CN216604048U - A multistage purification device for chemical industry is synthetic - Google Patents
A multistage purification device for chemical industry is synthetic Download PDFInfo
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- CN216604048U CN216604048U CN202122622600.XU CN202122622600U CN216604048U CN 216604048 U CN216604048 U CN 216604048U CN 202122622600 U CN202122622600 U CN 202122622600U CN 216604048 U CN216604048 U CN 216604048U
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- 238000000746 purification Methods 0.000 title claims abstract description 31
- 239000000126 substance Substances 0.000 title claims description 5
- 238000003786 synthesis reaction Methods 0.000 claims abstract description 17
- 238000003756 stirring Methods 0.000 abstract description 24
- 230000000694 effects Effects 0.000 abstract description 8
- 238000010438 heat treatment Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 230000005540 biological transmission Effects 0.000 description 5
- 239000003153 chemical reaction reagent Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 3
- 238000007599 discharging Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 238000010795 Steam Flooding Methods 0.000 description 1
- 230000003044 adaptive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000012824 chemical production Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
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Abstract
The utility model relates to the field of chemical synthesis, in particular to a multistage purification device for chemical synthesis, which comprises a first box body, wherein a second box body is fixed in an inner cavity of the first box body, a filter screen is fixed on the lower side of the inner cavity of the second box body, the top of the second box body is fixedly communicated with a feed pipe, the feed pipe penetrates through the first box body, the right side wall of the first box body is fixedly connected with a power box, the top of the power box is fixedly communicated with a steam pipe, the tail end of the power box is communicated with the first box body through a conduit, and a first rotating shaft is arranged in the inner cavity of the power box. The utility model can generate gas through the air pump to act on the surface of the blade, thereby generating auxiliary power or resistance, and simultaneously, the rotating speed of the stirring rod can be detected by utilizing the rotating speed sensor, so that the stirring rod can be in the optimal stirring speed, thereby avoiding the situation of insufficient stirring or excessive stirring, effectively ensuring the purification effect, being more practical and being suitable for wide popularization and use.
Description
Technical Field
The utility model relates to the field of chemical synthesis, in particular to a multistage purification device for chemical synthesis.
Background
Separation and purification means separating impurities from a mixture to improve the purity of the mixture. The separation and purification as an important chemical method not only has important function in chemical research, but also has very important function in chemical production.
Current patent number CN202021524202.3 discloses a multistage purification device for chemical reagent synthetic production, relates to chemical reagent technical field. This a multistage purification device for synthetic production of chemical reagent, comprising a base plate, the top fixed mounting of bottom plate has the box, and the inside of box is provided with the purification case, and the top fixed mounting of bottom plate has the fixed plate, and the opposite side outer wall fixed mounting of fixed plate has the transmission case, and the top fixedly connected with steam inlet pipe and the steam inlet pipe of transmission case extend to the inside of transmission case, and the bottom fixed mounting of transmission case has the second steam inlet pipe and the inside of second steam inlet pipe and transmission case communicates with each other. Use through the cooperation of dwang, guide vane and stirring leaf, make steam drive dwang, guide vane and stirring leaf move, reduced the consumption of the energy, prevent to appear the caking among the reagent heating process and lead to the inhomogeneous condition of reagent purification to take place, improved work efficiency, saved operating time.
Above-mentioned patent is at the in-process of in-service use, drives the dwang through steam and rotates, but has steam power not enough or have steam power too big, and the stirring leaf stirs excessively to influence the purification effect, though utilize steam to heat from the outer wall simultaneously, and the inhomogeneous condition of inside heating exists at any time. Therefore, we propose a multi-stage purification device for chemical synthesis.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide a multistage purification device for chemical synthesis, which solves the problems in the background technology.
In order to achieve the purpose, the utility model provides the following technical scheme: a multi-stage purification device for chemical synthesis comprises a first box body, wherein a second box body is fixed in an inner cavity of the first box body, and a filter screen is fixed on the lower side of the inner cavity of the second box body;
the top of the second box body is fixedly communicated with an inlet pipe, the inlet pipe penetrates through the first box body, the right side wall of the first box body is fixedly connected with a power box, the top of the power box is fixedly communicated with a steam pipe, the tail end of the power box is communicated with the first box body through a pipe, a first rotating shaft is arranged in an inner cavity of the power box, the outer wall of the first rotating shaft is fixedly provided with first blades, the outer end of the first rotating shaft penetrates through the first box body and the second box body and is fixedly connected with a second rotating shaft, the second rotating shaft penetrates through the second box body and the first box body and is fixedly connected with a rotary table, the outer wall of the rotary table is uniformly provided with second blades, the outer wall of the rotary table is fixedly provided with a rotating speed sensor, the upper side of the outer wall of the first box body is fixedly provided with a controller, the upper side wall and the lower side of the left side wall of the first box body are respectively provided with an air pump, and the outlet pipes of the two sets of the air pumps are obliquely aligned to the second blades in a staggered manner, the outer wall fixedly connected with puddler of first pivot.
As a preferred embodiment of the present invention, the first rotating shaft and the stirring rod are respectively a hollow rotating shaft and a hollow stirring rod, the first rotating shaft is communicated with the stirring rod, and the outer end of the stirring rod is fixedly connected with a one-way valve.
As a preferred embodiment of the present invention, the signal output ends of the rotation speed sensors are respectively communicated with the two sets of air pumps.
In a preferred embodiment of the present invention, the top portions of the first tank and the second tank are both communicated with a relief valve.
In a preferred embodiment of the present invention, a first discharge pipe and a second discharge pipe are respectively connected to a lower side of a left side wall of the second tank.
Compared with the prior art, the utility model has the following beneficial effects:
1. according to the multistage purification device for chemical synthesis, disclosed by the utility model, the gas generated by the gas pump acts on the surface of the blade, so that auxiliary power or resistance can be generated, and meanwhile, the rotating speed of the stirring rod can be detected by using the rotating speed sensor, so that the stirring rod can be at the optimal stirring speed, the situation that stirring is insufficient or excessive is avoided, and the purification effect is effectively ensured.
2. According to the multi-stage purification device for chemical synthesis, the first rotating shaft and the stirring rod are hollow, so that steam can be guided into the second box body to heat the interior of a material, double heating is realized, the heating uniformity is further ensured, and the purification effect can be further ensured.
Drawings
Other features, objects and advantages of the utility model will become more apparent upon reading of the detailed description of non-limiting embodiments with reference to the following drawings:
FIG. 1 is a schematic diagram of the overall structure of a multistage purification apparatus for chemical synthesis according to the present invention;
FIG. 2 is a schematic view of the structure of a turntable of the multi-stage purification device for chemical synthesis according to the present invention.
In the figure: 1. a first case; 2. a second case; 3. a power box; 4. a steam pipe; 5. a first rotating shaft; 6. a first blade; 7. a stirring rod; 8. filtering with a screen; 9. a conduit; 10. a second rotating shaft; 11. a feed pipe; 12. a first discharge pipe; 13. a second discharge pipe; 14. a controller; 15. an air pump; 16. a turntable; 17. a second blade; 18. a rotation speed sensor.
Detailed Description
Referring to fig. 1-2, the present invention provides a technical solution: a multi-stage purification device for chemical synthesis comprises a first box body 1, wherein a second box body 2 is fixed in an inner cavity of the first box body 1, and a filter screen 8 is fixed on the lower side of the inner cavity of the second box body 2;
the top of the second box body 2 is fixedly communicated with an inlet pipe 11, the inlet pipe 11 penetrates through the first box body 1, the right side wall of the first box body 1 is fixedly connected with a power box 3, the top of the power box 3 is fixedly communicated with a steam pipe 4, the tail end of the power box 3 is communicated with the first box body 1 through a pipe 9, a first rotating shaft 5 is arranged in an inner cavity of the power box 3, a first blade 6 is fixed on the outer wall of the first rotating shaft 5, the outer end of the first rotating shaft 5 penetrates through the first box body 1 and the second box body 2 and is fixedly connected with a second rotating shaft 10, the second rotating shaft 10 penetrates through the second box body 2 and the first box body 1 and is fixedly connected with a turntable 16, second blades 17 are uniformly distributed on the outer wall of the turntable 16, a rotating speed sensor 18 is fixed on the outer wall of the turntable 16, a controller 14 is fixedly mounted on the upper side of the outer wall of the first box body 1, an air pump 15 is fixedly mounted on the upper portion and the lower portion of the left side wall of the first box body 1, the air outlet pipes of the two groups of air pumps 15 are obliquely aligned to the second blades 17 in a staggered mode, and the outer wall of the first rotating shaft 5 is fixedly connected with a stirring rod 7.
In this embodiment, can monitor the rotational speed through speed sensor 18, then start air pump 15 and carry out auxiliary power or provide the resistance to guarantee that puddler 7 can be in best stirring speed, thereby promoted the purification effect.
In this embodiment, first pivot 5 and puddler 7 are hollow pivot and hollow puddler 7 and first pivot 5 and puddler 7 intercommunication respectively, the outer end fixedly connected with check valve of puddler 7 for steam can get into and heat in the second box 2, thereby promotes the heating effect.
In this embodiment, the signal output ends of the rotation speed sensors 18 are respectively communicated with the two sets of air pumps 15, so that automatic control is realized.
In this embodiment, the top of the first box 1 and the top of the second box 2 are both communicated with a pressure release valve, so that the pressure is balanced.
In this embodiment, a first discharge pipe 12 and a second discharge pipe 13 are respectively connected to the lower side of the left sidewall of the second tank 2, the first discharge pipe 12 is disposed on the upper side of the filter screen 8, and the second discharge pipe 13 is disposed on the lower side of the filter screen 8.
The working principle is as follows: when the device is used, firstly, materials are guided into the inner cavity of the second box body 2 through the feeding pipe 11, then the materials are guided into the power box 3 through steam, so that the first blade 6 can be driven to rotate, further, the first rotating shaft 5 is driven to rotate, further, the stirring rod 7 is driven to stir the materials, then the steam enters the inner cavity of the first box body 1 to be heated, meanwhile, the steam enters the cavity of the first rotating shaft 5 and then enters the cavity of the stirring rod 7, further, the steam enters the inner cavity of the second box body 2 through the one-way valve to heat the interior of the materials, so that the heating effect is ensured, meanwhile, the rotating speed sensor 18 monitors the rotating speed, when the device is not at the optimal rotating speed, the controller 14 can aim at one of the two groups of air pumps 15 which is started too fast or too slow, so that the air is blown to the surface of the second blade 17 to generate auxiliary power or resistance, thereby ensuring that the rotating speed is at the optimal rotating speed, thereby guaranteed the effect of purification, can utilize first discharging pipe 12 and second discharging pipe 13 to derive the material respectively after the purification, simultaneously at the in-process of in-service use, the relief valve at the top of first box 1 and second box 2 can carry out the pressure release, guarantees pressure balance.
In addition, the parts included in the multistage purification device for chemical synthesis of the utility model are all universal standard parts or parts known by technicians in the field, the structure and principle of the device can be known by technicians through technical manuals or conventional experimental methods, at the idle position of the device, all the electric devices refer to power elements, electric devices, adaptive monitoring computers and power supplies which are connected through leads, and specific connection means are provided.
Claims (5)
1. The utility model provides a multistage purification device for chemical industry is synthetic, includes first box (1), its characterized in that: a second box body (2) is fixed in the inner cavity of the first box body (1), and a filter screen (8) is fixed on the lower side of the inner cavity of the second box body (2);
the top of the second box body (2) is fixedly communicated with an inlet pipe (11) and the inlet pipe (11) penetrates through the first box body (1), the right side wall of the first box body (1) is fixedly connected with a power box (3), the top of the power box (3) is fixedly communicated with a steam pipe (4), the tail end of the power box (3) is communicated with the first box body (1) through a pipe (9), a first rotating shaft (5) is arranged in the inner cavity of the power box (3), the outer wall of the first rotating shaft (5) is fixed with a first blade (6), the outer end of the first rotating shaft (5) penetrates through the first box body (1) and the second box body (2) and is fixedly connected with a second rotating shaft (10), the second rotating shaft (10) penetrates through the second box body (2) and the first box body (1) and is fixedly connected with a turntable (16), and second blades (17) are uniformly distributed on the outer wall of the turntable (16), carousel (16) outer wall is fixed with speed sensor (18), the outer wall upside fixed mounting of first box (1) has controller (14), all be fixed with air pump (15) from top to bottom on the left side wall of first box (1), two sets of the crisscross slope of outlet duct of air pump (15) is aimed at second blade (17), the outer wall fixedly connected with puddler (7) of first pivot (5).
2. The multi-stage purification device for chemical synthesis according to claim 1, wherein: first pivot (5) and puddler (7) are hollow pivot and hollow puddler (7) and first pivot (5) and puddler (7) intercommunication respectively, the outer end fixedly connected with check valve of puddler (7).
3. The multi-stage purification device for chemical synthesis according to claim 1, wherein: and the signal output ends of the rotating speed sensors (18) are respectively communicated with the two groups of air pumps (15).
4. The multi-stage purification device for chemical synthesis according to claim 1, wherein: the top parts of the first box body (1) and the second box body (2) are communicated with pressure release valves.
5. The multi-stage purification device for chemical synthesis according to claim 1, wherein: the lower side of the left side wall of the second box body (2) is respectively communicated with a first discharge pipe (12) and a second discharge pipe (13).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202122622600.XU CN216604048U (en) | 2021-10-29 | 2021-10-29 | A multistage purification device for chemical industry is synthetic |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202122622600.XU CN216604048U (en) | 2021-10-29 | 2021-10-29 | A multistage purification device for chemical industry is synthetic |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN216604048U true CN216604048U (en) | 2022-05-27 |
Family
ID=81693626
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202122622600.XU Expired - Fee Related CN216604048U (en) | 2021-10-29 | 2021-10-29 | A multistage purification device for chemical industry is synthetic |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN216604048U (en) |
-
2021
- 2021-10-29 CN CN202122622600.XU patent/CN216604048U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information |
Inventor after: Zhang Benling Inventor before: Cui Ruiping |
|
| CB03 | Change of inventor or designer information | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20220527 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |