CN216704370U - Hydrolysis equipment is used in production of oxolinic acid - Google Patents

Hydrolysis equipment is used in production of oxolinic acid Download PDF

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Publication number
CN216704370U
CN216704370U CN202123292996.2U CN202123292996U CN216704370U CN 216704370 U CN216704370 U CN 216704370U CN 202123292996 U CN202123292996 U CN 202123292996U CN 216704370 U CN216704370 U CN 216704370U
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wall
fixedly connected
rotary drum
net
oxolinic acid
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CN202123292996.2U
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王冰超
曹宜申
张齐伟
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Dalian Baosheng Fine Chemical Technology Co ltd
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Dalian Baosheng Fine Chemical Technology Co ltd
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Abstract

The utility model discloses hydrolysis equipment for producing oxolinic acid, which comprises an outer barrel, wherein a discharge valve is arranged at the bottom of the outer wall of the side surface of the outer barrel, a feeding mechanism is arranged at the top of the outer barrel, a liquid feeding pipe is inserted into one side of the outer wall of the top of the outer barrel, the inner wall of the bottom of the outer barrel is rotatably connected with a rotary drum, a driving motor which is in transmission fit with the rotary drum is fixedly connected with the outer wall of the bottom of the outer barrel, three net rings which are uniformly distributed up and down are arranged on the outer side of the rotary drum, a separation net is fixedly connected with the inner wall of the side surface of each net ring, the aperture of each separation net is gradually reduced from top to bottom, the outer wall of the side surface of the rotary drum, which is positioned above the net rings, is fixedly connected with stirring rods which are uniformly distributed in an annular shape, and the feeding mechanism is arranged at the top of the outer barrel. The utility model layers the solid of the oxolinic acid by the multilayer separation net, then leads the oxolinic acid falling on the separation net to float by the upward liquid flow generated by the axial flow paddle at the bottom, and then leads the oxolinic acid to be stirred by the stirring rod, thereby improving the hydrolysis efficiency.

Description

Hydrolysis equipment is used in production of oxolinic acid
Technical Field
The utility model relates to the technical field of chemical production, in particular to hydrolysis equipment for producing oxolinic acid.
Background
Oxolinic acid is also known as oxolinic acid, oxolinic acid and the like, and the chemical name is as follows: 1-ethyl-6, 7-methyleneoxy-4-oxine-copper-3-carboxylic acid, the raw medicine is low in toxicity, has no stimulation to skin, has mild stimulation to eyes and no sensitization, has no teratogenesis, carcinogenesis and mutagenesis effects in animal tests, and the oxolinic acid belongs to a second-generation quinolinone bactericide.
The hydrolysis of the oxolinic acid is a process of decomposing a substance into a new substance by using water, the hydrolysis is a reaction of the substance and the water which causes the substance to be decomposed, and can also be said to be a reaction of the substance and hydrogen ions or hydroxyl ions in the water, however, the oxolinic acid is very difficult to dissolve in the water, the dissolution efficiency of the oxolinic acid is improved by the existing hydrolysis device only by stirring, but the oxolinic acid is easy to be accumulated together after being added into the hydrolysis device, so that the dissolution is very slow, and the hydrolysis efficiency is low.
SUMMERY OF THE UTILITY MODEL
The utility model aims to solve the defects in the prior art and provides hydrolysis equipment for producing oxolinic acid.
In order to achieve the purpose, the utility model adopts the following technical scheme:
the utility model provides a hydrolysis equipment is used in production of paoquizac acid, includes outer barrel, and the side outer wall bottom of outer barrel is provided with the bleeder valve, the top of outer barrel is provided with reinforced mechanism, and pegs graft in top outer wall one side of outer barrel has the liquid feeding pipe, the bottom inner wall of outer barrel rotates and is connected with the rotary drum, and the bottom outer wall fixedly connected with of outer barrel forms transmission complex driving motor with the rotary drum, the outside of rotary drum is provided with three net circle of evenly distributed from top to bottom, and the side inner wall fixedly connected with of net circle separates the net, and the aperture that separates the net reduces from top to bottom gradually, and the rotary drum is located the stirring rod of the side outer wall fixedly connected with annular evenly distributed of net circle top, and the top of outer barrel is provided with reinforced mechanism, the side outer wall bottom fixedly connected with axial compressor paddle leaf of rotary drum.
Preferably, reinforced mechanism is including seting up the round hole in outer barrel top outer wall, and the top of round hole is provided with the hopper of fixed connection in outer barrel top outer wall.
Preferably, the side inner wall of round hole rotates and is connected with down the charging tray, and unloading dish fixed connection in the side outer wall of rotary drum, and the top outer wall fixed connection of unloading dish has the guide block, and the unloading dish is located the top outer wall of guide block one side and opens the unloading hole that has two annular evenly distributed.
Preferably, the spiral blade is fixedly connected to the inner wall of the side surface of the rotating drum, the liquid spraying hole is formed in the top of the inner wall of the side surface of the rotating drum, the flow guide hole is formed in the bottom of the inner wall of the side surface of the rotating drum, and the flow guide hole is located below the axial flow blade.
Preferably, a separating cylinder is fixedly connected between the inner wall of the bottom part and the inner wall of the top part of the outer cylinder body, a flow guide gap is reserved between the outer wall of the side surface of the separating cylinder and the inner wall of the side surface of the outer cylinder body, a backflow hole is formed in the bottom of the inner wall of the side surface of the separating cylinder, and an upper flow guide hole is formed in the top of the inner wall of the side surface of the separating cylinder.
Preferably, the side inner wall of the separating cylinder is provided with an annular chute positioned on one side of the net ring, the net ring is connected to the side inner wall of the chute in a sliding manner, and a spring is fixedly connected between the bottom outer wall of the net ring and the bottom inner wall of the chute.
Preferably, the outer wall of the side surface of the rotating cylinder is fixedly connected with a support ring positioned below the net ring, the top of the support ring is fixedly connected with lower convex particles which are uniformly distributed in an annular manner, and the outer wall of the bottom of the net ring is fixedly connected with upper convex particles which are uniformly distributed in an annular manner.
Compared with the prior art, the hydrolysis equipment for producing the oxolinic acid provided by the utility model has the following beneficial effects: through the inside at outer barrel sets up the multilayer and separates net and puddler, can separate the layering of clomazel acid solid by the multilayer after the clomazel acid solid is added to outer barrel, and the ascending liquid stream that the axial compressor paddle of rethread bottom produced makes the clomazel acid that falls on separating the net float, stirs by the puddler again, and then can improve the efficiency of hydrolysising.
Drawings
FIG. 1 is a schematic view of the overall structure of a hydrolysis apparatus for producing oxolinic acid according to the present invention;
FIG. 2 is a schematic diagram of the internal structure of a hydrolysis apparatus for producing oxolinic acid provided by the present invention;
FIG. 3 is a schematic structural diagram of the part A in FIG. 2 of a hydrolysis device for producing oxolinic acid provided by the present invention;
FIG. 4 is a schematic structural diagram of a hydrolysis device for producing oxolinic acid shown in FIG. 2, wherein the structural diagram is B.
In the figure: the device comprises an outer cylinder body 1, a liquid feeding pipe 2, a hopper 3, a discharging hole 4, a material guiding block 5, a driving motor 6, a discharging disc 7, a liquid spraying hole 8, a spiral blade 9, a separating cylinder 10, a rotating cylinder 11, a stirring rod 12, a discharging valve 13, an axial flow blade 14, a flow guide hole 15, a backflow hole 16, a separating net 17, an upper flow guide hole 18, an annular sliding groove 19, a net ring 20, a spring 21, an upper convex particle 22, a support ring 23 and a lower convex particle 24.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
In the description of this patent, it is noted that unless otherwise specifically stated or limited, the terms "mounted," "connected," and "disposed" are to be construed broadly and can include, for example, fixedly connected, disposed, detachably connected, disposed, or integrally connected and disposed. The specific meaning of the above terms in this patent may be understood by those of ordinary skill in the art as appropriate.
In the description of the present invention, it is to be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", and the like, are used in the orientations and positional relationships indicated in the drawings, which are based on the orientations and positional relationships indicated in the drawings, and are used for convenience of description and simplicity of description, but do not indicate or imply that the devices or elements referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, are not to be construed as limiting the present invention.
Referring to fig. 1-4, a hydrolysis device for producing oxolinic acid comprises an outer cylinder body 1, a discharge valve 13 is arranged at the bottom of the outer wall of the side surface of the outer cylinder body 1, a feeding mechanism is arranged at the top of the outer cylinder body 1, and one side of the outer wall of the top of the outer cylinder 1 is inserted with a liquid feeding pipe 2, the inner wall of the bottom of the outer cylinder 1 is rotationally connected with a rotary drum 11, and the outer wall of the bottom of the outer cylinder body 1 is fixedly connected with a driving motor 6 which forms transmission fit with the rotary drum 11, three net rings 20 which are uniformly distributed up and down are arranged on the outer side of the rotary drum 11, and the side inner wall fixedly connected with of wire netting 20 separates the net 17, separates the aperture of net 17 and reduces from top to bottom gradually, and the side outer wall fixedly connected with annular evenly distributed's puddler 12 of rotary drum 11 position above wire netting 20, the top of outer barrel 1 is provided with reinforced mechanism, and the side outer wall bottom fixedly connected with axial compressor paddle 14 of rotary drum 11.
Wherein, reinforced mechanism is provided with fixed connection in the hopper 3 of the outer wall in outer barrel 1 top including seting up the round hole in outer barrel 1 top outer wall above the round hole.
Wherein, the side inner wall of round hole rotates and is connected with down charging tray 7, and unloading tray 7 fixed connection in the side outer wall of rotary drum 11, and the top outer wall fixed connection of unloading tray 7 has guide block 5, and the top outer wall that unloading tray 7 is located guide block 5 one side is opened has two annular evenly distributed's unloading hole 4.
Wherein, the side inner wall of rotary drum 11 is fixedly connected with spiral leaf 9, and the side inner wall top of rotary drum 11 opens and has hydrojet hole 8, and the side inner wall bottom of rotary drum 11 opens and has water conservancy diversion hole 15, and water conservancy diversion hole 15 is located the below of axial compressor paddle 14.
Wherein, a separating cylinder 10 is fixedly connected between the bottom inner wall and the top inner wall of the outer cylinder 1, a flow guide gap is reserved between the side outer wall of the separating cylinder 10 and the side inner wall of the outer cylinder 1, a backflow hole 16 is arranged at the bottom of the side inner wall of the separating cylinder 10, and an upper flow guide hole 18 is arranged at the top of the side inner wall of the separating cylinder 10.
Wherein, separate the side inner wall of section of thick bamboo 10 and open and to have the annular spout 19 that is located net ring 20 one side, and net ring 20 sliding connection is in the side inner wall of spout 19, and fixedly connected with spring 21 between the bottom outer wall of net ring 20 and the bottom inner wall of spout 19.
Wherein, the outer wall of the side of the rotating cylinder 11 is fixedly connected with a support ring 23 positioned below the net ring 20, the top of the support ring 23 is fixedly connected with lower convex particles 24 which are uniformly distributed in an annular shape, and the outer wall of the bottom of the net ring 20 is fixedly connected with upper convex particles 22 which are uniformly distributed in an annular shape.
The working principle is as follows: when in use, the solid material of the oxolinic acid is added into the hopper 3, the hydrolysate is introduced into the outer cylinder body 1 through the liquid feeding pipe 2, the liquid level is higher than the upper diversion holes 18, the driving motor 6 rotates to drive the lower material disc 7 to rotate, so that the solid material of the oxolinic acid uniformly falls into the hydrolysate, the raw material is layered from top to bottom by the separation net 17 when falling in the hydrolysate, the hydrolysate generates upward liquid flow when the axial flow paddle 14 rotates, so that the solid material of the praziquantel on the separation net 17 floats upwards, then is stirred and hydrolyzed by the stirring rod 12, meanwhile, the spiral blade 9 drives the hydrolysate at the bottom to move upwards and be sprayed out from the liquid spraying hole 8, and then improve the homogeneity of dissolving, can drive through the cooperation of lower bulge 24 and upper bulge 22 when rotary drum 11 rotates and shake about separating the net 17, and then make the solid raw materials of the obtained cloquintocet acid on separating the net 17 fall the layering more easily.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and equivalent alternatives or modifications according to the technical solution of the present invention and the inventive concept thereof should be covered by the scope of the present invention.

Claims (7)

1. The hydrolysis equipment for producing the oxolinic acid comprises an outer barrel (1), wherein a discharge valve (13) is arranged at the bottom of the outer side wall of the outer barrel (1), and is characterized in that a feeding mechanism is arranged at the top of the outer barrel (1), a liquid feeding pipe (2) is inserted into one side of the outer side wall of the top of the outer barrel (1), a rotary drum (11) is rotatably connected to the inner wall of the bottom of the outer barrel (1), a driving motor (6) which is in transmission fit with the rotary drum (11) is fixedly connected to the outer wall of the bottom of the outer barrel (1), three net rings (20) which are uniformly distributed up and down are arranged on the outer side of the rotary drum (11), a separation net (17) is fixedly connected to the inner wall of the side of each net ring (20), the pore diameter of each separation net (17) is gradually reduced from top to bottom, and stirring rods (12) which are uniformly distributed in an annular shape are fixedly connected to the outer side wall of the rotary drum (11) which is positioned above each net ring (20), the top of outer barrel (1) is provided with reinforced mechanism, and the side outer wall bottom fixedly connected with axial compressor paddle (14) of rotary drum (11).
2. The hydrolysis equipment for the production of the oxolinic acid as claimed in claim 1, wherein the feeding mechanism comprises a circular hole arranged on the outer wall of the top of the outer cylinder body (1), and a hopper (3) fixedly connected to the outer wall of the top of the outer cylinder body (1) is arranged above the circular hole.
3. The hydrolysis equipment for producing the oxolinic acid as claimed in claim 2, wherein the inner wall of the side surface of the round hole is rotatably connected with a discharging tray (7), the discharging tray (7) is fixedly connected with the outer wall of the side surface of the rotary drum (11), the outer wall of the top part of the discharging tray (7) is fixedly connected with a material guide block (5), and the outer wall of the top part of the discharging tray (7) on one side of the material guide block (5) is provided with two discharging holes (4) which are uniformly distributed in an annular shape.
4. The hydrolysis equipment for producing the oxolinic acid as claimed in claim 1, wherein the inner wall of the side surface of the rotary drum (11) is fixedly connected with a spiral blade (9), the top of the inner wall of the side surface of the rotary drum (11) is provided with a liquid spraying hole (8), the bottom of the inner wall of the side surface of the rotary drum (11) is provided with a flow guide hole (15), and the flow guide hole (15) is positioned below the axial flow blade (14).
5. The hydrolysis equipment for producing the oxolinic acid as claimed in claim 1, wherein a separation barrel (10) is fixedly connected between the inner wall of the bottom and the inner wall of the top of the outer barrel body (1), a flow guide gap is left between the outer wall of the side surface of the separation barrel (10) and the inner wall of the side surface of the outer barrel body (1), a backflow hole (16) is formed at the bottom of the inner wall of the side surface of the separation barrel (10), and an upper flow guide hole (18) is formed at the top of the inner wall of the side surface of the separation barrel (10).
6. The hydrolysis equipment for producing the oxolinic acid as claimed in claim 5, wherein an annular chute (19) is formed in the inner wall of the side surface of the separation cylinder (10) and is positioned on one side of the net ring (20), the net ring (20) is slidably connected to the inner wall of the side surface of the chute (19), and a spring (21) is fixedly connected between the outer wall of the bottom of the net ring (20) and the inner wall of the bottom of the chute (19).
7. The hydrolysis equipment for producing the oxolinic acid as claimed in claim 6, wherein a support ring (23) positioned below the net ring (20) is fixedly connected to the outer wall of the side surface of the rotary drum (11), lower convex particles (24) which are uniformly distributed in an annular shape are fixedly connected to the top of the support ring (23), and upper convex particles (22) which are uniformly distributed in an annular shape are fixedly connected to the outer wall of the bottom of the net ring (20).
CN202123292996.2U 2021-12-25 2021-12-25 Hydrolysis equipment is used in production of oxolinic acid Active CN216704370U (en)

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CN202123292996.2U CN216704370U (en) 2021-12-25 2021-12-25 Hydrolysis equipment is used in production of oxolinic acid

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Application Number Priority Date Filing Date Title
CN202123292996.2U CN216704370U (en) 2021-12-25 2021-12-25 Hydrolysis equipment is used in production of oxolinic acid

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115282736A (en) * 2022-07-07 2022-11-04 唐山国环环保科技有限公司 Exhaust device for ammonia water safety production
CN115678769A (en) * 2022-11-15 2023-02-03 河北壳亮生物科技有限公司 Biological enzymolysis tank

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115282736A (en) * 2022-07-07 2022-11-04 唐山国环环保科技有限公司 Exhaust device for ammonia water safety production
CN115282736B (en) * 2022-07-07 2023-11-03 唐山国环环保科技有限公司 Exhaust device for ammonia water safety production
CN115678769A (en) * 2022-11-15 2023-02-03 河北壳亮生物科技有限公司 Biological enzymolysis tank

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