CN216358965U - Batch feeding reactor for dimethyl disulfide vulcanization processing - Google Patents

Batch feeding reactor for dimethyl disulfide vulcanization processing Download PDF

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Publication number
CN216358965U
CN216358965U CN202123060337.6U CN202123060337U CN216358965U CN 216358965 U CN216358965 U CN 216358965U CN 202123060337 U CN202123060337 U CN 202123060337U CN 216358965 U CN216358965 U CN 216358965U
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reaction tank
tank body
dimethyl disulfide
connecting plate
reaction
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CN202123060337.6U
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杨超美
李生军
冯道友
殷大会
王娟娟
曹晓英
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Gansu Qinyu Biotechnology Co ltd
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Gansu Qinyu Biotechnology Co ltd
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Abstract

The utility model discloses a batch feeding reactor for dimethyl disulfide vulcanization processing, which comprises: the outer side of the upper end of the reaction tank body is fixedly provided with an upper connecting cover through a bolt, the upper end of the reaction tank body is provided with a first feeding pipe, and the rear side of the upper end face of the upper connecting cover is provided with a second feeding pipe; the driving motor is arranged in the middle of the upper end face of the upper connecting cover, and a stirring rod positioned on the inner side of the reaction tank body is arranged on the lower end side of the driving motor; the connecting plate is fixedly arranged at the middle end of the inner side of the reaction tank body, and the lower end of the inner side of the reaction tank body is provided with a reaction cavity; the installation cavity is arranged inside the lower wall end of the reaction tank body, and the inner side end of the installation cavity is provided with the heating ring. This dimethyl disulfide vulcanization processing is with batch feeding reactor is provided with 2 first inlet pipes of group, can be used to batch feeding, possesses better even feeding structure simultaneously, avoids the material to take place the phenomenon of jam at the feeding in-process, and has the function of heating during the reaction.

Description

Batch feeding reactor for dimethyl disulfide vulcanization processing
Technical Field
The utility model relates to the technical field of dimethyl disulfide vulcanization processing, in particular to a batch feeding reactor for dimethyl disulfide vulcanization processing.
Background
Dimethyl disulfide is a chemical substance mainly used as a solvent and a pesticide intermediate, and is also a main raw material of methylsulfonyl chloride and a methanesulfonic acid product, and a reactor is required to be used in the vulcanization processing process of the dimethyl disulfide.
The reactor with stirring and mixing for the safe production of the dimethyl disulfide with the publication number of CN209752863U in the Chinese patent authorization comprises a mixing reactor body, wherein a discharge hole is formed in the center of the bottom shell of the mixing reactor body, and a stirring motor is spirally fixed at the center of the top of the mixing reactor body through a motor fixing seat. According to the utility model, the first connecting branch pipe and the second connecting branch pipe are connected to the ingredient inlet, so that ingredients and a catalyst can be added into the ingredient inlet through the first connecting branch pipe and the second connecting branch pipe simultaneously, then the stirring rod is driven to rotate through the mixing motor, the ingredients and the catalyst are firstly mixed through the mixing stirring frame and the spiral stirrer on the stirring rod, and then the ingredients and the catalyst enter the mixing reactor body to be mixed with raw materials, so that the steps of mixing the catalyst are reduced, the production and preparation are more convenient, and the working efficiency is improved.
However, the above prior art solutions have the following drawbacks: the batch feeding reactor for the dimethyl disulfide vulcanization processing is not provided with a good uniform feeding structure, so that the phenomenon that materials are easily blocked in the feeding process is caused, and the batch feeding reactor does not have a heating function during reaction, so that certain use defects exist.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide a batch feeding reactor for dimethyl disulfide vulcanization processing, which aims to solve the problems that the existing batch feeding reactor in the background art does not have a good uniform feeding structure, so that the material is easy to block in the feeding process, and does not have a heating function during reaction, so that certain use defects exist.
In order to achieve the purpose, the utility model provides the following technical scheme: a batch feed reactor for dimethyl disulfide vulcanization processing, comprising:
the reaction tank comprises a reaction tank body, wherein an upper connecting cover is fixedly arranged on the outer side of the upper end of the reaction tank body through a bolt, a first feeding pipe is arranged at the upper end of the reaction tank body, an installation assembly is arranged in the first feeding pipe, and a second feeding pipe is arranged on the rear side of the upper end face of the upper connecting cover;
the driving motor is arranged in the middle of the upper end face of the upper connecting cover, a stirring rod positioned on the inner side of the reaction tank body is arranged on the lower end side of the driving motor, and a connecting plate is fixedly arranged at the outer side end of the stirring rod;
the connecting plate is fixedly arranged at the middle end of the inner side of the reaction tank body, a reaction cavity is arranged at the lower end of the inner side of the reaction tank body, and a discharge pipe is arranged on the lower end surface of the reaction tank body;
the installation cavity is arranged inside the lower wall end of the reaction tank body, the heating ring is installed at the inner side end of the installation cavity, and the observation window is arranged at the front end of the reaction tank body.
Preferably, the mounting assembly comprises a fixing rod and a mounting block;
the fixed rod is arranged at the middle end of the inner side of the first feeding pipe;
and the mounting block is fixedly mounted at the inner side end of the fixed rod monomer.
Preferably, the fixing rods are circumferentially distributed at equal angles on the outer side of the lower end of the mounting block, and the mounting block is conical.
Preferably, the connecting plate forms a rotating structure on the inner side of the reaction tank body through a stirring rod, and the longitudinal section of the connecting plate is U-shaped.
Preferably, the connecting plates are located right below the connecting plates, and hole structures for blanking are formed in the middle ends of the connecting plates in a penetrating mode.
Preferably, the heating ring is arranged in the reaction tank body at equal intervals through the installation cavity, and the heating ring is positioned at the outer side end of the reaction cavity.
Compared with the prior art, the utility model has the beneficial effects that: the batch feeding reactor for the dimethyl disulfide vulcanization processing is provided with 2 groups of first feeding pipes, can be used for batch feeding, has a better uniform feeding structure, avoids the phenomenon of material blockage in the feeding process, and has a heating function during reaction;
1. the first feeding pipes are arranged in bilateral symmetry about a vertical central axis of the upper connecting cover, and the sealing covers are mounted on the outer sides of the upper ends of the first feeding pipes through hinges, so that batch feeding work can be conveniently carried out through 2 groups of first feeding pipes in the reaction process, and the use is convenient;
2. the material feeding device is characterized in that the material feeding device is arranged at the middle end of the inner side of a first material feeding pipe through a fixing rod, an installation block is fixedly arranged at the inner side end of a fixing rod monomer, the fixing rods are distributed on the outer side of the lower end of the installation block in an equiangular and circumferential manner, the installation block is conical in shape, and the fixing rod and the installation block have the effect of uniform material feeding;
3. the heating ring is arranged in the reaction tank body at equal intervals through the mounting cavity, and the heating ring is located at the outer side end of the reaction cavity, so that the heating work of the reaction cavity is facilitated through the heating ring in the reaction process, and the better vulcanization reaction is facilitated.
Drawings
FIG. 1 is a schematic front sectional view of the present invention;
FIG. 2 is a schematic top view of the cross-sectional structure of the present invention;
FIG. 3 is a schematic side view of the present invention;
fig. 4 is a schematic view of the overall structure of the mounting assembly of the present invention.
In the figure: 1. a reaction tank body; 2. an upper connecting cover; 3. a first feed tube; 4. mounting the component; 401. fixing the rod; 402. mounting blocks; 5. a drive motor; 6. a stirring rod; 7. a connecting plate; 8. a connector tile; 9. a reaction chamber; 10. a discharge pipe; 11. a mounting cavity; 12. a heating ring; 13. an observation window; 14. a second feed tube.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-4, the present invention provides a technical solution: a batch feeding reactor for dimethyl disulfide vulcanization processing comprises an upper connecting cover 2 fixedly installed on the outer side of the upper end of a reaction tank body 1 through bolts, a first feeding pipe 3 is arranged on the upper end of the reaction tank body 1, an installation component 4 is installed inside the first feeding pipe 3, a second feeding pipe 14 is arranged on the rear side of the upper end face of the upper connecting cover 2, a driving motor 5 is installed in the middle of the upper end face of the upper connecting cover 2, a stirring rod 6 located on the inner side of the reaction tank body 1 is arranged on the lower end side of the driving motor 5, a connecting plate 7 is fixedly installed on the outer side of the stirring rod 6, a connecting plate 8 is fixedly installed on the inner middle end of the reaction tank body 1, a reaction cavity 9 is arranged on the lower end of the inner side of the reaction tank body 1, a discharging pipe 10 is installed on the lower end of the reaction tank body 1, an installation cavity 11 is arranged inside the lower wall end of the reaction tank body 1, and a heating ring 12 is installed on the inner side end of the installation cavity 11, and the front end of the reaction tank body 1 is provided with an observation window 13, and the observation window 13 is combined to form a batch feeding reactor for the dimethyl disulfide vulcanization processing.
When the batch feeding reactor for the dimethyl disulfide vulcanization processing is used, as shown in fig. 1 and 4, firstly, the whole is stably placed on a designated plane through a foot rest, then a driving motor 5 arranged on the outer side of the upper end of an upper connecting cover 2 is opened, so that a stirring rod 6 rotates on the inner side of a reaction tank body 1, at the moment, a sealing cover hinged on the outer side of the upper end of a first feeding pipe 3 is opened, and materials required by the vulcanization reaction are injected into the reaction tank body 1 through the first feeding pipe 3;
because dead lever 401 installs in the inboard middle-end of first inlet pipe 3, and installation piece 402 fixed mounting is in dead lever 401 monomer medial extremity, dead lever 401 is the equal angle circumference distribution in the lower extreme outside of installation piece 402 simultaneously, and the shape of installation piece 402 is the taper shape, installation piece 402 passes through dead lever 401 fixed mounting in the medial extremity of first inlet pipe 3, dead lever 401 and installation piece 402 have the effect of even feeding to the material simultaneously, avoid the material to take place the phenomenon of jam in the feeding process, and be convenient for carry out batch feeding work through 2 first inlet pipes 3 of group in the reaction process.
As shown in fig. 1 and fig. 2, when feeding, the catalyst required by the reaction is injected into the inner side of the reaction tank body 1 through the second feeding pipe 14, at the moment, the stirring rod 6 and the connecting plate 7 have the stirring and mixing effects on the material and the catalyst, so that the reaction can be performed sufficiently, because the connecting plate 7 forms a rotating structure in the inner side of the reaction tank body 1 through the stirring rod 6, and the longitudinal section of the connecting plate 7 is in a U shape, during stirring, the connecting plate 7 enhances the stirring effect on the material, and meanwhile, the connecting plate 7 is connected with the inner wall of the reaction tank body 1, so that the material can be effectively prevented from being adsorbed on the inner wall of the reaction tank body 1.
Specifically, as shown in fig. 1 and 3, the connection plate 8 is located under the connection plate 7, and the middle end of the connection plate 8 is penetrated through and provided with a hole structure for blanking, the materials subjected to intensive mixing and stirring fall into the inner side of the reaction cavity 9 through the hole structure inside the connection plate 8, at the moment, the heating ring 12 which is installed inside the reaction tank body 1 at equal intervals through the installation cavity 11 starts to perform heating operation, so that better vulcanization reaction operation is facilitated, the work efficiency of the vulcanization reaction is improved, after the reaction is completed, the produced materials can be collected through the discharge pipe 10, the inside of the reaction tank body 1 can be observed through the observation window 13 in the reaction process, and the method is the use method of the batch feeding reactor for dimethyl disulfide vulcanization processing.
The standard parts used in the utility model can be purchased from the market, the special-shaped parts can be customized according to the description of the specification and the accompanying drawings, the specific connection mode of each part adopts conventional means such as bolts, rivets, welding and the like mature in the prior art, the machinery, parts and equipment adopt conventional models in the prior art, and the circuit connection adopts the conventional connection mode in the prior art, and the details are not described, and the content not described in detail in the specification belongs to the prior art known by persons skilled in the art.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that various changes in the embodiments and/or modifications of the utility model can be made, and equivalents and modifications of some features of the utility model can be made without departing from the spirit and scope of the utility model.

Claims (6)

1. A batch feed reactor for dimethyl disulfide vulcanization processing, characterized in that: the method comprises the following steps:
the reaction tank comprises a reaction tank body, wherein an upper connecting cover is fixedly arranged on the outer side of the upper end of the reaction tank body through a bolt, a first feeding pipe is arranged at the upper end of the reaction tank body, an installation assembly is arranged in the first feeding pipe, and a second feeding pipe is arranged on the rear side of the upper end face of the upper connecting cover;
the driving motor is arranged in the middle of the upper end face of the upper connecting cover, a stirring rod positioned on the inner side of the reaction tank body is arranged on the lower end side of the driving motor, and a connecting plate is fixedly arranged at the outer side end of the stirring rod;
the connecting plate is fixedly arranged at the middle end of the inner side of the reaction tank body, a reaction cavity is arranged at the lower end of the inner side of the reaction tank body, and a discharge pipe is arranged on the lower end surface of the reaction tank body;
the installation cavity is arranged inside the lower wall end of the reaction tank body, the heating ring is installed at the inner side end of the installation cavity, and the observation window is arranged at the front end of the reaction tank body.
2. The batch feed reactor for dimethyl disulfide vulcanization processing according to claim 1, wherein: the mounting assembly comprises a fixing rod and a mounting block;
the fixed rod is arranged at the middle end of the inner side of the first feeding pipe;
and the mounting block is fixedly mounted at the inner side end of the fixed rod monomer.
3. The batch feed reactor for dimethyl disulfide vulcanization processing according to claim 2, characterized by: the fixed rods are distributed on the outer side of the lower end of the mounting block in an equiangular and circumferential manner, and the mounting block is conical.
4. The batch feed reactor for dimethyl disulfide vulcanization processing according to claim 1, wherein: the connecting plate passes through the puddler and constitutes revolution mechanic at the inboard of retort body, and the longitudinal section of connecting plate is "U" style of calligraphy.
5. The batch feed reactor for dimethyl disulfide vulcanization processing according to claim 1, wherein: the connecting plate is located under the connecting plate, and a hole structure for blanking is arranged at the middle end of the connecting plate in a penetrating mode.
6. The batch feed reactor for dimethyl disulfide vulcanization processing according to claim 1, wherein: the heating ring is arranged in the reaction tank body at equal intervals through the installation cavity, and the heating ring is located at the outer side end of the reaction cavity.
CN202123060337.6U 2021-12-07 2021-12-07 Batch feeding reactor for dimethyl disulfide vulcanization processing Active CN216358965U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202123060337.6U CN216358965U (en) 2021-12-07 2021-12-07 Batch feeding reactor for dimethyl disulfide vulcanization processing

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202123060337.6U CN216358965U (en) 2021-12-07 2021-12-07 Batch feeding reactor for dimethyl disulfide vulcanization processing

Publications (1)

Publication Number Publication Date
CN216358965U true CN216358965U (en) 2022-04-22

Family

ID=81191824

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202123060337.6U Active CN216358965U (en) 2021-12-07 2021-12-07 Batch feeding reactor for dimethyl disulfide vulcanization processing

Country Status (1)

Country Link
CN (1) CN216358965U (en)

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