CN216458750U

CN216458750U - Be used for immobilized ionic liquid preparation reaction unit

Info

Publication number: CN216458750U
Application number: CN202123162610.6U
Authority: CN
Inventors: 宋�莹; 王晴; 张庆达
Original assignee: Liaoyang Dongchang Chemical Co ltd
Current assignee: Liaoyang Dongchang Chemical Co ltd
Priority date: 2021-12-16
Filing date: 2021-12-16
Publication date: 2022-05-10
Anticipated expiration: 2031-12-16

Abstract

The utility model belongs to the technical field of the ionic liquid preparation equipment of solid-borne, especially, be used for ionic liquid preparation reaction unit of solid-borne, including base and reaction vessel, the equal fixed mounting in top both sides of base has the riser, and one side top that two risers are close to each other all rotates and installs the back shaft, and the one end fixed mounting that two back shafts are close to each other has same hollow slab, the installing port has been seted up on the hollow slab, and reaction vessel demountable installation in the installing port, and one side slidable mounting that two risers are close to each other has same lifter plate, fixed mounting has the platform of placing on the lifter plate. The utility model relates to a rationally, easy operation can be as required to the height of side pipe and heating device highly adjust, is convenient for get the quick of putting of going on of reaction vessel simultaneously, and can adjust reaction vessel's inclination as required, and it is comparatively convenient to use.

Description

Be used for immobilized ionic liquid preparation reaction unit

Technical Field

The utility model relates to an immobilized ionic liquid preparation equipment technical field, in particular to a preparation reaction device for immobilized ionic liquid.

Background

Need use reaction unit when the preparation of solid-borne ionic liquid, a reaction unit who needs to be used for the preparation of solid-borne ionic liquid includes three flasks, the condenser pipe, buchner flask and buchner funnel etc. reaction vessel's such as current three-neck flask opening relatively fixed, do not possess the function of regulation, simultaneously need support and supplementary regulation reaction vessel through equipment such as test-tube clamp and support frame at the in-process that carries out the preparation, be not convenient for reaction vessel's quick getting put, because the auxiliary assembly that needs to use is more, operate comparatively loaded down with trivial details, can influence the efficiency of preparation, the utility model provides a be used for solid-borne ionic liquid preparation reaction unit to solve above-mentioned problem.

SUMMERY OF THE UTILITY MODEL

The utility model aims at solving the defects of the prior art and providing a preparation reaction device for immobilized ionic liquid.

The above technical purpose of the present invention can be achieved by the following technical solutions: a reaction device for preparing immobilized ionic liquid comprises a base and a reaction container, wherein vertical plates are fixedly arranged on two sides of the top of the base, supporting shafts are rotatably arranged on the top of one side, close to each other, of each vertical plate, one end, close to each other, of each supporting shaft is fixedly provided with one hollow plate, each hollow plate is provided with a mounting opening, the reaction container is detachably arranged in the mounting opening, one side, close to each other, of each vertical plate is slidably provided with one lifting plate, a placing table is fixedly arranged on each lifting plate, one side, close to each other, of the top side of the base and one side, close to each other, of each vertical plate are provided with one lifting mechanism, a plurality of hollow cylinders are fixedly arranged on the inner side wall of each hollow plate, supporting columns are slidably arranged in the hollow cylinders, one ends, close to each supporting column, of each rotating wheel are rotatably arranged on each supporting column, and the rotating wheels are abutted to the reaction container, reaction vessel's top fixed mounting has the standpipe, two bar mouths have been seted up on reaction vessel's the outer peripheral face, equal vertical fixed mounting has the guide bar in two bar mouths, slidable mounting has the slider on the guide bar, fixed mounting has the connecting pipe on the slider, reaction vessel's one end fixed mounting is kept away from to the connecting pipe has the rotary joint, rotate on the joint and rotate and install the side pipe, and fixed cover is equipped with the radiation shield on the side pipe.

Preferably, one end of the supporting column, which is far away from the rotating wheel, is fixedly provided with a pushing spring, and one end of the pushing spring, which is far away from the supporting column, is fixedly connected with the inner wall of one side of the hollow cylinder.

Preferably, the lifting mechanism comprises a driving motor, a bidirectional lead screw, two moving blocks, a driving gear, a driven gear and two support rods, the bidirectional lead screw is horizontally rotatably installed on the two vertical plates, the driving motor is fixedly installed on the vertical plate on the right side, the driving gear and the driven gear are respectively fixedly sleeved on an output shaft of the driving motor and the bidirectional lead screw, the driving gear is meshed with the driven gear, two moving blocks are respectively and threadedly installed on the bidirectional lead screw, the two support rods are respectively and rotatably installed on the corresponding moving blocks, fixing plates are respectively and fixedly installed at two ends of the bottom side of the lifting plate, and one ends, far away from the moving blocks, of the two support rods are respectively and rotatably connected with the corresponding fixing plates.

Preferably, the last fixed mounting of runner has a branch, and the one end fixed mounting that the runner was kept away from to branch has anti-skidding rubber slab, and after reaction vessel got into the installing port and contacted with the runner, anti-skidding rubber slab and reaction vessel looks butt.

Preferably, two supporting plates are fixedly mounted on one sides, close to each other, of the two vertical plates, two guide columns are vertically and fixedly mounted on the two supporting plates on the same side, the four guide columns are connected with the lifting plate in a sliding mode, and scale plates are arranged on the guide columns.

Preferably, a sleeve is installed on the inner side wall of the reaction vessel in a sliding and sealing mode, and one end, far away from the rotary joint, of the connecting pipe penetrates through the sleeve and is communicated with the reaction vessel.

Preferably, the fixed cover of one end that the hollow plate was kept away from to the back shaft that is located the right side is equipped with the rolling disc, and the thread mounting has spacing lead screw on the rolling disc, and the one side that the hollow plate was kept away from to the riser that is located the right side has seted up a plurality of spacing screws for the centre of a circle based on the back shaft, and spacing lead screw thread mounting is in the spacing screw that corresponds, and the fixed cover of one end that the riser was kept away from to spacing lead screw is equipped with the anti-skidding handle cover.

The beneficial effects of the utility model are that: in the utility model, the lifting plate can be controlled to lift through the mutual matching between the driving motor, the rotating gear, the driven gear, the bidirectional screw rod, the moving block and the support rod, the lifting plate can be kept to stably lift under the matching of the guide post, the lifting height of the lifting plate can be accurately controlled under the matching of the scale plate, the inclination angle of the reaction vessel can be controlled through the hollow plate under the matching of the rotating disc and the support shaft, the position of the rotating disc can be fixed under the matching of the limiting screw rod and the limiting screw hole, the height of the side pipe can be adjusted according to requirements under the matching of components such as the strip-shaped port, the guide rod and the slide block, and the strip-shaped port can be sealed under the matching of the sleeve, thereby effectively avoiding the liquid leakage in the using process, when the reaction vessel is put into the mounting port, can be in the butt state with reaction vessel at support column, hollow section of thick bamboo and the cooperation that pushes away the spring down, simultaneously along with reaction vessel downstream drive runner rotates to can make branch drive anti-skidding rubber slab and reaction vessel's lateral surface butt, and then can fix reaction vessel.

Drawings

In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the drawings needed to be used in the description of the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings without creative efforts.

Fig. 1 is a schematic perspective view of a reaction apparatus for immobilized ionic liquid preparation according to the present invention;

FIG. 2 is a schematic cross-sectional view of a reaction apparatus for immobilized ionic liquid preparation according to the present invention;

FIG. 3 is a schematic structural diagram of part A of an immobilized ionic liquid preparation reaction device according to the present invention;

fig. 4 is a schematic structural diagram of a part B in the immobilized ionic liquid preparation reaction apparatus according to the present invention.

In the figure: 1. a base; 2. a vertical plate; 21. a bidirectional screw rod; 22. a drive motor; 23. a driving gear; 24. a driven gear; 25. a moving block; 26. a stay bar; 27. a guide post; 271. a scale plate; 28. a lifting plate; 29. a placing table; 3. a hollow slab; 31. a hollow cylinder; 32. a support pillar; 33. a rotating wheel; 34. a strut; 35. a support shaft; 4. a reaction vessel; 41. a vertical tube; 42. a strip-shaped opening; 43. a guide bar; 44. a slider; 45. a connecting pipe; 46. a rotating joint; 47. a side tube; 48. a sleeve.

Detailed Description

The technical solution of the present invention will be clearly and completely described below with reference to the specific embodiments. It is obvious that the described embodiments are only some of the embodiments of the present invention, and not all of them. Based on the embodiments of the present invention, all other embodiments obtained by a person of ordinary skill in the art without creative efforts belong to the protection scope of the present invention.

Referring to fig. 1-4, a reaction device for immobilized ionic liquid preparation, comprising a base 1 and a reaction vessel 4, wherein two sides of the top of the base 1 are fixedly provided with vertical plates 2, the top of one side of each of the two vertical plates 2 close to each other is rotatably provided with a supporting shaft 35, one end of each of the two supporting shafts 35 close to each other is fixedly provided with a same hollow plate 3, the hollow plate 3 is provided with a mounting opening, the reaction vessel 4 is detachably mounted in the mounting opening, one side of each of the two vertical plates 2 close to each other is slidably provided with a same lifting plate 28, the lifting plate 28 is fixedly provided with a placing table 29, the top side of the base 1 and one side of each of the two vertical plates 2 close to each other are provided with a same lifting mechanism, the inner side wall of the hollow plate 3 is fixedly provided with a plurality of hollow cylinders 31, the plurality of hollow cylinders 31 are slidably provided with supporting columns 32, one ends of the plurality of supporting columns 32 close to each other are rotatably provided with a rotating wheel 33, and a plurality of runners 33 all abut against the reaction vessel 4, a vertical pipe 41 is fixedly installed at the top of the reaction vessel 4, two strip-shaped openings 42 are formed in the outer peripheral surface of the reaction vessel 4, guide rods 43 are vertically and fixedly installed in the two strip-shaped openings 42, sliders 44 are slidably installed on the guide rods 43, the sliders 44 can be guided through the guide rods 43, so that the sliders 44 can stably slide along the strip-shaped openings 42, a connecting pipe 45 is fixedly installed on the sliders 44, a rotary joint 46 is fixedly installed at one end, far away from the reaction vessel 4, of the connecting pipe 45, a side pipe 47 is rotatably installed on the rotary joint 46, the opening direction of the side pipe 47 can be conveniently adjusted through the rotary joint 46, a heat insulation sleeve is fixedly installed on the side pipe 47 in a fixing mode, and the side pipe 47 can be conveniently operated through the heat insulation sleeve.

In this embodiment, a pushing spring is fixedly installed at one end of the supporting column 32 far away from the rotating wheel 33, one end of the pushing spring far away from the supporting column 32 is fixedly connected with the inner wall of one side of the hollow cylinder 31, and the rotating wheel 33 and the reaction vessel 4 can be kept in an abutting state through the pushing spring.

In this embodiment, the lifting mechanism includes a driving motor 22, a bidirectional screw rod 21, two moving blocks 25, a driving gear 23, a driven gear 24 and two support rods 26, the bidirectional screw rod 21 is horizontally and rotatably mounted on the two vertical plates 2, the driving motor 22 is fixedly mounted on the vertical plate 2 on the right side, the driving gear 23 and the driven gear 24 are respectively and fixedly sleeved on the output shaft of the driving motor 22 and the bidirectional screw rod 21, the driving gear 23 is engaged with the driven gear 24, the two moving blocks 25 are both threadedly mounted on the bidirectional screw rod 21, the two support rods 26 are respectively and rotatably mounted on the corresponding moving blocks 25, the two bottom ends of the lifting plate 28 are both fixedly mounted with fixing plates, one ends of the two support rods 26 away from the moving blocks 25 are respectively and rotatably connected with the corresponding fixing plates, the elevating mechanism can control the elevating plate 28 to perform the elevating operation, so that the height of the placing table 29 can be adjusted.

In this embodiment, last fixed mounting of runner 33 has branch 34, and the one end fixed mounting that runner 33 was kept away from to branch 34 has the anti-skidding rubber slab, and after reaction vessel 4 got into the installing port and contacted with runner 33, can drive runner 33 and rotate under the effect of reaction vessel 4 dead weight to can make branch 34 drive anti-skidding rubber slab and reaction vessel 4 and get into the butt state, and then can fix the position of reaction vessel 4.

In this embodiment, two equal fixed mounting in one side that two risers 2 are close to each other have two extension boards, lie in vertical fixed mounting have two guide posts 27 on two extension boards with one side, four guide posts 27 all with lifter plate 28 sliding connection, be provided with scale plate 271 on the guide post 27, can lead to lifter plate 28 through guide post 27 to can make lifter plate 28 keep stable going up and down, can carry out effectual control to the height of lifter plate 28 under the cooperation of scale plate 271 simultaneously.

In this embodiment, a sleeve 48 is installed on the inner side wall of the reaction vessel 4 in a sliding and sealing manner, one end of the connecting pipe 45, which is far away from the rotary joint 46, penetrates through the sleeve 48 and is communicated with the reaction vessel 4, and the sleeve 48 installed in a sliding and sealing manner can prevent the position of the strip-shaped opening 42 from being air-leaked in the using process.

In this embodiment, the fixed cover of one end that hollow plate 3 was kept away from to back shaft 35 that is located the right side is equipped with the rolling disc, and the thread mounting has spacing lead screw on the rolling disc, the one side that hollow plate 3 was kept away from to riser 2 that is located the right side has seted up a plurality of spacing screws for the centre of a circle based on back shaft 35, spacing lead screw thread mounting is in the spacing screw that corresponds, and the fixed cover of one end that riser 2 was kept away from to spacing lead screw is equipped with anti-skidding handle cover, it can control hollow plate 3 and deflect to rotate back shaft 35 through the rolling disc, can carry on spacingly to the rolling disc under the cooperation of spacing lead screw and spacing screw simultaneously, thereby can fix the deflection angle of hollow plate 3.

The working principle is as follows: when the device is used, firstly, the device is placed on an operation table, a power supply is connected, a heating device is placed on a placing table, a driving motor 22 is started, the driving motor 22 drives a bidirectional screw rod 21 to rotate through a driving gear 23 and a driven gear 24, so that two moving blocks 25 can be controlled to move towards directions far away from each other, a lifting plate 28 can be upwards lifted under the coordination of a support rod 26, the lifting plate 28 can keep stable movement under the coordination of a guide column 27, meanwhile, the height of the lifting plate 28 can be accurately controlled under the coordination of a scale plate 271, a reaction container 4 is downwards placed through a mounting opening, and because the bottom of the reaction container 4 is arranged in a spherical surface manner, the support column 32 can be pushed to slide towards the position far away from the mounting opening along a hollow cylinder 31 when the reaction container 4 is in contact with a rotating wheel 33, and the rotating wheel 33 rotates along with the movement of the reaction container 4, so that the support rod 34 drives the anti-skid rubber plate to abut against the reaction vessel 4, thereby fixing the reaction vessel 4, conveying the raw material for preparing immobilized ionic liquid into the reaction vessel through the side pipe 47 and the vertical pipe 41, heating the reaction vessel 4 through the heating device, when the reaction vessel 4 needs to be deflected, the limiting screw rod is rotated and separated from the limiting screw hole, then the rotating disc is rotated, the angle of the hollow plate 3 can be adjusted under the coordination of the supporting shaft 35, after the adjustment is finished, the limiting screw rod is screwed into the corresponding limiting screw hole, the handheld heat insulation sleeve is convenient to adjust the side pipe 47 under the coordination of the rotating joint 46, the height of the side pipe 47 can be adjusted according to requirements through the matching of the strip-shaped opening 42, the slide block 44, the guide rod 43 and other components, meanwhile, the liquid leakage at the position of the strip-shaped opening 42 in the use process can be avoided under the action of the sleeve 48.

The above details are provided for the immobilized ionic liquid preparation reaction device provided by the utility model. The principles and embodiments of the present invention have been explained herein using specific embodiments, which are merely used to help understand the method and its core ideas of the present invention. It should be noted that, for those skilled in the art, without departing from the principle of the present invention, the present invention can be further modified and modified, and such modifications and modifications also fall within the scope of the appended claims.

Claims

1. The reaction device for preparing the immobilized ionic liquid comprises a base (1) and a reaction container (4), and is characterized in that vertical plates (2) are fixedly mounted on two sides of the top of the base (1), supporting shafts (35) are rotatably mounted on the tops of two sides, close to each other, of the two vertical plates (2), one end, close to each other, of each supporting shaft (35) is fixedly mounted with a same hollow plate (3), a mounting opening is formed in each hollow plate (3), the reaction container (4) is detachably mounted in the mounting opening, one side, close to each other, of each vertical plate (2) is slidably mounted with a same lifting plate (28), a placing table (29) is fixedly mounted on each lifting plate (28), one side, close to each other, of the top side of the base (1) and one side, close to each vertical plate (2), of each vertical plate (3) is fixedly mounted with a plurality of hollow cylinders (31), equal slidable mounting has support column (32) in a plurality of hollow section of thick bamboo (31), and the one end that a plurality of support columns (32) are close to each other all rotates and installs runner (33), and a plurality of runner (33) all with reaction vessel (4) looks butt, the top fixed mounting of reaction vessel (4) has standpipe (41), seted up two bar mouth (42) on the outer peripheral face of reaction vessel (4), equal vertical fixed mounting has guide bar (43) in two bar mouth (42), slidable mounting has slider (44) on guide bar (43), fixed mounting has connecting pipe (45) on slider (44), the one end fixed mounting that reaction vessel (4) were kept away from in connecting pipe (45) has rotary joint (46), rotary joint (46) are gone up to rotate and are installed side pipe (47), and fixed cover is equipped with the radiation shield on side pipe (47).

2. The apparatus for preparing immobilized ionic liquid according to claim 1, wherein: and one end of the supporting column (32) far away from the rotating wheel (33) is fixedly provided with a pushing spring, and one end of the pushing spring far away from the supporting column (32) is fixedly connected with the inner wall of one side of the hollow cylinder (31).

3. The apparatus for preparing immobilized ionic liquid according to claim 1, wherein: the lifting mechanism comprises a driving motor (22), a bidirectional screw rod (21), two moving blocks (25), a driving gear (23), a driven gear (24) and two support rods (26), two-way lead screw (21) horizontal rotation is installed on two riser (2), driving motor (22) fixed mounting is on riser (2) on right side, driving gear (23) and driven gear (24) fixed cover are respectively established on the output shaft of driving motor (22) and two-way lead screw (21), driving gear (23) and driven gear (24) mesh mutually, two equal screw thread installations in movable block (25) are on two-way lead screw (21), two vaulting poles (26) rotate respectively and install on corresponding movable block (25), the equal fixed mounting in bottom side both ends of lifter plate (28) has the fixed plate, the one end that movable block (25) were kept away from in two vaulting poles (26) is connected with the fixed plate rotation that corresponds respectively.

4. The apparatus for preparing immobilized ionic liquid according to claim 1, wherein: the last fixed mounting of runner (33) has branch (34), and the one end fixed mounting that runner (33) were kept away from in branch (34) has anti-skidding rubber slab, and after reaction vessel (4) got into the installing port and contacted runner (33), anti-skidding rubber slab and reaction vessel (4) looks butt.

5. The apparatus for preparing immobilized ionic liquid according to claim 1, wherein: two supporting plates are fixedly mounted on one sides, close to each other, of the two vertical plates (2), two guide columns (27) are vertically and fixedly mounted on the two supporting plates on the same side, the four guide columns (27) are connected with the lifting plate (28) in a sliding mode, and a scale plate (271) is arranged on each guide column (27).

6. The apparatus for preparing immobilized ionic liquid according to claim 1, wherein: and a sleeve (48) is arranged on the inner side wall of the reaction container (4) in a sliding and sealing manner, and one end, far away from the rotating joint (46), of the connecting pipe (45) penetrates through the sleeve (48) and is communicated with the reaction container (4).

7. The apparatus for preparing immobilized ionic liquid according to claim 1, wherein: the fixed cover of one end that is located back shaft (35) on right side and keeps away from hollow slab (3) is equipped with the rolling disc, and the thread installs spacing lead screw on the rolling disc, and one side that is located riser (2) on right side and keeps away from hollow slab (3) has seted up a plurality of spacing screws for the centre of a circle based on back shaft (35), and spacing lead screw thread is installed in the spacing screw that corresponds, and the fixed cover of one end that riser (2) were kept away from to spacing lead screw is equipped with the anti-skidding handle cover.