11), clear water district (13) are connected with the pipeline that is used for exporting the clear liquid.
3. The apparatus for treating suspended solid of desulfurization wastewater from catalytic cracking as claimed in claim 2, wherein: still be provided with first agitator and mud scraper (14) in high density settler (1), first agitator is located gravity settling zone (11) middle part, mud scraper (14) are located gravity settling zone (11) bottom and are pressed close to the interior bottom arrangement of high density settler (1).
4. The catalytic cracking desulfurization wastewater suspension treatment apparatus as set forth in claim 1, 2 or 3, characterized in that: the sludge buffer tank (2) is connected with the bottom of the high-density settler (1), a valve (15) for controlling the circulation of fluid is arranged between the sludge buffer tank and the high-density settler, and a second stirrer (22) is arranged in the sludge buffer tank (2).
5. The catalytic cracking desulfurization wastewater suspension treatment apparatus as set forth in claim 1, 2 or 3, characterized in that: be provided with ability pivoted rotary drum (42) in vacuum rotary drum hydroextractor (4), this rotary drum periphery covers there is the filter cloth, the inside cavity of rotary drum just is connected with vacuum pump (6) and knockout drum (5), still be provided with in vacuum rotary drum hydroextractor (4) and be used for scraping down scraper blade (43) of collection with the filter cake on the filter cloth outer wall.
6. The apparatus for treating suspended solid of desulfurization wastewater from catalytic cracking as claimed in claim 5, wherein: and a third stirrer (41) for stirring the materials is also arranged in the vacuum drum dehydrator (4).
7. The apparatus for treating suspended solid of desulfurization wastewater from catalytic cracking as claimed in claim 5, wherein: the bottom of knockout drum (5) is connected with sediment thick liquid collecting pit (7), be provided with fourth agitator (71) in sediment thick liquid collecting pit (7).
8. The catalytic cracking desulfurization wastewater suspension treatment apparatus as set forth in claim 1, 2 or 3, characterized in that: and a slurry collecting tank pump (8) for conveying the liquid phase upwards is arranged between the slurry collecting tank (7) and the second mixer (17).
9. The catalytic cracking desulfurization wastewater suspension treatment apparatus as set forth in claim 1, 2 or 3, characterized in that: and a sludge reflux pump (3) is arranged between the high-density settler (1) and the second mixer (17).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202123425463.7U CN216918850U (en) | 2021-12-29 | 2021-12-29 | Catalytic cracking desulfurization waste water suspended solid processing apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202123425463.7U CN216918850U (en) | 2021-12-29 | 2021-12-29 | Catalytic cracking desulfurization waste water suspended solid processing apparatus |
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| CN216918850U true CN216918850U (en) | 2022-07-08 |
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| CN202123425463.7U Active CN216918850U (en) | 2021-12-29 | 2021-12-29 | Catalytic cracking desulfurization waste water suspended solid processing apparatus |
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| CN (1) | CN216918850U (en) |
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